Abstract
Tensile studies on Superni 263 superalloy were carried out by employing various strain rates and temperatures in the range of (298–923 K), to explore the tensile deformation and fracture characteristics. It is found that Superni 263 alloy was sensitive to strain rate and peak value in yield strength was obtained at intermediate strain rate 1.3 × 10−3 S−1 and 673 K. The alloy exhibited serrated plastic flow, anomalous variations in tensile properties, minimum in ductility, work hardening rate and negative strain rate sensitivity which are the important manifestations of dynamic strain ageing (DSA) in the intermediate temperature range. The species responsible for the occurrence of DSA were identified as Cr and Mo with the activation energy measurements of 68–74 kJ/mol, indicating the pipe diffusion in austenite matrix. The alloy exhibited mixed ductile and intergranular mode of fracture in the entire temperature range. Few grains exhibited transgranular quasi-cleavage facets in the DSA range.
Similar content being viewed by others
References
Ankamma K et al (2011a) Effect of aging on work hardening behavior of cold rolled Nimonic C-263 alloy. Mater Sci Technol 27:1333–1340
Ankamma K, Satyanarayana DVV, Chandramohan Reddy G, Komaraiah M, Eswara Prasad N (2011b) In-plane anisotropy in tensile deformation and its influence on the drawability of Nimonic C–263 alloy sheets. SADHANA Acad Proc Eng Sci 36:223–249
ASTM E 8M-04 (2005a) Standard test methods for tension testing of metallic materials, vol 3.01. ASTM International, West Conshohocken, pp 86–109
ASTM E 21-03a (2005b) Standard test methods for elevated temperature tension tests of metallic materials, vol 3.01. ASTM International, West Conshohocken, pp 150–157
Bhanu Sankara Rao K, Seetharaman V, Mannan SL, Rodriguez P (1986) Strain rate and temperature dependence of formation and fracture behavior of a Nimonic PE16 Superalloy. High Temp Mater Process 7:63–81
Brechet Y, Estrin Y (1995) On the influence of precipitation on the Portevin-Le Chatelier effect. Acta Metall Mater 43:955–963
Cai Y, Tian C, Zhang G, Han G, Yang S, Fu S, Cui C, Zhang Q (2017) Influence of γ′ precipitates on the critical strain and localized deformation of serrated flow in Ni-based superalloys. J Alloys Compd 690:707–715
Choudhary BK, Bhanu Sankara Rao K, Mannan SL, Kashyap BP (1999) Serrated Yielding in 9Cr-1Mo ferritic steel. Mater Sci Technol 15:791–797
Cottrell AH (1953) A note on the Portevin-Le Chatelier effect. Philos Mag 44:829–832
Dingley DJ, Mclean D (1967) Components of flow stress of Iron. Acta Metall 15:885–901
Doi H, Shimanuki Y (1972) In: Proceedings of 2nd international conference on superalloys-processing, Champion, Pennsylvania
Embury JD (1971) Strengthening methods in crystals. Wiley Publishers, New York, p 331
Garde AM, Santhanam AT, Reed-Hill RE (1972) Acta Metall 20:215
Gianfrancesco AD (2017) Materials for ultra-supercritical and advanced ultra-supercritical power plants. Elsevier, New York, p 571
Gopinath K, Gogia AK, Kamath SV, Ramamurty U (2009) Dynamic strain aging in Ni based superalloy 720Li. Acta Mater 57:1243–1253
Han GM, Tian CG, Chu ZK, Cui CY, Hu ZQ, Sun XF (2015) Activation energy calculations for the Portevin–Le Chatelier effect in nimonic 263 superalloy. Metall Mater Trans A 46:4629–4635
Hirth JP (1982) In: Meshii M (ed) Mechanical properties of BCC metals, vol 181. TMS, Warrendale, PA, pp 181–187
Hornbogen E (1964) Trans ASM 57:122–132
Jadav J, Rajulapati KV, Bhanu Sankara Rao K, Eswara Prasad N, Mythili R, Prasad K (2019) Strain controlled isothermal low cycle fatigue life, deformation and fracture characteristics of Superni 263 superalloy. Mater Sci Eng A 760:296–315
Jenkins CF, Smith GV (1969) Serrated plastic flow in austenitic stainless steel. Trans TMS-AIME 245:2149–2156
Koul AK, Pickering FB (1982) Serrated yielding in Ni-Fe base superalloys at 700°C. Scripta Met 16:119–124
Maile K (2013) Qualification of Ni-based alloys for advanced ultra supercritical plants. Proc Eng 55:214
Mannan SL, Samuel KG, Rodriguez P (1982) In: Giffkins RC (ed) Proceedings of 6th international conference on strength of metals and alloys, p 637
McCormick PG (1972) A model for the Portevin-Le Chatelier effect in substitutional alloys. Acta Metall 20:351
Morris JG (1974) Dynamic strain aging in aluminium alloys. Mater Sci Eng 13:101–108
Penning P (1972) Mathematics of the Portevein-Le Chatelier effect. Acta Metall 20:1169–1175
Pope DP, Ezz SS (1984) Int Mater Rev 29:136
Rodriguez P (1984) Serrated plastic flow. Bull Mater Sci 6:653–663
Shankar V, Valsan M, Bhanu Sankara Rao K, Mannan SL (2004) Effects of temperature and strain rate on tensile properties and activation energy for dynamic strain aging in alloy 625. Metall Mater Trans A 35:3129–3139
Sleeswyk AW (1958) Slow strain-hardening of ingot iron. Acta Metall 6:598–603
Smith SA, West GD, Chi K, Gamble W, Thomson RC (2010) Advances in materials technology for fossil power plants. In: Proceedings from 6th international conference, pp 110–126
Wang X, Han G, Cui C, Guan S, Jin T, Sun X, Hu Z (2016) The dependence of Portevin–Le Châtelier effect on the γ′ precipitates in a wrought Ni-Base Superalloy. Metall Mater Trans A 47:5994–6003
Wanga WZ, Honga HU, Kima IS (2009) Influence of and grain boundary carbide on tensile fracture behaviours of Nimonic 263. Mater Sci Eng A 523:242–245
Zhao JC, Ravikumar V, Beltran AM (2001) Phase precipitation and phase stability in Nimonic 263. Metall Mater Trans A 32:1271–1282
Acknowledgements
The authors gratefully acknowledge DST-PURSE and DST-FIST programs of School of Engineering Sciences and Technology, University of Hyderabad for providing some of the experimental facilities used in this investigation.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Jadav, J., Rajulapati, K.V., Bhanu Sankara Rao, K. et al. Effects of Strain Rate and Temperature on Tensile Properties, Deformation and Dynamic Strain Ageing Behavior of Ni-Base Superalloy Superni 263. INAE Lett 4, 241–250 (2019). https://doi.org/10.1007/s41403-019-00083-9
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s41403-019-00083-9