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In situ X-ray micro-CT for investigation of damage evolution in black shale under uniaxial compression

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Abstract

Crack damage evolution of shale is crucial to the hydraulic fracturing treatment and engineering stability. Although many effects have been done on the macroscopic characteristics of shale, yet the microscopic failure mechanism is not well understood. A uniaxial compressive test on black shale was conducted under topographic monitoring using in situ X-ray micro-tomography (µCT). A series of high-resolution reconstruction images were obtained by carrying out CT scans at six key points throughout the test to obtain the internal structure of shale sample. In addition, the CT values for the purpose of crack damage evolution in shale were identified. Clear 2D/3D CT images, CT value analysis and image segmentation analysis reveal that the sample experiences compression, damage, cracking, crack propagation, and collapse stages. Crack geometry and distribution in the shale sample is visualized by rendered CT images, and a combined tension and shear failure mode is observed from the fracture rose diagram. This work suggests that formation and propagation of fractures are influenced by the stratified structure and weak cementation medium between layers.

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References

  • Duchesne MJ, Moore F, Long BF, Labrie J (2009) A rapid method for converting medical computed tomography scanner topogram attenuation scale to Hounsfield Unit scale and to obtain relative density values. Eng Geol 103(3–4):100–105

    Article  Google Scholar 

  • Fjær E, Nes OM (2014) The impact of heterogeneity on the anisotropic strength of an outcrop shale. Rock Mech Rock Eng 47(5):1603–1611

    Article  Google Scholar 

  • Heng S, Yang CH, Zhang BP, Guo YT, Wang L, Wei YL (2014) Experimental research on anisotropic properties of shale. Rock Soil Mech 2014, 36(3):610–616

    Google Scholar 

  • Heng S, Guo Y, Yang CH (2015) Experimental and theoretical study of the anisotropic properties of shale. Int J Rock Mech Min Sci 74:58–68

    Article  Google Scholar 

  • Karpyn ZT, Alajmi A, Radaelli F, Halleck PM, Grader AS (2009) X-ray CT and hydraulic evidence for a relationship between fracture conductivity and adjacent matrix porosity. Eng Geol 103(3):139–145

    Article  Google Scholar 

  • King GE (2010) Thirty years of gas shale fracturing: what have we learned? In: Proceedings of the SPE annual technical conference and exhibition, Florence, Italy, 19–22 September

  • Lemaitre J, Chaboche JL (1990) Mechanics of solid materials. Cambridge University Press, Cambridge

    Book  Google Scholar 

  • Liu J, Li Y, Zhang H (2015) Study on shale’s dynamic damage constitutive model based on statistical distribution. Shock Vib 33:323–334

    Google Scholar 

  • Masri M, Sibai M, Shao JF (2014) Experimental investigation of the effect of temperature on the mechanical behavior of Tournemire shale. Int J Rock Mech Min Sci 70:185–191

    Article  Google Scholar 

  • Meier T, Rybacki E, Backers T (2015) Influence of bedding angle on borehole stability: a laboratory investigation of transverse isotropic oil shale. Rock Mech Rock Eng 48(4):1535–1546

    Article  Google Scholar 

  • Mokhtari M, Alqahtani AA, Tutuncu AN (2013) Failure behavior of anisotropic shales[C]//47th US Rock Mechanics/Geomechanics Symposium. American Rock Mechanics Association

  • Mokhtari M, Bui BT, Tutuncu AN (2014) Tensile failure of shales: impacts of layering and natural fractures. In SPE Western North American and Rocky Mountain Joint Meeting. Society of Petroleum Engineers

  • Pradhan S, Stroisz AM, Fjær E, Hans KL, Eyvind FS (2015) Stress-induced fracturing of reservoir rocks: acoustic monitoring and µCT image analysis. Rock Mech Rock Eng 48(6):2529–2540

    Article  Google Scholar 

  • Rybacki E, Reinicke A, Meier T, Makasi M, Dresen G (2015) What controls the mechanical properties of shale rocks?—part I: strength and Young’s modulus. J Petrol Sci Eng 135:702–722

    Article  Google Scholar 

  • Rybacki E, Meier T, Dresen G (2016) What controls the mechanical properties of shale rocks?—part II: brittleness. J Petrol Sci Eng 144:39–58

    Article  Google Scholar 

  • Singh UK, Digby PJ (1989) A continuum damage model for simulation of the progressive failure of brittle rocks. Int J Solids Struct 25(6):647–663

    Article  Google Scholar 

  • Sone H, Zoback MD (2013) Mechanical properties of shale-gas reservoir rocks—part 2: Ductile creep, brittle strength, and their relation to the elastic modulus. Geophysics 78(5):D393–D402

    Article  Google Scholar 

  • Suarez-Rivera R, Burghardt J, Stanchits S (2013) Understanding the effect of rock fabric on fracture complexity for improving completion design and well performance[C]//IPTC 2013: International Petroleum Technology Conference

  • Tan P, Jin Y, Han K, Hou B, Chen M, Guo X, Gao J (2017) Analysis of hydraulic fracture initiation and vertical propagation behavior in laminated shale formation. Fuel 206:482–493

    Article  Google Scholar 

  • Wang Y, Li CH (2017) Investigation of the P-and S-wave velocity anisotropy of a Longmaxi formation shale by real-time ultrasonic and mechanical experiments under uniaxial deformation. J Petrol Sci Eng 158:253–267

    Article  Google Scholar 

  • Wang Y, Li X, Wu YF, Lin C, Zhang B (2015) Experimental study on meso-damage cracking characteristics of RSA by CT test. Environ Earth Sci 73(9):5545–5558

    Article  Google Scholar 

  • Wang Y, Li X, Zhang B (2016a) Analysis of fracturing network evolution behaviors in random naturally fractured rock block. Rock Mech Rock Eng 49(11):4339–4347

    Article  Google Scholar 

  • Wang Y, Li X, Zhang B, Zhao ZH (2016b) Optimization of multiple hydraulically fractured factors to maximize the stimulated reservoir volume in silty laminated shale formation, Southeastern Ordos Basin, China. J Petrol Sci Eng 145:370–381

    Article  Google Scholar 

  • Wang Y, Li CH, Hao J, Zhou RQ (2018) X-ray micro-tomography for investigation of meso-structural changes and crack evolution in Longmaxi formation shale during compressive deformation. J Petrol Sci Eng 164:278–288

    Article  Google Scholar 

  • Watanabe Y, Lenoir N, Otani J, Nakai T (2012) Displacement in sand under triaxial compression by tracking soil particles on X-ray CT data. Soils Found 52(2):312–320

    Article  Google Scholar 

  • Wei YL, Yang CH, Guo YT, Liu W, Xu JB (2015) Experimental research on deformation and fracture characteristics of shale under cyclic loading. Chin J Geotech Eng 37(12):2263–2271

    Google Scholar 

  • Zhou XP, Zhang YX, Ha QL (2008) Real-time computerized tomography (CT) experiments on limestone damage evolution during unloading. Theoret Appl Fract Mech 50(1):49–56

    Article  Google Scholar 

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Acknowledgements

The authors would like to thank the editors and the anonymous reviewers for their helpful and constructive comments. This work was supported by the National key technologies Research & Development program (2018YFC0808402), the Fundamental Research Funds for the Central Universities (2302017FRF-TP-17-027A1), and the National Natural Science Foundation of China (Grants Nos. 41502294).

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Correspondence to Y. Wang.

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Wang, Y., Hou, Z.Q. & Hu, Y.Z. In situ X-ray micro-CT for investigation of damage evolution in black shale under uniaxial compression. Environ Earth Sci 77, 717 (2018). https://doi.org/10.1007/s12665-018-7904-6

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