Abstract
A weak transverse static magnetic field (WTSMF, 0–0.5 T) is applied to the directional solidification process of a DD3 Ni-based SX superalloy, aiming to tailor the microstructure and microsegregation of alloys. The mechanisms of microstructural refinement and microsegregation distribution caused by a WTSMF during directional solidification are discussed. It is shown that the primary dendrite arm spacing is rapidly reduced from 181 to 143 μm, and the average size of γ′ phase is significantly refined from 0.85 to 0.25 μm as the magnetic field increases from 0 to 0.5 T. At the same time, the volume fractions of γ/γ′ eutectic and the segregation coefficient are also gradually decreased. The 3D numerical simulations of the multiscale convection in liquid phase show that the modifications of the microstructure and microsegregation in DD3 are mainly attributed to the enhanced liquid flow caused by thermoelectric magnetic convection (TEMC) at dendrite/sample scale under the WTSMF. The maximum of the TEMC increases with increasing the magnetic field intensity. This work paves a simple way to optimize the microstructure and microsegregation in directionally solidified Ni-based SX superalloys without changing the processing parameters and composition.
Similar content being viewed by others
References
N. D’Souza, P.A. Jennings, X.L. Yang, H.B. Dong, P.D. Lee, M. McLean, Metall. Mater. Trans. B 36, 657 (2005)
H.B. Long, S.C. Mao, Y.N. Liu, Z. Zhang, X.D. Han, J. Alloys Compd. 743, 203 (2018)
C.J. Li, G. Guo, Z.J. Yuan, W.D. Xuan, Z.M. Ren, Y.B. Zhong, J. Alloys Compd. 720, 272 (2017)
D.X. Ma, A. Bührig-Polaczek, Metall. Mater. Trans. B 40, 738 (2009)
J. Zhang, L. Wang, D. Wang, G. Xie, Y.Z. Lu, J. Shen, L.H. Lou, Acta Metall. Sin. 55, 1077 (2019)
W.D. Xuan, H. Liu, C.J. Li, Z.M. Ren, Y.B. Zhong, X. Li, G.H. Cao, Metall. Mater. Trans. B 40, 828 (2016)
M.M. Franke, R.M. Hilbinger, A. Lohmüller, R.F. Singer, J. Mater. Proc. Technol. 213, 2081 (2013)
Y.J. Liang, A. Li, X. Cheng, X.T. Pang, H.M. Wang, J. Alloys Compd. 688, 133 (2016)
M.V. Nathal, Metal. Mater. Trans. A 18, 1961 (1987)
F. Pyczak, B. Devrient, F.C. Neuner, H. Mughrabi, Acta Mater. 53, 3879 (2005)
L. Liu, T.W. Huang, J. Zhang, H.Z. Fu, Mater. Lett. 61, 227 (2007)
G.E. Fuchs, Mater. Sci. Eng. A 300, 52 (2001)
M. Konter, M. Thumann, J. Mater. Process. Technol. 117, 386 (2001)
C.L. Brundidge, D. Vandrasek, B. Wang, T.M. Pollock, Metall. Mater. Trans. A 43, 965 (2012)
A.J. Elliott, S. Tin, W.T. King, S.C. Huang, M.F.X. Gigliotti, T.M. Pollock, Metall. Mater. Trans. A 35, 3221 (2004)
M. Konter, E. Kats, N. Hofmann, Superalloys, TMS (The Minerals, Metals and Materials Society). Pennsylvania 2000, 189–200 (2000)
S.D. Hu, L. Hou, K. Wang, Z.M. Liao, W. Zhu, A.H. Yi, W.F. Li, Y. Fautrelle, X. Li, J. Mater. Sci. Technol. 76, 207 (2021)
H. Yasuda, I. Ohnaka, S. Fujimoto, N. Takezawa, A. Tsuchiyama, T. Nakan, Scr. Mater. 54, 527 (2006)
Y. Hou, Z.Q. Zhang, W.D. Xuan, J. Wang, J.B. Yu, Z.M. Ren, Acta Metall. Sin. -Engl. Lett. 31, 681 (2018)
K.L. Zhang, Y.J. Li, Y.S. Yang, Acta Metall. Sin. -Engl. Lett. 33, 1442 (2020)
X. Li, A. Gagnoud, Y. Fautrelle, R. Moreau, D.F. Du, Z.M. Ren, Metall. Mater. Trans. A 47, 2952 (2016)
X.T. Yuan, T. Zhou, W.L. Ren, J.C. Peng, T.X. Zheng, L. Hou, J.B. Yu, Z.M. Ren, P.K. Liaw, Y.B. Zhong, J. Mater. Sci. Technol. 62, 52 (2021)
X. Li, Y. Fautrelle, A. Gagnoud, D.F. Du, J. Wang, Z.M. Ren, H. Nguyen-Thi, N. Mangelinck-Noel, Acta Mater. 64, 367 (2014)
I. Kaldre, Y. Fautrelle, J. Etay, A. Bojarevics, L. Buligins, J. Alloys Compd. 571, 50 (2013)
X. Li, J. Wang, J. Zhang, Y.F. Han, X. Li, Mater. 8, 3428 (2015)
W.D. Xuan, H. Liu, J. Lan, C.J. Li, Y.B. Zhong, X. Li, G.H. Cao, Z.M. Ren, Metall. Trans. B 47, 3231 (2016)
Y.J. Li, Y.F. Teng, X.H. Feng, Y.S. Yang, J. Mater. Sci. Technol. 33, 105 (2017)
X. Li, Y. Fautrelle, Z.M. Ren, Acta Mater. 55, 3803 (2007)
X. Li, Z.M. Ren, J. Wang, Y.F. Han, B.D. Sun, Mater. Lett. 67, 205 (2012)
G. Pottlacher, H. Hosaeus, B. Wilthan, E. Kaschnitb, A. Seifter, Thermochim. Acta 382, 255 (2002)
H. Carreon, Nondestruct. Test Eval. 24, 233 (2009)
B.C. Dupree, J.E. Enderby, R.J. Newport, J.B. Van Zytveld, Inst. Phys. Conf. Ser. 30, 337 (1977)
S. Steinbach, L. Ratke, Metall. Mater. Trans. A 38, 1388 (2007)
C.J. Paradies, R.N. Smith, M.E. Glicksman, Metall. Mater. Trans. A 28, 875 (1997)
P.A. Curreri, J.E. Lee, D.M. Stefanescu, Metall. Trans. Trans. A 19, 2671 (1988)
P. Lehamann, R. Moreau, D. Camel, R. Bolcato, J. Cryst. Growth 183, 690 (1998)
W.D. Xuan, J. Lan, H. Liu, C.J. Li, X. Li, Z.M. Ren, Metall. Mater. Trans. A 48, 3804 (2017)
X.P. Guo, H.Z. Fu, J.H. Sun, Metall. Trans. A 28, 997 (1997)
J.M. Xiao, Alloy Phase and Its Transformation (The Chinese Metallurgical Publishing House, Beijing, 1987), pp. 233–235
F. Wang, D. Ma, J. Zhang, L. Liu, J. Hong, S. Bogner, A. Bührig-Polaczek, J. Cryst. Growth 389, 47 (2014)
L. Abou-Khalil, G. Salloum-Abou-Jaoude, G. Reinhart, C. Pickmann, G. Zimmermann, H. Nguyen-Thi, Acta Mater. 110, 44 (2016)
Acknowledgements
This work was financially supported by the National Natural Science Foundation of China (Nos. 51690163, 52130204, 52174376, 51822405), the Science and Technology Innovation Team Plan of Shaan Xi Province (No. 2021TD-17), the Joint Research Funds of the Department of Science & Technology of Shaanxi Province and NPU (No. 2020GXLH-Z-024), the Fundamental Research Funds for the Central Universities (No. D5000210902), the Key R&D Program of ShaanXi Province (No. 2019ZDLGY 04-04), and the Research Fund of the State Key Laboratory of Solidification Processing (NPU) (No. 2019-QZ-02).
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
The authors state that there are no conflicts of interest to disclose.
Additional information
Available online at http://link.springer.com/journal/40195
Rights and permissions
About this article
Cite this article
Zhao, Y., Su, H., Fan, G. et al. Tailoring Microstructure and Microsegregation in a Directionally Solidified Ni-Based SX Superalloy by a Weak Transverse Static Magnetic Field. Acta Metall. Sin. (Engl. Lett.) 35, 1164–1174 (2022). https://doi.org/10.1007/s40195-022-01372-z
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s40195-022-01372-z