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Hydrothermal Synthesis and Properties of Chitosan–Silver Nanocomposites

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Abstract

A facile “green chemistry” hydrothermal method of chitosan-Ag nanoparticles (NPs) synthesis has been proposed. Chitosans of different molecular weight (from 20 to 1200 kDa) have been used as reducing agents and particle stabilizers. The obtained chitosan–Ag nanocomposites have been studied by UV–Vis and IR spectroscopy, X-ray powder diffraction analysis, and transmission electron microscopy. Nanocomposites have a “core-shell” structure, spherical shape with size up to 60.0 nm and the surface ξ-potential value >40.0 mV. Optimal parameters of synthesis (time, temperature, molecular weight of chitosan) of chitosan–Ag nanoparticles with highest antimicrobial activity against gram-positive and gram-negative bacteria and fungi have been found.

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Funding

This work was financially supported by the State Committee for Science and Technology and the Belarusian Republican Foundation for Fundamental Research (project no. X20SRBG-002).

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Authors and Affiliations

  1. Institute of Chemistry of New Materials, 220141, Minsk, Belarus

    K. S. Hileuskaya, M. E. Mashkin, A. N. Kraskouski, V. S. Kabanava, V. I. Kulikouskaya & V. E. Agabekov

  2. Vyshelesski Institute of Experimental Veterinary Medicine, 220063, Minsk, Belarus

    E. A. Stepanova & I. I. Kuzminski

Authors
  1. K. S. Hileuskaya
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  2. M. E. Mashkin
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  3. A. N. Kraskouski
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  4. V. S. Kabanava
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  5. E. A. Stepanova
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  6. I. I. Kuzminski
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  7. V. I. Kulikouskaya
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  8. V. E. Agabekov
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Contributions

K.S. Hileuskaya devised and developed experiment, M.E. Mashkin and A.N. Kraskouski synthesized samples and conducted physicochemical study, V.S. Kabanava performed IR spectral study, E.A. Stepanova and I.I. Kuzminski carried out the screening of antimicrobial activity of prepared samples. V.I. Kulikouskaya took part in data treatment. K.S. Hileuskaya, A.N. Kraskouski, and V.E. Agabekov participated in paper writing. All the authors were involved in results discussion.

Corresponding author

Correspondence to K. S. Hileuskaya.

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CONFLICT OF INTEREST

The authors declare no conflict of interest.

ADDITIONAL INFORMATION

This paper was reported on the Sixth Interdisciplinary Scientific Forum with International Participation “New Materials and Promising Technologies”, Moscow, November 23–26, 2020. https://n-materials.ru.

Additional information

Translated by I. Kudryavtsev

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Hileuskaya, K.S., Mashkin, M.E., Kraskouski, A.N. et al. Hydrothermal Synthesis and Properties of Chitosan–Silver Nanocomposites. Russ. J. Inorg. Chem. 66, 1128–1134 (2021). https://doi.org/10.1134/S0036023621080064

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  • DOI: https://doi.org/10.1134/S0036023621080064

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