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Columns for cyclic extraction-chromatographic device

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Abstract

Three constructions of the columns of extraction-chromatographic device operating in cyclic mode have been compared. Experiments have been conducted with = shots containing caffeine, coumarin, and salicylic and acetylsalicylic acids using hexane-isopropyl alcohol-water biphase solvent system at a 1 : 1 : 1 ratio, respectively. All columns have demonstrated fairly high effectiveness. The certain advantage of the column with stirrers is the possibility to control contact time of phases.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, Russia

    A. A. Erastov, N. V. Kodin, Yu. A. Zakhodyaeva & A. E. Kostanyan

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  1. A. A. Erastov
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  2. N. V. Kodin
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  3. Yu. A. Zakhodyaeva
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  4. A. E. Kostanyan
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Corresponding author

Correspondence to A. E. Kostanyan.

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Original Russian Text © A.A. Erastov, N.V. Kodin, Yu.A. Zakhodyaeva, A.E. Kostanyan, 2013, published in Khimicheskaya Tekhnologiya, 2013, Vol. 14, No. 10, pp. 631–635.

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Erastov, A.A., Kodin, N.V., Zakhodyaeva, Y.A. et al. Columns for cyclic extraction-chromatographic device. Theor Found Chem Eng 48, 733–736 (2014). https://doi.org/10.1134/S0040579514050042

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  • DOI: https://doi.org/10.1134/S0040579514050042

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