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Thermocycling effect on mechanical and tribological characterization of two indirect dental restorative materials

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Abstract

The purpose of this study is to evaluate the effects of aging by thermocycling on the mechanical and tribological properties of two indirect filling commercial resin-based restorative composite materials. The studied composites are referenced by the capital letters: A and B. The commercial trade names are omitted, to avoid commercial references. Forty specimens of each material were produced and divided into three groups: a control group not subjected to aging, and two groups, T1 and T2 submitted to different thermocycling conditions. The studied properties were surface roughness, elastic modulus (determined dynamically by impulse excitation of vibration, and statically by four-point bending test), flexural strength and work of fracture (four-point bending test), micro-hardness (Vickers micro-indentation) and coefficient of friction (scratch test). From this study, it was possible to conclude that Composite A, in addition to having better mechanical properties, is less affected by thermocycling than Composite B, which suggests that it will better withstand the stresses, both mechanical and thermal, which it is subjected to. It is also possible to infer that the thermocycling regimen proposed by Standard ISO 11405 (Dental materials—testing of adhesion to tooth structure, 2003) is not sufficient to adequately simulate the degradation caused by the oral environment on current commercial resin-based restorative composites.

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References

  1. ISO/TS 11405:2015 Dental materials—testing of adhesion to tooth structure. International Organization for Standardization, Geneva, Switzerland. https://www.iso.org/obp/ui/#iso:std:iso:ts:11405:ed-3:v1:en

  2. Antunes PV, Ramalho A, Carrilho EVP (2014) Mechanical and wear behaviors of nano and microfilled polymeric composite: effect of filler fraction and size. Mater Des 61:50–60

    Article  Google Scholar 

  3. Asmussen E, Peutzfeldt A (1998) Influence of UEDMA, BisGMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater 14:51–56

    Article  Google Scholar 

  4. Ru S, Raab WH, Janda R (2007) Polymerization shrinkage and hygroscopic expansion of contemporary posterior resin-based filling materials—A comparative study. J Dent 35:806–813

    Article  Google Scholar 

  5. Amirouche-Korichi A, Mouzali M, Watts DC (2009) Effects of monomer ratios and highly radiopaque fillers on degree of conversion and shrinkage-strain of dental resin composites. Dent Mater 25:1411–1418

    Article  Google Scholar 

  6. Amirouche-Korichi A, Mouzali M, Watts DC (2012) Shrinkage strain—rates study of dental composites based on (BisGMA/TEGDMA) monomers. Arab J Chem. doi:10.1016/j.arabjc.2012.07.021

    Google Scholar 

  7. Indrani DJ, Cooks WD, Televantosd F, Martin J, Harcourtl JK (1995) Fracture toughness of water-aged resin composite restorative materials. Dent Mater 11:201–207

    Article  Google Scholar 

  8. Sideridou ID, Karabela MM, Bikiaris DN (2007) Aging studies of light cured dimethacrylate-based dental resins and a resin composite in water or ethanol/water. Dent Mater 23:1142–1149

    Article  Google Scholar 

  9. Mesquita RV, Geis-Gerstorfer J (2008) Influence of temperature on the visco-elastic properties of direct and indirect dental composite resins. Dent Mater 24:623–632

    Article  Google Scholar 

  10. Ramalho A, Braga de Carvalho MD, Antunes PV (2013) Effects of temperature on mechanical and tribological properties of dental restorative composite materials. Tribol Int 63:186–195

    Article  Google Scholar 

  11. Musanje L, Darvell BW (2004) Effects of strain rate and temperature on the mechanical properties of resin composites. Dent Mater 20:750–765

    Article  Google Scholar 

  12. Gale MS, Darvell BW (1999) Thermal cycling procedures for laboratory testing of dental restorations. J Dent 27:89–99

    Article  Google Scholar 

  13. Göhring TN, Gallo L, Lüthy H (2005) Effect of water storage, thermocycling, the incorporation and site of placement of glass-fibers on the flexural strength of veneering composite. Dent Mater 21:761–772

    Article  Google Scholar 

  14. Meriç G, Ruyter IE (2007) Effect of thermal cycling on composites reinforced with two differently sized silica-glass fibers. Dent Mater 23:1157–1163

    Article  Google Scholar 

  15. Morresi AL, D’Amario M, Capogreco M, Gatto R, Marzo G, D’Arcangelo C, Monaco A (2014) Thermal cycling for restorative materials: does a standardized protocol exist in laboratory testing? A literature review. J Mech Behav Biomed Mater 29:295–308

    Article  Google Scholar 

  16. Zheng SY, Zheng J, Gao SS, Yu BJ, Yu HY, Qian LM, Zhou ZR (2011) Investigation on the microtribological behaviour of human tooth enamel by nanoscratch. Wear 271:2290–2296

    Article  Google Scholar 

  17. Palaniappan S, Celis J-P, Meerbeek BV, Peumans M, Lambrechts P (2013) Correlating in vitro scratch test with in vivo contact free occlusal area wear of contemporary dental composites. Dent Mater 29(3):259–268

    Article  Google Scholar 

  18. Fereira VR, Sukumaran J, Delgado YP, Staia M, Iost A, Baets PD (2013) Scratch evaluation on a high performance polymer. Mech Eng Lett 9:76–84

    Google Scholar 

  19. Yamamoto T, Hanabusa M, Momoi Y, Sakaguchi RL (2015) Polymerization stress of dental resin composite continues to develop 12 hours after irradiation. J Esthet Restor Dent 27(1):44–54

    Article  Google Scholar 

  20. Fugolin APP, Correr-Sobrinho L, Correr AB, Sinhoreti MAC, Guiraldo RD, Consani S (2016) Influence of irradiance on Knoop hardness, degree of conversion, and polymerization shrinkage of nanofilled and microhybrid composite resins. General Dent 64:26–31

    Google Scholar 

  21. Narene AVK, Veniashok B, Subbiya A, Vivekanandhan P, Sukumaran VG (2014) Polymerisation shrinkage in resin composites—a review. Middle East J Sci Res 21:107–112

    Google Scholar 

  22. Yang S, Choi J, Cho M (2012) Elastic stiffness and filler size effect of covalently grafted nanosilica polyimide composites: molecular dynamics study. ACS Appl Mater Interfaces 4:4792–4799

    Article  Google Scholar 

  23. Mandikos MN, McGivney GP, Davis E, Bush PJ, Carter JM (2001) A comparison of the wear resistance and hardness of indirect composite Resins. J Prosthet Dent 85(4):386–395

    Article  Google Scholar 

  24. ISO 4288:1996/Cor.1:1998 (en), Geometrical Product Specifications (GPS)—Surface texture: profile method—rules and procedures for the assessment of surface texture, International Organization for Standardization, Geneva, Switzerland

  25. Braem M, Lambrechts P, Doren VVAN, Vanherle G (1986) The impact of composite structure on its elastic response. J Dent Res 65:648–653

    Article  Google Scholar 

  26. C1259 (2015) Standard test method for dynamic young’s modulus, Shear modulus, and poisson’s ratio for advanced ceramics by impulse excitation of vibration, Developed by subcommittee: C28.01, Book of standards vol 15.01, American Society for Testing and Materials ASTM C1259

  27. C1161 (2013) Standard test method for flexural strength of advanced ceramics at ambient temperature, Developed by subcommittee: C28.01, Book of standards vol 15.01, American Society for Testing and Materials ASTM C1161

  28. E384 (2016) Standard test method for microindentation hardness of materials, Developed by subcommittee: E04.05, Book of standards vol 03.01, American Society for Testing and Materials ASTM E384-16

  29. G171 (2009) Standard test method for scratch hardness of materials using a diamond stylus, Developed by subcommittee: G02.30, Book of standards vol 03.02, American Society for Testing and Materials ASTM G171-03(2009)e2

  30. Stalio E (2002) Direct numerical simulation of heat transfer enhancing surfaces. Doctoral Thesis, pp 75–90

  31. Tuncer S, Demirci M, Tiryaki M, Ünlü N, Uysal Ö (2013) The effect of a modeling resin and thermocycling on the surface hardness, roughness, and color of different resin composites. J Esthet Restor Dent 25:404–419

    Article  Google Scholar 

  32. Beun S, Glorieux T, Devaux J, Vreven J, Leloup G (2013) Characterization of nanofilled compared to universal and microfilled composites. Dent Mater 23:51–59

    Article  Google Scholar 

  33. Heintze SD, Zellweger G, Zappini G (2007) The relationship between physical parameters and wear of dental composites. Wear 263:1138–1146

    Article  Google Scholar 

  34. Mesquita RV, Axmann D, Geis-Gerstorfer J (2006) Dynamic visco-elastic properties of dental composite resins. Dent Mater 22:258–267

    Article  Google Scholar 

  35. Xu HH, Smith DT, Jahanmir S, Romberg E, Kelly JR, Thompson VP, Rekow ED (1998) Indentation damage and mechanical properties of human enamel and dentin”. J Dent Res 77:472–480

    Article  Google Scholar 

  36. El-Safty S, Akhtar R, Silikas N, Watts DC (2012) Nanomechanical properties of dental resin-composites. Dent Mater 28:1292–1300

    Article  Google Scholar 

  37. Belli R, Petschelt A, Lohbauer U (2014) Are linear elastic material properties relevant predictors of the cyclic fatigue resistance of dental resin composites? Dent Mater 30:381–391

    Article  Google Scholar 

  38. ISO 4049:2009 (2009) Dentistry—polymer-based restorative materials, ISO/TC 106/SC 1, standard was last reviewed in 2014, International Organization for Standardization, Geneva, Switzerland

  39. Asmussen E, Peutzfeldt A (1998) Influence of UDMA, bis-GMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater 56:14–51

    Google Scholar 

  40. Sideridou ID, Karabela MM, Bikiaris DN (2009) Aging studies of light cured dimethacrylate-based dental resins and a resin composite in water or ethanol/water. Dent Mater 23(9):1142–1149

    Article  Google Scholar 

  41. Ruyter IE, Øysæd H (1987) Composites for use in posterior teeth: composition and conversion. J Biomed Mater Res 21:11–23

    Article  Google Scholar 

  42. Peutzfeldt A, Asmussen E (1992) Modulus of resilience as predictor for clinical wear of restorative resins. Dent Mater 8:146–148

    Article  Google Scholar 

  43. Asmussen E, Peutzfeldt A (1998) Influence of UEDMA BisGMA and TEGDMA on selected mechanical properties of experimental resin composites. Dent Mater 14(1):51–56

    Article  Google Scholar 

  44. Ho CT, Vijayaraghavan TV, Lee SY, Tsai A, Huang HM, Pan LC (2001) Flexural behaviour of post-cured composites at oral-simulating temperatures. J Oral Rehabil 28:658–667

    Article  Google Scholar 

  45. Kao EC (1989) Influence of food-simulating solvents on resin composites and glass-ionomer restorative cement. Dent Mater 5:201–208

    Article  Google Scholar 

  46. Ferracane JL, Berge HX, Condon JR (1998) In vitro aging of dental composites in water—effect of degree of conversion, filler volume, and fillermatrix coupling. J Biomed Mater Res 42:465–472

    Article  Google Scholar 

  47. Ferracane JL, Berge HX (1988) Fracture toughness of experimental dental composites aged in ethanol. J Dent Res 74:1418–1423

    Article  Google Scholar 

  48. Pilliar RM, Vowles R, Williams DF (1987) The effect of environmental aging on the fracture toughness of dental composites. J Dent Res 66:722–726

    Article  Google Scholar 

  49. Prakki A, Cilli R, Mondelli RFL, Kalachandra S, Pereira JC (2005) Influence of pH environment on polymer based dental material properties. J Dent 33:91–98

    Article  Google Scholar 

  50. Ortengren U, Andersson F, Elgh U, Terselius B, Karlsson S (2001) Influence of pH and storage time on the sorption and solubility behaviour of three composite resin materials. J Dent 29:35–41

    Article  Google Scholar 

  51. Sarkar NK, Karmaker A, Prasad A, Shih F (1999) Simulation of in vivo degradation of dental composites. J Mater Sci Lett 18:1749–1752

    Article  Google Scholar 

  52. Zaytsev D, Panfilov P (1999) Deformation behavior of human enamel and dentin-enamel junction under compression. Mater Sci Eng C 34:15–21

    Article  Google Scholar 

  53. Alshali RZ, Salim NA, Satterthwaite JD, Silikas N (2015) Post-irradiation hardness development, chemical softening, and thermal stability of bulk-fill and conventional resin-composites. J Dent 43:209–218

    Article  Google Scholar 

  54. Rahim TNAT, Mohamad D, Akil HM, Rahman IA (2012) Water sorption characteristics of restorative dental composites immersed in acidic drinks. Dent Mater 28(6):e63–e70

    Article  Google Scholar 

  55. Ferracane JL (2006) Hygroscopic and hydrolytic effects in dental polymer networks. Dent Mater 22(3):211–222

    Article  Google Scholar 

  56. Curtis AR, Shortall AC, Marquis PM, Palin WM (2008) Water uptake and strength characteristics of a nanofilled resin-based composite. J Dent 36(3):186–193

    Article  Google Scholar 

  57. Moraes RR, Sinhoreti MAC, Correr-Sobrinho L, Ogliari FA, Piva E, Petzhold CL (2010) Preparation and evaluation of dental resin luting agents with increasing content of bisphenol-A ethoxylated dimethacrylate. J Biomater Appl 24(5):453–473

    Article  Google Scholar 

  58. Kalachandra S, Turner DT (1987) Water sorption of polymethacrylate networks: Bis-GMA/TEGDM copolymers. J Biomed Mater Res 21(3):329–338

    Article  Google Scholar 

  59. Kobrick RL, Klaus DM, Street KW (2011) Standardization of a volumetric displacement measurement for two-body abrasion scratch test data analysis. Wear 270(9–10):650–657

    Article  Google Scholar 

  60. Jardret V, Morel P (2003) Viscoelastic effects on the scratch resistance of polymers: relationship between mechanical properties and scratch properties at various temperatures. Prog Org Coat 48:322–331

    Article  Google Scholar 

  61. Barletta M, Gisario A, Trovalusci F, Vesco S (2013) Visual appearance and scratch resistance of high performance thermoset and thermoplastic powder coatings. Prog Org Coat 76:244–256

    Article  Google Scholar 

  62. Barletta M, Tagliaferri V, Gisario A, Venettacci S (2013) Progressive and constant load scratch testing of single- and multi-layered composite coatings. Tribol Int 64:39–52

    Article  Google Scholar 

  63. Bastos FS, Oliveira EA, Fonseca LG, Vargas SM, Las Casas EB (2016) A FEM-based study on the influence of skewness and kurtosis surface texture parameters in human dental occlusal contact. J Comput Appl Math 295:139–148

    Article  MathSciNet  MATH  Google Scholar 

  64. Sedlaček M, Podgornik B, Vižintin J (2012) Correlation between standard roughness parameters skewness and kurtosis and tribological behaviour of contact surfaces. Tribol Int 48:102–112

    Article  Google Scholar 

  65. Ţălu Ş, Stach S, Lainović T, Vilotić M, Blažić L, Alb SF, Kakaš D (2015) Surface roughness and morphology of dental nanocomposites polished by four different procedures evaluated by a multifractal approach. Appl Surf Sci 330:20–29

    Article  Google Scholar 

  66. Palaniappan S, Celis J-P, Van Meerbeek B, Peumans M, Lambrechts P (2013) Correlating in vitro scratch test with in vivo contact free occlusal area wear of contemporary dental composites. Dent Mater 29:259–268

    Article  Google Scholar 

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Correspondence to P. V. Antunes.

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Technical Editor: Estevam Las Casas.

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Carreira, M., Antunes, P.V., Ramalho, A. et al. Thermocycling effect on mechanical and tribological characterization of two indirect dental restorative materials. J Braz. Soc. Mech. Sci. Eng. 39, 1–17 (2017). https://doi.org/10.1007/s40430-016-0579-6

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  • DOI: https://doi.org/10.1007/s40430-016-0579-6

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