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Confining FeNi nanoparticles in biomass-derived carbon for effectively photo-Fenton catalytic reaction for polluted water treatment

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Abstract

Photo-Fenton catalytic degradation organic contaminant is considered as a promising approach to water purification and environmental remediation. The novel class of photo-Fenton heterogeneous composite with large specific surface area, abundant active sites, uniform and stable metal ions, and fast Fe2+/Fe3+ conversion rate is considered as potential catalysts. Herein, a highly efficient and sustainable photo-Fenton heterogeneous composite (FeNi@corncob-activated carbon (CCAC)) was prepared by confining FeNi nanoparticles in CCAC through a simple solvothermal and activated-carbonization method. The porous structure and a high specific surface area of CCAC would effectively disperse FeNi nanoparticles, causing a significantly enhanced photo-Fenton catalytic performance. The RhB degradation rate of FeNi@CCAC was 2.3 times higher than that of FeNi. After five cycles, RhB degradation rate of FeNi@CCAC was barely decreased, confirming that FeNi@CCAC had high cyclability and reproducibility. Moreover, the reaction mechanism was analyzed in-depth via photoelectrochemical and electron spin resonance characterization. The outstanding results can be attributed to the contribution of the active species ‧OH, ‧O2–, and h+ in photo-Fenton degradation of RhB. Notably, FeNi@CCAC also has excellent photo-Fenton catalytic performance in sewage. This work illustrates a simple and effective method to improve the photo-Fenton catalytic reaction.

Graphical abstract

MOF-derived FeNi nanoparticles were confined in corncob-activated carbon to prepare a high-efficiency photo-Fenton heterogeneous composite for catalytic degradation of organic pollutants.

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Funding

This work was financially supported by the National Natural Science Foundation of China (No. 32071713), and the Natural Science Funds for Distinguished Young Scholar of Heilongjiang Province (No. JQ2019C001).

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Authors and Affiliations

  1. Key Laboratory of Bio-Based Material Science and Technology, Ministry of Education, College of Material Science and Engineering, Northeast Forestry University, Harbin, 150040, China

    Zhe Sun, Yixiang Zhang, Sitong Guo, Junming Shi, Cai Shi, Keqi Qu, Houjuan Qi & Zhanhua Huang

  2. Advanced Materials Division, Engineered Multifunctional Composites (EMC) Nanotech LLC, Knoxville, TN, 37934, USA

    Vignesh Murugadoss & Mina Huang

  3. Integrated Composites Laboratory (ICL), Department of Chemical and Bimolecular Engineering, University of Tennessee, Knoxville, TN, 37996, USA

    Vignesh Murugadoss & Zhanhu Guo

  4. College of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan, 030024, China

    Mina Huang

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  1. Zhe Sun
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Sun, Z., Zhang, Y., Guo, S. et al. Confining FeNi nanoparticles in biomass-derived carbon for effectively photo-Fenton catalytic reaction for polluted water treatment. Adv Compos Hybrid Mater 5, 1566–1581 (2022). https://doi.org/10.1007/s42114-022-00477-4

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