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Thermal decomposition of layered double hydroxides Mg-Al, Ni-Al, Mg-Ga: Structural features of hydroxide, dehydrated, and oxide phases

  • The Bridging and Bonding Role of Crystallography
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Abstract

The analysis of the literature data reveals that, as a rule, layered double hydroxides prepared by co-precipitation have an imperfect structure; however, there are different viewpoints on the type of the defects. Thermal decomposition of Mg-Al, Mg-Ga, and Ni-Al hydroxides occurs through dehydration, dehydroxylation, and decarbonization. The first stage affords a layered dehydrated phase with a strongly disordered structure, which is a subject of controversy. Also, the question on the diffusion of cations during thermolysis is still open, i.e., whether the Mg-Al, Mg-Ga and Ni-Al systems degrade with the development of a nanoheterogenous oxide systems or a single-phase mixed oxide, but with very defective structure, is formed.

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Authors and Affiliations

  1. Institute of Hydrocarbons Processing, Siberian Branch, Russian Academy of Sciences, Omsk, Russia

    N. N. Leont’eva & V. A. Drozdov

  2. Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    S. V. Cherepanova

  3. Novosibirsk State University, Novosibirsk, Russia

    S. V. Cherepanova

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  1. N. N. Leont’eva
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  3. V. A. Drozdov
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Correspondence to S. V. Cherepanova.

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Original Russian Text © 2014 N. N. Leont’eva, S. V. Cherepanova, V. A. Drozdov.

__________

Translated from Zhurnal Strukturnoi Khimii, Vol. 55, Supplement 1, pp. S145–S162, 2014.

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Leont’eva, N.N., Cherepanova, S.V. & Drozdov, V.A. Thermal decomposition of layered double hydroxides Mg-Al, Ni-Al, Mg-Ga: Structural features of hydroxide, dehydrated, and oxide phases. J Struct Chem 55, 1326–1341 (2014). https://doi.org/10.1134/S0022476614070142

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  • DOI: https://doi.org/10.1134/S0022476614070142

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