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An Effective Approach to the Synthesis of Nanocrystalline PbMoO4 in Na2Mo4O13–PbCO3 Melts

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Abstract

This paper presents thermodynamic analysis of reactions of sodium tetramolybdate with Pb3O4, PbO2, PbO, and lead carbonate and describes an effective approach to PbMoO4 synthesis in melts of the Na2Mo4O13–PbCO3 system, which offers a low synthesis temperature, waste-free character of the process, high rate, and high yield of a reagent-grade synthesis product in a nanocrystalline state. The synthesis product has been identified by chemical analysis, X-ray diffraction, and particle size measurements.

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Authors and Affiliations

  1. Berbekov State University, ul. Chernyshevskogo 173, Nalchik, 360004, Russia

    G. K. Shurdumov, Z. A. Cherkesov & E. F. Kandurova

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  1. G. K. Shurdumov
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  2. Z. A. Cherkesov
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  3. E. F. Kandurova
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Correspondence to Z. A. Cherkesov.

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Original Russian Text © G.K. Shurdumov, Z.A. Cherkesov, E.F. Kandurova, 2018, published in Neorganicheskie Materialy, 2018, Vol. 54, No. 5, pp. 513–519.

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Shurdumov, G.K., Cherkesov, Z.A. & Kandurova, E.F. An Effective Approach to the Synthesis of Nanocrystalline PbMoO4 in Na2Mo4O13–PbCO3 Melts. Inorg Mater 54, 490–496 (2018). https://doi.org/10.1134/S0020168518050138

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  • DOI: https://doi.org/10.1134/S0020168518050138

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