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Synthesis and Characterization of Novel Magnetic Poly(urethane-imide)/Fe3O4@SiO2–NH2 Nanocomposites

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Abstract

Poly(urethane-imide)/Fe3O4@SiO2–NH2 nanocomposites were synthesized by the reaction of 4,4′-diphenylmethane diisocyanate (MDI), polypropylene glycol (PPG), 4,4'-(hexafluoroisopropylidene) diphthalic anhydride and Fe3O4@SiO2–NH2 nanoparticles in propylene carbonate (PC) as an alternative green solvent. Poly(urethane-imide)s combined with Fe3O4@SiO2–NH2 nanoparticles (NPs) at various NPs ranging from loadings levels of 0.5 and 3.5 pbw were prepared and characterized by fourier transform infrared spectroscopy (FT-IR), proton nuclear magnetic resonance spectroscopy (1H NMR), thermogravimetric analysis (TGA), X-ray diffraction (XRD) and vibrating sample magnetometery (VSM). The results showed the performances of Fe3O4@SiO2–NH2 nanoparticles in improving of thermal resistance and magnetic properties of PUI/Fe3O4@SiO2–NH2 in comparison with pristine poly(urethane-imide).

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Imam Khomeini International University, P.O. Box 288, Qazvin, Iran

    Baharak Pooladian & Mir Mohammad Alavi Nikje

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  1. Baharak Pooladian
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  2. Mir Mohammad Alavi Nikje
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Correspondence to Mir Mohammad Alavi Nikje.

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Pooladian, B., Nikje, M.M.A. Synthesis and Characterization of Novel Magnetic Poly(urethane-imide)/Fe3O4@SiO2–NH2 Nanocomposites. Russ J Appl Chem 91, 671–679 (2018). https://doi.org/10.1134/S1070427218040213

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  • DOI: https://doi.org/10.1134/S1070427218040213

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