Skip to main content
Log in

The modified experimental X-ray powder diffraction station on the SR beamline no. 2 of VEPP-3 storage ring

  • Applications of Synchrotron Radiation in Structural Chemistry
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

Modernization of the experimental station mounted on the beamline No. 2 of VEPP-3 synchrotron radiation electron storage ring at Siberian Synchrotron and Terahertz Radiation Center and intended for X-ray diffraction studies of the structure and phase composition of functional materials with high angular resolution and the possibility of using the effect of resonance scattering has been done. In operating mode the diffractometer of the beamline is equipped with a perfect flat analyzer crystal Ge(111), located in front of the detector. XRD patterns can be obtained in the range of photon energies from 7 keV to 18 keV (or wavelength range ~0.18÷0.07 nm). The angular range of the X-ray registration is limited to 2θ = 140°. The work was performed using a complex VEPP-3/VEPP-4.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. G. N. Kulipanov and A. N. Skrinskii, Sov. Phys.–Usp., 20, 550–586 (1977).

    Article  Google Scholar 

  2. Ya. V. Zubavichus and Yu. L. Slovokhotov, Russ. Chem. Rev., 70, No. 5, 373–403 (2001).

    Article  CAS  Google Scholar 

  3. J. Jackson, Classical Electrodynamics, John Wiley (1962).

    Google Scholar 

  4. J.-L. Hodeau, V. Favre-Nicolin, S. Bos, H. Renevier, E. Lorenzo, and J.-F. Berar, Chem. Rev., 101, No. 6, 1843–1868 (2001).

    Article  CAS  Google Scholar 

  5. D. E. Cox, J. B. Hastings, W. Thomlinson, and C. T. Prewitt, Nucl. Instrum. Methods Phys. Res., 208, Nos. 1-3, 573–578 (1983).

    Article  CAS  Google Scholar 

  6. J. B. Hastings, W. Thomlinson, and D. E. Cox, J. Appl. Crystallogr., 17, No. 2, 85–95 (1984).

    Article  CAS  Google Scholar 

  7. R. Pynn, Y. Fujii, and G. Shirane, Acta Crystallogr. A, 39, No. 1, 38–46 (1983).

    Article  Google Scholar 

  8. T. Wroblewski, Acta Crystallogr. A, 47, No. 5, 571–577 (1991).

    Article  Google Scholar 

  9. T. M. Sabine, J. Appl. Crystallogr., 20, No. 1, 23–27 (1987).

    Article  CAS  Google Scholar 

  10. T. M. Sabine, J. Appl. Crystallogr., 20, No. 3, 173–178 (1987).

    Article  CAS  Google Scholar 

  11. https://www-s.nist.gov/srmors/view_detail.cfm?srm=640D.

  12. M. G. Ivanov, A. N. Shmakov, O. Yu. Podyacheva, and Z. R. Ismagilov, J. Struct. Chem., 51, Suppl., S47–S52 (2010).

    Article  Google Scholar 

  13. T. P. Smirnova, A. M. Badalyan, V. O. Borisov, L. V. Yakovkina, V. V. Kaichev, A. N. Shmakov, A. V. Nartova, V. I. Rakhlin, and A. N. Fomina, High Energy Chem., 37, No. 5, 303–309 (2003).

    Article  CAS  Google Scholar 

  14. L. A. Solovyov, S. D. Kirik, A. N. Shmakov, and V. N. Romannikov, Microporous Mesoporous Mater., 44/45, 17–23 (2001).

    Article  Google Scholar 

  15. V. N. Romannikov, S. D. Kirik, L. A. Solov'ev, A. N. Shmakov, A. Yu. Derevyankin, V. B. Fenelonov, O. A. Kholdeeva, O. B. Lapina, and E. A. Paukshtis, Kinet. Catal., 42, No. 6, 857–866 (2001).

    Article  CAS  Google Scholar 

  16. E. M. Moroz, V. P. Pakharukova, and A. N. Shmakov, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 99–101 (2009).

    Article  CAS  Google Scholar 

  17. V. P. Pakharukova, E. M. Moroz, and D. A. Zyuzin, J. Struct. Chem., 51, No. 2, 274–280 (2010).

    Article  CAS  Google Scholar 

  18. A. N. Shmakov, E. M. Moroz, and A. L. Chuvilin, Nucl. Instrum. Methods Phys. Res., Sect. A, 405, Nos. 2/3, 470–472 (1998).

    Article  CAS  Google Scholar 

  19. O. Y. Podyacheva, Z. R. Ismagilov, A. E. Shalagina, V. A. Ushakov, A. N. Shmakov, S. V. Tsybulya, V. V. Kriventsov, and A. V. Ischenko, Carbon, 48, No. 10, 2792–2801 (2010).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to A. N. Shmakov.

Additional information

Translated from Zhurnal Strukturnoi Khimii, Vol. 57, No. 7, pp. 1395-1400, September-October, 2016.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Shmakov, A.N., Tolochko, B.P., Dementiev, E.N. et al. The modified experimental X-ray powder diffraction station on the SR beamline no. 2 of VEPP-3 storage ring. J Struct Chem 57, 1321–1326 (2016). https://doi.org/10.1134/S0022476616070040

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476616070040

Keywords

Navigation