Abstract
Novel compounds 2-(2-(2-hydroxy-4-nitrophenyl) hydrazono)-1,3-diphenyl propane-1,3-dione and 2-(2-(2-hydroxy-4-nitrophenyl) hydrazono)-1-phenyl butane-1,3-dione are prepared on the base of β-diketones. Crystal and molecular structures of synthesized compounds are determined by X-ray diffraction analysis. The crystals are found to be monoclinic. The compounds are represented only by their hydrazo forms. The structural data for the two obtained compounds are compared with previously reported data.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
M. A. Magerramov, R. A. Alieva, R. Z. Nazarova et al. J. Struct. Chem., 2011, 52(1), 198.
M. A. Magerramov, R. A. Alieva, R. N. Sulhnejat et al. Russ. J. Coord. Chem., 2011, 37(1), 45.
M. A. Magerramov, R. A. Alieva, R. Z. Nazarova et al. J. Struct. Chem., 2016, 57(4), 819.
P. A. Stabnikov, L. G. Bulusheva, N. I. Alferova et al. J. Struct. Chem., 2012, 53(4), 740.
P. A. Stabnikov, I. A. Baydina, S. V. Sysoev et al. J. Struct. Chem., 2003, 44(6), 1054.
I. A. Baydina, P. A. Stabnikov, A. D. Vasiliev et al. J. Struct. Chem., 2014, 45(4), 671.
G. I. Zharkova, S. V. Sysoev, I. A. Baidina et al. J. Struct. Chem., 2015, 46(3), 494.
N. B. Morozova, P. A. Stabnikov, I. A. Baidina et al. J. Struct. Chem., 2007, 48(5), 889.
N. V. Kuratyeva, E. S. Vikulova, A. D. Shushanyan et al. J. Struct. Chem., 2017, 58(5), 1004.
K. T. Mahmudov. Investigation and Analytical Application of Complexes of Copper(II) With Azoderivatives of β-Diketones. Dissertation for PhD, Chemistry, Baku, 2006.
G. M. Sheldrick. SHELXTL, 6.12. Structure Determination software Suite, Bruker AXS. Madison, Wisconsin, USA, 2001.
F. H. Allen, D. G. Watson, L. Brammer et al. Int. Tables Crystallogr., 2006, C9(5), 790.
R. Gawinecki, E. Kolehmainen, H. Janota et al. J. Phys. Org. Chem., 2001, 14, 797.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
The authors declare that they have no conflict of interests.
Additional information
Russian Text © The Author(s), 2019, published in Zhurnal Strukturnoi Khimii, 2019, Vol. 60, No. 10, pp. 1746–1752.
Rights and permissions
About this article
Cite this article
Bahmanova, F.N., Tahirli, S.A., Askerov, R.K. et al. X-Ray Diffraction Study of Crystal and Molecular Structures of Azo Compounds of Two β-Diketones. J Struct Chem 60, 1681–1687 (2019). https://doi.org/10.1134/S0022476619100147
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0022476619100147