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Effect of Deformation Temperatures on Microstructure of AQ80 Magnesium Alloy under Repeated Upsetting-Extrusion

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Acta Metallurgica Sinica (English Letters) Aims and scope

Abstract

A new repeated upsetting-extrusion (RUE) process was proposed to improve the microstructure and the mechanical properties of Mg alloys. The effects of deformation temperature on the microstructure and microhardness of RUEed AQ80 Mg alloy were studied. The results showed that Mg alloy is subjected to sufficient corner shear deformation, upsetting deformation, and extrusion deformation, resulting in a large and uniformly distributed effective strain after RUE deformation. The microstructure is refined to an average grain size of 2.1 μm by the continuous dynamic recrystallization (CDRX) mechanism at 250 °C. As the temperature increases to 300 °C, the discontinuous dynamic recrystallization (DDRX) mechanism is activated and the average grain size is refined to 1.6 µm by the combined effect of CDRX and DDRX. In comparison to their parent grains, the orientations of the CDRXed grains show a clearly preferred orientation, but those of the DDRXed grains are completely different. At 350 °C, {10-12} extension twins appear in the microstructure, and the twinning-induced recrystallization (TDRX) mechanism plays an important role in grain refinement. With the two strengthening mechanisms of fine-grained strengthening and dislocation strengthening, the microhardness of the 250 °C sample is greatly improved, with an increase of about 35.1% compared to the initial sample.

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References

  1. P.D. Huo, F. Li, Y. Wang, R.Z. Wu, R.H. Gao, A.X. Zhang, Mater. Des. 219, 110696 (2022)

    Article  CAS  Google Scholar 

  2. K. Sheng, L.W. Lu, Y. Xiang, M. Ma, Z.Q. Wu, J. Magnes. Alloys 7, 717 (2019)

    Article  CAS  Google Scholar 

  3. W. Kang, L.W. Lu, L.B. Feng, F.C. Lu, C.L. Gan, X.H. Li, J. Magnes. Alloys 11, 317 (2023)

    Article  CAS  Google Scholar 

  4. B. Che, L.W. Lu, W. Kang, J. Luo, M. Ma, L.F. Liu, J. Alloys Compd. 862, 158700 (2021)

    Article  CAS  Google Scholar 

  5. X.W. Liu, L.P. Bian, F. Tian, S.J. Han, T. Wang, W. Liang, Mater. Charact. 188, 111910 (2022)

    Article  CAS  Google Scholar 

  6. H. Torabi, G. Faraji, A. Masoumi, J. Alloys Compd. 832, 154922 (2020)

    Article  CAS  Google Scholar 

  7. C. Cui, W.C. Zhang, W.Z. Chen, J. He, X.M. Chen, J.B. Hou, J. Magnes. Alloys 10, 2745 (2021)

    Article  Google Scholar 

  8. W.C. Liu, Y.J. Ke, K. Sugio, X.G. Liu, Y. Guo, G. Sasaki, Mater. Sci. Eng. A 850, 143574 (2022)

    Article  CAS  Google Scholar 

  9. M.D.A. Lage, M.D. Oliveira, P.H.R. Pereira, R.B. Figueiredo, V.F.C. Lins, J. Mater. Res. Technol. 18, 2745 (2022)

    Article  CAS  Google Scholar 

  10. H.K. Kim, W.J. Kim, Mater. Sci. Eng. A 385, 300 (2004)

    Article  Google Scholar 

  11. Q.H. Wei, L. Yuan, X. Ma, M.Y. Zheng, D.B. Shan, B. Guo, Mater. Sci. Eng. A 831, 142144 (2022)

    Article  CAS  Google Scholar 

  12. S.H. Lu, D. Wu, M. Yan, R.S. Chen, Materials 15, 1508 (2022)

    Article  CAS  Google Scholar 

  13. L.W. Lu, Z.J. Yin, S.H. Hu, L.F. Liu, D.F. Shi, B.L. Yang, Rare Metal Mater. Eng. 45, 1467 (2016)

    Google Scholar 

  14. X.Y. Liu, L.W. Lu, K. Sheng, T. Zhou, Acta Metall. Sin. -Engl. Lett. 32, 710 (2019)

    Article  CAS  Google Scholar 

  15. S. Amani, G. Faraji, K. Abrinia, J. Manuf. Process. 28, 197 (2017)

    Article  Google Scholar 

  16. Y.D. Yu, J. Li, S.Z. Kuang, J. Harbin Inst. Technol. 20, 20 (2015)

    Article  Google Scholar 

  17. L.C. Tang, C.M. Liu, Z.Y. Chen, D.W. Ji, H.C. Xiao, Mater. Des. 50, 587 (2013)

    Article  CAS  Google Scholar 

  18. M.J. Hao, W.L. Cheng, L.F. Wang, E. Mostaed, L.P. Bian, H.X. Wang, X.F. Niu, J. Magnes. Alloys 8, 899 (2020)

    Article  CAS  Google Scholar 

  19. Z.R. Liu, X. Zhao, K. Chen, S.Q. Wang, X.W. Ren, Z.M. Zhang, Y. Xue, Acta Metall. Sin. -Engl. Lett. 35, 839 (2022)

    Article  CAS  Google Scholar 

  20. X.Y. Liu, L.W. Lu, K. Sheng, Y. Xiang, Z.Q. Wu, JOM-US 71, 4726 (2019)

    Article  CAS  Google Scholar 

  21. T.T. Liu, Q.S. Yang, N. Guo, Y. Lu, B. Song, J. Magnes. Alloys 8, 66 (2020)

    Article  CAS  Google Scholar 

  22. C. Cui, J. He, W.K. Wang, W.Z. Chen, W.C. Zhang, J. Alloys Compd. 909, 164795 (2022)

    Article  CAS  Google Scholar 

  23. J.J. Bhattacharyya, S.R. Agnew, G. Muralidharan, Acta Mater. 86, 80 (2015)

    Article  CAS  Google Scholar 

  24. B. Li, M. Liao, Q. Ma, Z. McClelland, Comput. Mater. Sci. 101, 175 (2015)

    Article  CAS  Google Scholar 

  25. C.D. Barrett, A. Imandoust, A.L. Oppedal, K. Inal, M.A. Tschopp, H. El Kadiri, Acta Mater. 128, 270 (2017)

    Article  CAS  Google Scholar 

  26. K.D. Molodov, T. Al-Samman, D.A. Molodov, G. Gottstein, Acta Mater. 76, 314 (2014)

    Article  CAS  Google Scholar 

  27. I. Basu, T. Al-Samman, Acta Mater. 96, 111 (2015)

    Article  CAS  Google Scholar 

  28. S.H. Lu, D. Wu, R.S. Chen, E.-H. Han, Mater. Des. 191, 108600 (2020)

    Article  CAS  Google Scholar 

  29. H.C. Pan, R. Kang, J.R. Li, H.B. Xie, Z.R. Zeng, Q.Y. Huang, C.L. Yang, Y.P. Ren, G.W. Qin, Acta Mater. 186, 278 (2020)

    Article  CAS  Google Scholar 

  30. M.G. Jiang, C. Xu, H. Yan, G.H. Fan, T. Nakata, C.S. Lao, R.S. Chen, S. Kamado, E.H. Han, B.H. Lu, Acta Mater. 157, 53 (2018)

    Article  CAS  Google Scholar 

  31. H.X. Wang, W.Z. Chen, W.C. Zhang, D.Q. Fang, S.H. Wang, W.K. Wang, Mater. Sci. Eng. A 806, 140807 (2021)

    Article  CAS  Google Scholar 

  32. C.H. Park, C. Oh, S. Kim, Mater. Sci. Eng. A 542, 127 (2012)

    Article  CAS  Google Scholar 

  33. D.D. Gu, J. Peng, J.W. Wang, Z.T. Liu, F.S. Pan, Acta Metall. Sin. -Engl. Lett. 34, 1 (2021)

    Article  CAS  Google Scholar 

  34. A. Galiyev, R. Kaibyshev, G. Gottstein, Acta Mater. 49, 1199 (2001)

    Article  CAS  Google Scholar 

  35. Y.Z. Meng, J.M. Yu, G.S. Zhang, Y.J. Wu, Z.M. Zhang, Z. Shi, J. Magnes. Alloys 8, 1228 (2020)

    Article  CAS  Google Scholar 

  36. O. Sitdikov, R. Kaibyshev, Mater. Trans. 42, 1928 (2001)

    Article  CAS  Google Scholar 

  37. X. Liu, J.J. Jonas, L.X. Li, B.W. Zhu, Mater. Sci. Eng. A 583, 242 (2013)

    Article  CAS  Google Scholar 

  38. B.Q. Shi, R.S. Chen, W. Ke, J. Magnes. Alloys 1, 210 (2013)

    Article  CAS  Google Scholar 

  39. S.Q. Zhu, H.G. Yan, J.H. Chen, Y.Z. Wu, B. Su, Y.G. Du, X.Z. Liao, Scr. Mater. 67, 404 (2012)

    Article  CAS  Google Scholar 

  40. J.B. Jia, Y. Xu, Y. Yang, C. Chen, W.C. Liu, L.X. Hu, J.T. Luo, J. Alloys Compd. 721, 347 (2017)

    Article  CAS  Google Scholar 

  41. Q.H. Wang, B. Jiang, A.T. Tang, C. He, D.F. Zhang, J.F. Song, T.H. Yang, G.S. Huang, F.S. Pan, Mater. Sci. Eng. A 746, 259 (2019)

    Article  CAS  Google Scholar 

  42. S.B. Xu, J.Y. Liu, G.C. Ren, C.N. Jing, P. Liu, J. Plast. Eng. 28, 160 (2021)

    Google Scholar 

  43. W.L. Xu, J.M. Yu, L.C. Jia, C. Gao, Z. Miao, G.Q. Wu, G.J. Li, Z.M. Zhang, J. Magnes. Alloys 10, 3506 (2021)

    Article  Google Scholar 

  44. H. Yu, Y. Xin, M. Wang, Q. Liu, J. Mater. Sci. Technol. 34, 248 (2018)

    Article  CAS  Google Scholar 

  45. W.T. Sun, X.G. Qiao, M.Y. Zheng, X.J. Zhao, H.W. Chen, N. Gao, M.J. Starink, Scr. Mater. 155, 21 (2018)

    Article  CAS  Google Scholar 

  46. P. Zhang, S.X. Li, Z.F. Zhang, Mater. Sci. Eng. A 529, 62 (2011)

    Article  CAS  Google Scholar 

  47. X.Q. Zeng, Q.C. Zhu, Y.X. Li, W.J. Ding, Mater. China 38, 109 (2019)

    Google Scholar 

  48. M. Wang, X.Y. Xu, H.Y. Wang, L.H. He, M.X. Huang, Acta Mater. 201, 102 (2020)

    Article  CAS  Google Scholar 

  49. J.R. Li, D.S. Xie, H.S. Yu, R.L. Liu, Y.Z. Shen, X.S. Zhang, C.L. Yang, L.F. Ma, H.C. Pan, G.W. Qin, J. Alloys Compd. 835, 155228 (2020)

    Article  CAS  Google Scholar 

  50. M.J. Starink, X.Y. Cheng, S.F. Yang, Acta Mater. 61, 183 (2013)

    Article  CAS  Google Scholar 

  51. B. Che, L.W. Lu, J.L. Zhang, J.H. Zhang, M. Ma, L.F. Wang, F.G. Qi, Mater. Sci. Eng. A 832, 142475 (2022)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This work was partly supported by the National Natural Science Foundation of China (Grant Nos. 52174362 and 51975207), the Natural Science Foundation of Hunan Province (Grant no. 2023JJ10020 & 2021JJ30257), the Xiangtan Special Project for Building a National Innovative City (Grant No. CG-YB20221043), the Yancheng “Talent Plan of Yellow Sea Pearl” for Leading Talent Project.

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Correspondence to Liwei Lu, Hongliang Zhao or Wen Wang.

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Fan, Y., Lu, L., Zhao, H. et al. Effect of Deformation Temperatures on Microstructure of AQ80 Magnesium Alloy under Repeated Upsetting-Extrusion. Acta Metall. Sin. (Engl. Lett.) 36, 1649–1664 (2023). https://doi.org/10.1007/s40195-023-01562-3

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