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Change in the Crystallographic Texture of the Martensitic Phase in Superelastic Ti–Zr–Nb Alloys with Increasing Tensile Strain

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Abstract

Superelastic alloys based on Ti–Zr–Nb are low-modulus biocompatible alloys for medical applications. We analyzed the regularities of the development of martensitic transformations (MT) β (bcc) → α′′ (orthorhombic lattice) in Ti–(17–19)Zr–(14–15)Nb (at.%) alloys, where α′′-phase arises under the influence of tensile or compressive stress. The crystallographic texture of β-titanium alloys was well studied. However, this is precisely what determines the recoverable strain in the material. Phase analysis using synchrotron radiation showed that the MT begins at 1% deformation, and at 1.5% the martensite lines are clearly distinguishable. The orientational dependences of the formation of domains of the martensite phase were studied using generalized direct pole figures. The main texture components of the cold rolled up to 97% and then recrystallized foils are {221}〈114〉 and {100}〈011〉. Under tensile deformation up to 1.4%, α′′-phase domains with the orientation (100)[001] is formed from β-grains compressed along the normal direction of the foil. With an increase in the degree of deformation to 1.6%, in addition to the main texture component, the second texture component appears. Its orientation depends on the direction of application of the external stress: (001)[110] in tension along the rolling direction and (\(\overline{1 }\)05)[501] in tension in the transverse direction.

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Data Availability

The data required to reproduce these findings are available to download from [43].

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Acknowledgements

The work was carried out with the financial support of the Russian Federation represented by the Ministry of Science and Higher Education of the Russian Federation (Agreement No. 075-15-2021-1352).

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Authors and Affiliations

  1. National Research Nuclear University MEPhI (Moscow Engineering Physics Institute), Kashirskoe shosse, 31, Moscow, Russian Federation, 115409

    Mariia Zaripova, Vladimir Fesenko, Olga Krymskaya, Ilya Kozlov & Margarita Isaenkova

  2. National Research Center “Kurchatov Institute”, 1, Akademika Kurchatova Pl., Moscow, Russian Federation, 123182

    Roman Svetogorov

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  1. Mariia Zaripova
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Zaripova, M., Fesenko, V., Krymskaya, O. et al. Change in the Crystallographic Texture of the Martensitic Phase in Superelastic Ti–Zr–Nb Alloys with Increasing Tensile Strain. Shap. Mem. Superelasticity 8, 188–199 (2022). https://doi.org/10.1007/s40830-022-00383-0

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