Abstract
Modernization of the experimental station mounted on the beamline No. 2 of VEPP-3 synchrotron radiation electron storage ring at Siberian Synchrotron and Terahertz Radiation Center and intended for X-ray diffraction studies of the structure and phase composition of functional materials with high angular resolution and the possibility of using the effect of resonance scattering has been done. In operating mode the diffractometer of the beamline is equipped with a perfect flat analyzer crystal Ge(111), located in front of the detector. XRD patterns can be obtained in the range of photon energies from 7 keV to 18 keV (or wavelength range ~0.18÷0.07 nm). The angular range of the X-ray registration is limited to 2θ = 140°. The work was performed using a complex VEPP-3/VEPP-4.
Similar content being viewed by others
References
G. N. Kulipanov and A. N. Skrinskii, Sov. Phys.–Usp., 20, 550–586 (1977).
Ya. V. Zubavichus and Yu. L. Slovokhotov, Russ. Chem. Rev., 70, No. 5, 373–403 (2001).
J. Jackson, Classical Electrodynamics, John Wiley (1962).
J.-L. Hodeau, V. Favre-Nicolin, S. Bos, H. Renevier, E. Lorenzo, and J.-F. Berar, Chem. Rev., 101, No. 6, 1843–1868 (2001).
D. E. Cox, J. B. Hastings, W. Thomlinson, and C. T. Prewitt, Nucl. Instrum. Methods Phys. Res., 208, Nos. 1-3, 573–578 (1983).
J. B. Hastings, W. Thomlinson, and D. E. Cox, J. Appl. Crystallogr., 17, No. 2, 85–95 (1984).
R. Pynn, Y. Fujii, and G. Shirane, Acta Crystallogr. A, 39, No. 1, 38–46 (1983).
T. Wroblewski, Acta Crystallogr. A, 47, No. 5, 571–577 (1991).
T. M. Sabine, J. Appl. Crystallogr., 20, No. 1, 23–27 (1987).
T. M. Sabine, J. Appl. Crystallogr., 20, No. 3, 173–178 (1987).
https://www-s.nist.gov/srmors/view_detail.cfm?srm=640D.
M. G. Ivanov, A. N. Shmakov, O. Yu. Podyacheva, and Z. R. Ismagilov, J. Struct. Chem., 51, Suppl., S47–S52 (2010).
T. P. Smirnova, A. M. Badalyan, V. O. Borisov, L. V. Yakovkina, V. V. Kaichev, A. N. Shmakov, A. V. Nartova, V. I. Rakhlin, and A. N. Fomina, High Energy Chem., 37, No. 5, 303–309 (2003).
L. A. Solovyov, S. D. Kirik, A. N. Shmakov, and V. N. Romannikov, Microporous Mesoporous Mater., 44/45, 17–23 (2001).
V. N. Romannikov, S. D. Kirik, L. A. Solov'ev, A. N. Shmakov, A. Yu. Derevyankin, V. B. Fenelonov, O. A. Kholdeeva, O. B. Lapina, and E. A. Paukshtis, Kinet. Catal., 42, No. 6, 857–866 (2001).
E. M. Moroz, V. P. Pakharukova, and A. N. Shmakov, Nucl. Instrum. Methods Phys. Res., Sect. A, 603, Nos. 1/2, 99–101 (2009).
V. P. Pakharukova, E. M. Moroz, and D. A. Zyuzin, J. Struct. Chem., 51, No. 2, 274–280 (2010).
A. N. Shmakov, E. M. Moroz, and A. L. Chuvilin, Nucl. Instrum. Methods Phys. Res., Sect. A, 405, Nos. 2/3, 470–472 (1998).
O. Y. Podyacheva, Z. R. Ismagilov, A. E. Shalagina, V. A. Ushakov, A. N. Shmakov, S. V. Tsybulya, V. V. Kriventsov, and A. V. Ischenko, Carbon, 48, No. 10, 2792–2801 (2010).
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Zhurnal Strukturnoi Khimii, Vol. 57, No. 7, pp. 1395-1400, September-October, 2016.
Rights and permissions
About this article
Cite this article
Shmakov, A.N., Tolochko, B.P., Dementiev, E.N. et al. The modified experimental X-ray powder diffraction station on the SR beamline no. 2 of VEPP-3 storage ring. J Struct Chem 57, 1321–1326 (2016). https://doi.org/10.1134/S0022476616070040
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0022476616070040