Skip to main content
Log in

Evaluation of the Liberation Characteristic of Coarse Middling Coking Coal by Size-Density Fractionation

  • Published:
Mining, Metallurgy & Exploration Aims and scope Submit manuscript

Abstract

In this paper, the size-density distribution of coarse middling coking coal (CMCC) with different grinding fineness and flotation concentrates was investigated. Then, the flotation behaviors and liberation characteristics of different size-density fractions in ground CMCC were analyzed, and the different size-density fractions were divided into five categories: most-beneficial, secondary-beneficial, poorly liberated, insignificant-pollution, and serious-pollution. Based on the content of particles with different liberation characteristics, an evaluation index of the liberation characteristic of ground CMCC, namely, the liberation perfection index (LPI), was proposed. The results indicated that grinding changed the size-density composition of CMCC, which affected the flotation performance. Insufficient grinding and overgrinding were not beneficial to flotation. Insufficient grinding caused a higher content of poorly liberated particles and a lower content of most-beneficial particles. Overgrinding increased the content of serious-pollution particles and reduced the content of most-beneficial particles. The size order of the LPI values of different ground CMCC was consistent with the flotation efficiency, and the LPI values of the other two similar samples were overall positively correlated with their flotation performance, suggesting that the method is universal.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. Ma J, Wang F, Shi C, Chen L, Xie Q (2019) Numerical analysis of motion trajectory of coarse coal particle in interfering fluidized bed. J China Coal Soc 44(S1):243–248. https://doi.org/10.13225/j.cnki.jccs.2018.1707. (in Chinese)

    Article  Google Scholar 

  2. Gui X, Liu J, Cao Y, Miao Z, Li S, Xing Y, Wang D (2016) Coal preparation technology: status and development in China. Energy Environ 26(6–7):997–1014. https://doi.org/10.1260/0958-305X.26.6-7.997

    Article  Google Scholar 

  3. Yang Z, Xia Y, Wei C, Cao Y, Sun W, Liu P, Cheng H, Xing Y, Gui X (2019) New flotation flowsheet for recovering combustible matter from fine waste coking coal. J Clean Prod 225:209–219. https://doi.org/10.1016/j.jclepro.2019.03.324

    Article  Google Scholar 

  4. Zou W, Cao Y, Liu J, Li W, Liu C (2013) Wetting process and surface free energy components of two fine liberated middling bituminous coals and their flotation behaviors. Powder Technol 246:669–676. https://doi.org/10.1016/j.powtec.2013.06.028

    Article  Google Scholar 

  5. Zhu Z, Yin W, Li Z, Zhang C, Wang D, Yang B (2020) Investigation on the liberation and flotation behaviors of coking middlings. Energ Source Part A 42(5):536–542. https://doi.org/10.1080/15567036.2019.1587098

    Article  Google Scholar 

  6. Tao X, Cao Y, Liu J (2009) Studies on characteristics and flotation of a hard-to-float high-ash fine coal. Earth Planet Sc Lett 1:799–806. https://doi.org/10.1016/j.proeps.2009.09.126

    Article  Google Scholar 

  7. Gui X, Yang Z, Wang D, Ran J (2017) Liberation properties of middling coking coal under shear force. Powder Technol 319:483–493. https://doi.org/10.1016/j.powtec.2017.07.008

    Article  Google Scholar 

  8. Xie W, He Y, Wang Y, Ge Z, Wang S, Wang H (2017) Comparison of flotation behavior of middling coal ground by wet-milling with different media. Particul Sci Technol 35(5):616–620. https://doi.org/10.1080/02726351.2016.1189986

    Article  Google Scholar 

  9. Fu Y, Li Z, Zhou A, Xiong S, Yang C (2019) Evaluation of coal component liberation upon impact breakage by MLA. Fuel 258:116–136. https://doi.org/10.1016/j.fuel.2019.116136

    Article  Google Scholar 

  10. Ma F, Tao D, Tao Y, Liu S (2021) An innovative flake graphite upgrading process based on HPGR, stirred grinding mill, and nanobubble column flotation. Int J Min Sci Techno 31(6):1063–1074. https://doi.org/10.1016/j.ijmst.2021.06.005

    Article  Google Scholar 

  11. Oki T, Yotsumoto H, Owada S (2004) Calculation of degree of mineral matter liberation in coal from sink-float separation data. Miner Eng 17(1):39–51. https://doi.org/10.1016/j.mineng.2003.09.009

    Article  Google Scholar 

  12. Zou W, Cao Y, Zhang Z, Liu J (2013) Coal petrology characteristics of middlings from Qianjiaying fat coal mine. Int J Min Sci Techno 23(5):777–782. https://doi.org/10.1016/j.ijmst.2013.08.024

    Article  Google Scholar 

  13. Vianna S (2004) The effect of particle size, collector coverage and liberation on the floatability of galena particles in an ore. University of Queensland, Brisbane

    Google Scholar 

  14. Cheng G, Zhang M, Cao Y, Lu Y, Feng Y, Zhao S (2020) Preparation and evaluation of lignite flotation collector derived from waste hot-pot oil. Fuel 267:117–138. https://doi.org/10.1016/j.fuel.2020.117138

    Article  Google Scholar 

  15. Yoon R, Luttrell G (1989) The effect of bubble size on fine particle flotation. Miner Process Extr M 5(1–4):101–122. https://doi.org/10.1080/08827508908952646

    Article  Google Scholar 

  16. Nguyen A, Ralston J, Schulze H (1998) On modelling of bubble particle attachment probability in flotation. Int J Miner Process 53(4):225–249. https://doi.org/10.1016/S0301-7516(97)00073-22

    Article  Google Scholar 

  17. Sahoo S, Suresh N, Varma A (2020) Determining the best particle size-class for flotation of a high ash coal. Int J Coal Prep Util 40(11):755–765. https://doi.org/10.1080/19392699.2017.1409216

    Article  Google Scholar 

  18. Zou W, Cao Y, Sun C (2016) Scale effect of coking coal middlings and its influence on flotation. J China Coal Soc 41(2):469–474. https://doi.org/10.13225/j.cnki.jccs.2015.0335. (in Chinese)

    Article  Google Scholar 

  19. Wang B, Peng Y (2013) The behavior of mineral matter in fine coal flotation using saline water. Fuel 109:309–315. https://doi.org/10.1016/j.fuel.2013.01.030

    Article  Google Scholar 

  20. Wang L, Peng Y, Runge K (2015) A review of entrainment: mechanisms, contributing factors and modelling in flotation. Miner Eng 70:77–91. https://doi.org/10.1016/j.mineng.2014.09.003

    Article  Google Scholar 

  21. Hou S, Ma L, Huang G, Li J, Yu Y, Yan D (2016) Mechanism of the effect of fine coal with different densities on coarse coal flotation. J China Coal Soc 41(7):1813–1819. https://doi.org/10.13225/j.cnki.jccs.2016.0294. (in Chinese)

    Article  Google Scholar 

  22. Cheng G, Cao Y, Zhang C, Jiang Z, Yu Y, Mohanty M (2020) Application of novel flotation systems to fine coal cleaning. Int J Coal Prep Util 40(1):24–36. https://doi.org/10.1080/19392699.2018.1476348

    Article  Google Scholar 

  23. Gao J (n.d) Study on particle density-size bivariate distribution regularities in coal preparation process (in Chinese). Taiyuan: Taiyuan University of Technology

  24. Xie W, He Y, Zhu X, Ge L, Huang Y, Wang H (2013) Liberation characteristics of coal middlings comminuted by jaw crusher and ball mill. Int J Min Sci Techno 23:669–674. https://doi.org/10.1016/j.ijmst.2013.08.009

    Article  Google Scholar 

  25. Gui X, Liu J, Cao Y, Cheng G, Li S, Wu L (2014) Flotation process design based on energy input and distribution. Fuel Process Technol 120:61–70. https://doi.org/10.1016/j.fuproc.2013.12.011

    Article  Google Scholar 

  26. Yue Z, Ren R (2022) Study on the influence mechanism of the grinding fineness on the floatability of coking middings. Particul Sci Technol (in press). https://doi.org/10.1080/02726351.2022.2060153

    Article  Google Scholar 

  27. Bond F (1952) The third theory of comminution. Transations AIME Min Eng 193:484–494

    Google Scholar 

  28. Niu F, Liu Y, Xin X (2019) Experimental study on Bond work index of a coal mine in Hebei province. Multipurpose Utilization Mineral Resour 2:140–143. https://doi.org/10.3969/j.issn.1000-6532.2019.02.029. (in Chinese)

    Article  Google Scholar 

  29. Yue Z, Ma L, Li J, Du W, Wang J, Zhao W, Zhu Y (2014) Experiment study on characteristics of coarse slime rod-grinding and flotation. Coal Sci Technol 42(11):116–120. https://doi.org/10.13199/j.cnki.cst.2014.11.029. (in Chinese)

    Article  Google Scholar 

  30. GB/T 478–2008. (2008) Method for float and sink analysis of coal (in Chinese). Beijing: Standards Press of China

  31. Li C, Bai Y, Dong Q, Liu G, Zhao J (2019) Application of a small cone hydrocyclone on high ash fine coal pre-deslimg flotation. Int J Coal Prep Util 39(5):233–245. https://doi.org/10.1080/19392699.2018.1544559

    Article  Google Scholar 

  32. Xie G (2001) Mineral processing technology (in Chinese). China University of Mining and Technology Publishing Company Inc, Xuzhou

    Google Scholar 

  33. GB/T 4757–2001 (2001) Method for the forth flotation testing of coal (in Chinese). Beijing: Standards Press of China

  34. Wills B, Napier-Munn T (2006) Mineral processing technology: an introduction to the practical aspects of ore treatment and mineral recovery, 7th edn. Elsevier Science and Technology Books, Oxford

    Google Scholar 

  35. Cheng G, Li Y, Zhang M, Lau E (2022) Improving micro-fine mineral flotation via micro/nano technologies. Sep Sci Technol (in press). https://doi.org/10.1080/01496395.2022.2140293

    Article  Google Scholar 

Download references

Funding

This work was supported by the Liaoning Education Department (grant numbers LN2019ZL004, LJKZ1208).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Caixia Li.

Ethics declarations

Conflict of Interest

The authors declare no competing interests.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Yue, Z., Li, C., Han, X. et al. Evaluation of the Liberation Characteristic of Coarse Middling Coking Coal by Size-Density Fractionation. Mining, Metallurgy & Exploration 40, 517–528 (2023). https://doi.org/10.1007/s42461-023-00742-0

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s42461-023-00742-0

Keywords

Navigation