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Single-walled carbon nanohorns and cobalt@nitrogen-doped carbon nanotube polyhedrons modified electrode as sensitive electrochemical sensing platform for luteolin detection

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Abstract

In this work, ZIF-8@ZIF-67 was prepared and pyrolyzed to obtain Co nanoparticles-embedded N-doped carbon nanotube hollow polyhedron (Co@NCNHP). Then, single-walled carbon nanohorns (SWCNHs) were mixed with Co@NCNHP to obtain the SWCNHs-Co@NCNHP composite. The morphological structure of the prepared material was characterized by scanning electron microscopy, and the as-prepared SWCNHs-Co@NCNHP was modified on the surface of glassy carbon electrode (GCE). The modified electrode was used as electrochemical sensor for analysis of luteolin. Because of the excellent synergistic effects between SWCNHs and Co@NCNHP, the sensor based on SWCNHs-Co@NCNHP/GCE could be used to detect luteolin with the detection range from 0.1 to 4.0 μM and the low limit of detection of 10.0 nM (S/N = 3). Besides, the fabricated sensor showed favorable selectivity and stability, and was used in the analysis of luteolin in Duyiwei capsules with satisfactory results.

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Acknowledgements

The work is supported by the Key Research and Development Program of Hainan Province (ZDYF2020204), the National Natural Science Foundation of China (21964007, 21665007) and the Open Foundation of Key Laboratory of Laser Technology and Optoelectronic Functional Materials of Hainan Province (2022LTOM04).

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Author notes

  1. Yijing Ai and Guiling Luo these authors contributed to equllly to this work.

Authors and Affiliations

  1. Key Laboratory of Water Pollution Treatment and Resource Rouse of Hainan Province, Key Laboratory of Functional Materials and Photoelectrochemistry of Haikou, College of Chemistry and Chemical Engineering, Hainan Normal University, Haikou, 571158, People’s Republic of China

    Yijing Ai, Guiling Luo, Lijun Yan, Yucen Yao, Zejun Zhang, Bei Wang & Wei Sun

  2. College of Chemical and Environmental Engineering, Chongqing University of Arts and Sciences, Chongqing, 402160, People’s Republic of China

    Yucen Yao

  3. College of Chemistry and Chemical Engineering, Zhaotong University, Zhaotong, 657000, People’s Republic of China

    Zejun Zhang

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  1. Yijing Ai
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  2. Guiling Luo
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Correspondence to Bei Wang or Wei Sun.

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Ai, Y., Luo, G., Yan, L. et al. Single-walled carbon nanohorns and cobalt@nitrogen-doped carbon nanotube polyhedrons modified electrode as sensitive electrochemical sensing platform for luteolin detection. J IRAN CHEM SOC 20, 319–325 (2023). https://doi.org/10.1007/s13738-022-02652-2

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