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Synthesis, Spectroscopic Characterization, and XAFS Studies of Cu(II) Complexes with Bidentate Schiff Bases Derived from 2-Hydroxy-1-Naphthaldehyde

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Abstract

The new complexes of compositions [CuL1] and [CuL2] were prepared by treating with [1-(((4-nitrophenyl)imino)methyl)naphthalene-2-ol] (L1) and [1-(((4-chlorophenyl)imino)methyl)naphthalene-2-ol] (L2) ligands with Cu(OAc)2·H2O, respectively. Both Schiff base ligand act as bidentate ligands. The complexes were investigated by single crystal X-ray diffraction (XRD), X-ray absorption fine structure (XAFS), Fourier transform infrared spectroscopy (FTIR), and field emission scanning electron microscopy (FE-SEM). The X-ray diffraction studies suggest a monoclinic crystal system for the complexes.

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ACKNOWLEDGMENTS

I extend my thanks to UGC-DAE- Consortium for Scientific Research, Indore and RRCAT (Raja Ramanna Center for Advanced Technology), Indore for providing different experimental facilities in the lab.

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Authors and Affiliations

  1. School of Physics, Devi Ahilya Vishwavidyalaya, Indore, India

    Kritika Shukla & Ashutosh Mishra

  2. Govt. Holkar (Model, Autonomous) Science College, Indore, India

    Kritika Shukla & Pradeep Sharma

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  1. Kritika Shukla
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  2. Pradeep Sharma
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Correspondence to Kritika Shukla.

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Shukla, K., Sharma, P. & Mishra, A. Synthesis, Spectroscopic Characterization, and XAFS Studies of Cu(II) Complexes with Bidentate Schiff Bases Derived from 2-Hydroxy-1-Naphthaldehyde. Russ. J. Phys. Chem. 95 (Suppl 1), S128–S139 (2021). https://doi.org/10.1134/S0036024421140211

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