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Texture and inhibitor features of grain-oriented pure iron produced by different cold-rolling processes

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Abstract

To promote the manufacture of grain-oriented pure iron, the texture and inhibitor features of two samples A and B produced by different cold-rolling processes were studied by optical microscopy, X-ray diffraction, and transmission electron microscopy. The results showed that a higher content of inhibitor elements directly resulted in a greater number of fine inhibitors, which exhibited strong inhibitory ability, leading to more fine precipitates of appropriate size effectively inhibiting the growth of primary grains in decarburized bands (sheets) during the single-stage cold-rolling process. The formation of the component with {110}<001> Goss orientation was greatly suppressed in the stage of primary recrystallization, and this component could hardly be observed in the decarburized band; by contrast, the {411}<148>-oriented grains grew. During the process of high-temperature annealing, abnormal growth occurred and secondary recrystallized grains (Goss orientation) merged with other matrix grains such as {111}<112> and {411}<148>. The magnetic induction of samples A and B at 800 A/m was 1.939 T and 1.996 T, respectively.

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References

  1. Z.Z. He, Y. Zhao, H.W. Luo, Electrical steel, Metallurgical Industry Press, Beijing, 2012.

    Google Scholar 

  2. R.D. Blaugher, R.H. Hopkins, Development of grain-oriented iron sheet for electrical apparatus, US Patent, 4265683, 1981.

  3. D.R. Thornburg, Method of producing primary recrystallized textured iron alloy member having an open gamma loop, US Patent, 3892605, 1975.

  4. L.Z. Dai, Acta Metall. Sin. 3 (1958) 227–230.

    Google Scholar 

  5. L.Z. Dai, X.Y. Zhang, Acta Phys. Sin. 14 (1958) 17–22.

    Google Scholar 

  6. T. Wada, K. Takashima, M. Kawashima, AIP Conference Proceedings 18 (1974) 1363–1366.

    Google Scholar 

  7. Y. Hiroyoshi, T. Masashi, Manufacture of grain oriented electrical steel sheet, Japan Patent, 61-091329, 1986.

  8. Y. Hiroyoshi, O. Atsuki, Production of grain oriented electrical steel sheet, Japan Patent, 62-83421, 1987.

  9. Y. Hiroyoshi, K. Teruo, Production of grain-oriented magnetic steel sheet, Japan Patent, 1-309923, 1989.

  10. Y. Hiroyoshi, K. Teruo, Grain-oriented magnetic steel sheet and its production, Japan Patent, 1-309924, 1989.

  11. N. Yoshio, O. Yasuo, Production of unidirectionally oriented electrical steel sheet having high magnetic flux density, Japan Patent, 1991.

  12. N. Ujihiro, K. Tsutomu, N. Kiyohiko, S. Kazuhiro, Soft magnetic iron sheet excellent in magnetic property and its manufacture, Japan Patent, 5-24764, 1992.

  13. N. Yoshio, O. Yasuo, Production of grain-oriented electrical steel sheet having high magnetic flux density, Japan Patent, 4-13811, 1992.

  14. N. Yoshio, O. Yasuo, Grain-oriented pure iron excellent in magnetic permeability and coercive force in coil-width direction and its production, Japan Patent, 4-301052, 1992.

  15. N. Yoshio, O. Yasuo, N. Tadao, M. Takashi, N. Takeo, Y. Shuichi, F. Hiroyasu, K. Takao, Grain-oriented silicon steel sheet having excellent magnetostrictive characteristic, Japan Patent, 7-062501, 1995.

  16. K. Ryutaro, W. Takeaki, Production of grain-oriented silicon steel sheet extremely high in magnetic flux density, Japan Patent, 10-298651, 1998.

  17. K. Ryutaro, W. Takeaki, Manufacture of grain oriented silicon steel sheet having stable and extremely high magnetic flux density in longitudinal direction of coil, Japan Patent, 10-306318, 1998.

  18. K. Ryutaro, W. Takeaki, Manufacture of grain oriented silicon steel sheet having extremely high magnetic flux density, Japan Patent, 10-306319, 1998.

  19. K. Ryutaro, W. Takeaki, Production of grain oriented silicon steel sheet with extremely high magnetic flux density, Japan Patent, 11-50151, 1999.

  20. W. Takeaki, K. Ryutaro, Grain oriented silicon steel sheet with extremely high magnetic flux density, and its manufacture, Japan Patent, 11-189851, 1999.

  21. C.C. Liao, C.K. Hou, J. Magn. Magn. Mater. 322 (2010) 434–442.

    Article  Google Scholar 

  22. J. Flowers, IEEE Trans. Magn. 15 (1979) 1601–1603.

    Article  Google Scholar 

  23. Z. Rong, Exploration and laboratory trial production of grain oriented pure iron, Central Iron and Steel Research Institute, Beijing, 2015.

    Google Scholar 

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Acknowledgements

This work was financially supported by the National Natural Science Foundation of China (No. 51804003).

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Correspondence to Hai-jun Wang.

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Deng, Jj., Wang, Hj., Rong, Z. et al. Texture and inhibitor features of grain-oriented pure iron produced by different cold-rolling processes. J. Iron Steel Res. Int. 25, 1026–1032 (2018). https://doi.org/10.1007/s42243-018-0145-9

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  • DOI: https://doi.org/10.1007/s42243-018-0145-9

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