Abstract
The present study evaluates the influence of the replacement of natural sand for different contents of water treatment sludge (in wet and calcined conditions) on the performance of the concrete considering macro and micro scale analyses. Mixtures substituting 5, 7, and 10% of wet sludge (WS) and 5, 10, and 20% of calcined sludge (CS) were produced. For the macro scale analyses, the specimens were tested by water absorption, compressive and tensile strength, and modulus of elasticity. Carbonation, leaching, microtomography 3D, and SEM were carried out for the micro-scale analyses. From the results obtained, it can be observed that the WS significantly reduces the strength of concrete, not being indicated for applications in structural concrete. The replacement of up to 20% of sand with CS. In addition to increasing the compressive strength of the concrete, increased porosity, water absorption, and carbonation depth requires attention to durability aspects for using this residue in the production of structural and non-structural concretes. Using wastewater treatment sludge can contribute to circularity in the construction industry in line with sustainable development goals.
Graphical Abstract
Similar content being viewed by others
Data Availability
The data will be made available upon request to the authors.
References
Smol M. Circular economy approach in the water and wastewater sector. In: Circular Economy and Sustainability. Elsevier, London, 2022. p. 1–19
Brasil. Plano Nacional de Resíduos Sólidos [Internet]. Brasília; 2020 [cited 2023 Feb 24]. Available from: https://portal-api.sinir.gov.br/wp-content/uploads/2022/07/Planares-B.pdf
Ren, B., Zhao, Y., Ji, B., Wei, T., Shen, C.: Granulation of drinking water treatment residues: Recent advances and prospects. Water 12(5), 1400 (2020)
Bundhoo, Z.M.A.: Solid waste management in least developed countries: Current status and challenges faced. J. Mater. Cycles Waste Manag. 20, 1867–1877 (2018)
Bandieira, M., Zat, T., Schuster, S.L., et al.: Water treatment sludge in the production of red-ceramic bricks: Effects on the physico-mechanical properties. Mater. Struct. Mater. Constr. 54, 168 (2021)
Ramirez, K.G., Possan, E., Dezen, B.G., Colombo, M.: Potential uses of waste sludge in concrete production. Manag. Environ. Quality Int. J. 28(6), 821–38 (2017)
Carlos, A.R.: Tratamento de Lodos de Estações de Tratamento de Água, 1st edn. Bulcher, São Paulo (2021)
Ahmad, T., Ahmad, K., Alam, M.: Sustainable management of water treatment sludge through 3 ‘R’concept. J. Clean. Product. 15(124), 1–3 (2016)
Mojapelo, K.S., Kupolati, W.K., Ndambuki, J.M., Sadiku, E.R., Ibrahim, I.D., Maepa, C.: Sustainable usage and the positive environmental impact of wastewater dry sludge-based concrete. Results Mater. 1(16), 100336 (2022)
Andrade, J.J., Possan, E., Wenzel, M.C., Silva, S.R.: Feasibility of using calcined water treatment sludge in rendering mortars: A technical and sustainable approach. Sustainability 11(13), 3576 (2019)
de Oliveira Andrade, J.J., Wenzel, M.C., da Rocha, G.H., da Silva, S.R.: Performance of rendering mortars containing sludge from water treatment plants as fine recycled aggregate. J. Clean. Product. 10(192), 159–68 (2018)
Mañosa, J., Formosa, J., Giro-Paloma, J., Maldonado-Alameda, A., Quina, M.J., Chimenos, J.M.: Valorisation of water treatment sludge for lightweight aggregate production. Construct. Build. Mater. 1(269), 121335 (2021)
Cremades, L.V., Cusidó, J.A., Arteaga, F.: Recycling of sludge from drinking water treatment as ceramic material for the manufacture of tiles. J. Clean. Prod. 201, 1071–1080 (2018)
Ling, Y.P., Tham, R.H., Lim, S.M., et al.: Evaluation and reutilization of water sludge from fresh water processing plant as a green clay substituent. Appl. Clay. Sci. 143, 300 (2017)
Hagemann, S.E., Gastaldini, A.L.G., Cocco, M., et al.: Synergic effects of the substitution of Portland cement for water treatment plant sludge ash and ground limestone: Technical and economic evaluation. J. Clean. Prod. 214, 916–926 (2019)
Liu, Y., Zhuge, Y., Chow, C.W.K., et al.: The potential use of drinking water sludge ash as supplementary cementitious material in the manufacture of concrete blocks. Resour. Conserv. Recycl. 168, 105291 (2021)
de Godoy, L.G.G., Rohden, A.B., Garcez, M.R., et al.: Valorization of water treatment sludge waste by application as supplementary cementitious material. Constr. Build. Mater. 223, 939 (2019)
Danish, A., Ozbakkaloglu, T.: Greener cementitious composites incorporating sewage sludge ash as cement replacement: A review of progress, potentials, and future prospects. J. Clean. Prod. 371, 13334 (2022)
Ruviaro, A.S., Silvestro, L., Scolaro, T.P., et al.: Use of calcined water treatment plant sludge for sustainable cementitious composites production. J. Clean. Prod. 327, 129484 (2021)
Sales, A., De Souza, F.R., Dos Santos, W.N., et al.: Lightweight composite concrete produced with water treatment sludge and sawdust: Thermal properties and potential application. Constr. Build. Mater. 24, 2446–2453 (2010)
Sales, A., De Souza, F.R., Almeida, F.D.C.R.: Mechanical properties of concrete produced with a composite of water treatment sludge and sawdust. Constr. Build. Mater. 25, 2793–2798 (2011)
Mojapelo, K.S., Kupolati, W.K., Ndambuki, J.M., et al.: Utilization of wastewater sludge for lightweight concrete and the use of wastewater as curing medium. Case Stud. Constr. Mater. 15, e00667 (2021)
Ramirez, K.G., Possan, E., Bittencourt, P.R.S., et al.: Physico-chemical characterization of centrifuged sludge from the Tamanduá water treatment plant (Foz do Iguaçu, PR). Revista Materia. 18, 23 (2018)
Dahhou, M., El Hamidi, A., El Moussaouiti, M.: Reusing drinking water sludge: Physicochemical features, environmental impact and applications in building materials: A mini review. Chem. Afr. 20, 1–7 (2023)
Gomes, S.D.C., Zhou, J.L., Li, W., et al.: Recycling of raw water treatment sludge in cementitious composites: Effects on heat evolution, compressive strength and microstructure. Resour. Conserv. Recycl. 161, 104970 (2020)
Turner, T., Wheeler, R., Stone, A., et al.: Potential Alternative Reuse Pathways for Water Treatment Residuals: Remaining Barriers and Questions—A Review. Springer International Publishing, Water Air Soil Pollut (2019)
Fiore, F.A., Rodgher, S., Ito, C.Y., dos Santos Bardini, V.S., Klinsky, L.M.: Water sludge reuse as a geotechnical component in road construction: Experimental study. Clean. Eng. Technol. 1(9), 100512 (2022)
Smol, M., Kulczycka, J., Henclik, A., Gorazda, K., Wzorek, Z.: The possible use of sewage sludge ash (SSA) in the construction industry as a way towards a circular economy. J. Clean. Prod. 15(95), 45–54 (2015). https://doi.org/10.1016/j.jclepro.2015.02.051
Barrera-Díaz, C., Martínez-Barrera, G., Gencel, O., et al.: Processed wastewater sludge for improvement of mechanical properties of concretes. J. Hazard. Mater. 192, 108–115 (2011)
ABNT. NBR 9779: Mortar and Hardened Concrete — Determination of Water Absorption by Capillarity. Rio de Janeiro; 2021
ABNT. NBR 5739: Concrete - Compression Test of Cylindrical Specimens. Rio de Janeiro: Brazilian National Standards Organization; 2018
ABNT. NBR 7222: Concrete and Mortar - Determination of the Tension Strength by Diametrical Compression of Cylindrical Test Specimens. Rio de Janeiro: Brazilian National Standards Organization; 2011
ABNT. NBR 8522: Concrete - Determination of Static Modulus of Elasticity and Deformation by Compression. Rio de Janeiro: Brazilian National Standards Organization; 2017
Pauletti, C., Possan, E., Dal Molin, D.C.: Accelerated carbonation: State of the art of research in Brazil. Ambiente Construído. 7(4), 7–20 (2007)
ABNT. NBR 10005. Procedure for Obtention Leaching Extract of Solid Wastes. Rio de Janeiro; 2004
RILEM. Measurement of Hardened Concrete Carbonation Depth. 1988
Sandoval, G.F., Jussiani, E.I., de Moura, A.C., Andrello, A.C., Toralles, B.M.: Hydraulic and morphological characterization of clogged pervious concrete (PC). Constr. Build. Mater. 7(322), 126464 (2022)
Wang, Y.-S., Dai, J.-G.: X-ray computed tomography for pore-related characterization and simulation of cement mortar matrix. NDT E Int. 86, 28–35 (2017)
Provis, J.L., Myers, R.J., White, C.E., et al.: X-ray microtomography shows pore structure and tortuosity in alkali-activated binders. Cem. Concr. Res. 42, 855–864 (2012)
Rougelot, T., Burlion, N., Bernard, D., et al.: About microcracking due to leaching in cementitious composites: X-ray microtomography description and numerical approach. Cem. Concr. Res. 40, 271–283 (2010)
Rattanasak, U., Kendall, K.: Pore structure of cement/pozzolan composites by X-ray microtomography. Cem. Concr. Res. 35, 637–640 (2005)
Wang, L., Zou, F., Fang, X., et al.: A novel type of controlled low strength material derived from alum sludge and green materials. Constr. Build. Mater. 165, 792–800 (2018)
Gomes, S.D., Zhou, J.L., Li, W., Long, G.: Progress in manufacture and properties of construction materials incorporating water treatment sludge: A review. Resour. Conserv. Recycl. 1(145), 148–59 (2019)
Monzó, J., Payá, J., Borrachero, M.V., et al.: Use of sewage sludge ash(SSA)-cement admixtures in mortars. Cem. Concr. Res. 26, 1389–1398 (1996)
Toledo Filho RD, Fontes CMA. Sewage sludge ash. Sustainable Concrete Made with Ashes and Dust from Different Sources. Elsevier; 2022. pp. 233–279
Smol, M., Kulczycka, J., Henclik, A., Gorazda, K., Wzorek, Z.: The possible use of sewage sludge ash (SSA) in the construction industry as a way towards a circular economy. J. Clean. Product. 15(95), 45–54 (2015)
Hoppen, C., Portella, K.F., Joukoski, A., Trindade, E.M., Andreóli, C.V.: Uso de lodo de estação de tratamento de água centrifugado em matriz de concreto de cimento portland para reduzir o impacto ambiental. Química Nova 29, 79–84 (2006)
Yagüe, A., Valls, S., Vázquez, E., et al.: Durability of concrete with addition of dry sludge from waste water treatment plants. Cem. Concr. Res. 35, 1064–1073 (2005)
ABNT. NBR 10004: Solid Waste - Classification. Rio de Janeiro; 2004
Valls, S., Vazquez, E.: Leaching properties of stabilised/solidified cement-admixtures-sewage sludges systems. Waste Manag. 22(1), 37–45 (2002)
Liu, Y., Zhuge, Y., Chow, C.W., Keegan, A., Pham, P.N., Li, D., Qian, G., Wang, L.: Recycling drinking water treatment sludge into eco-concrete blocks with CO2 curing: Durability and leachability. Sci. Total Environ. 1(746), 141182 (2020)
Liu, Y., Zhuge, Y., Chow, C.W.K., et al.: Utilization of drinking water treatment sludge in concrete paving blocks: Microstructural analysis, durability and leaching properties. J. Environ. Manag. 262, 110352 (2020)
Kulakowski, M.P., Pereira, F.M., Dal Molin, D.C.: Carbonation-induced reinforcement corrosion in silica fume concrete. Constr. Build. Mater. 23(3), 1189–95 (2009)
Parrott, L.J.: A Review of Carbonation in Reinforced Concrete. British Cement Association, London (1987)
Possan, E., Thomaz, W.A., Aleandri, G.A., et al.: CO2 uptake potential due to concrete carbonation: A case study. Case Stud. Constr. Mater. 6, 147–161 (2017). https://doi.org/10.1016/j.cscm.2017.01.007
Mazurana, L., Bittencourt, P.R.S., Scremin, F.R., et al.: Determination of Co2 capture in rendering mortars produced with recycled construction and demolition waste by thermogravimetry. J. Therm. Anal. Calorim. 3, 1 (2021)
Ekolu, S.O.: A review on effects of curing, sheltering, and CO2 concentration upon natural carbonation of concrete. Constr. Build. Mater. 30(127), 306–20 (2016)
Yao, X., Xu, Z., Guan, J., Liu, L., Shangguan, L., Xi, J.: Influence of wastewater content on mechanical properties, microstructure, and durability of concrete. Buildings 12(9), 1343 (2022)
Andrade, J.J., Possan, E., Wenzel, M.C., Silva, S.R.: Feasibility of using calcined water treatment sludge in rendering mortars: A technical and sustainable approach. Sustainability 11(13), 3576 (2019). https://doi.org/10.3390/su11133576
Acknowledgements
The authors thank the Itaipu Concrete Technology Laboratory for supporting the experimental project and the Sanepar's research support. For research support, to Unila's Performance, Structures, and Materials Laboratory (CNM-LADEMA) and PRPPG. The authors also thank Professor Paulo Rodrigo Stival Bittencourt for his participation in the chemical part.
Author information
Authors and Affiliations
Contributions
EP: Funding acquisition; Conceptualization, Supervision, Methodology, writing-original draft preparation, writing- reviewing and editing. KGR: Experimental work and data collection. JJde OA: Discussion of results, writing- reviewing and editing. G F. B. S: writing-original draft preparation, discussion of results, writing-reviewing and editing.
Corresponding author
Ethics declarations
Conflict of interest
The authors declare that there is no conflict of interest.
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
About this article
Cite this article
Possan, E., Ramirez, K.G., de Oliveira Andrade, J.J. et al. Concrete with Wet and Calcined Water Treatment Plant Waste: Macro and Micro Scale Analysis. Waste Biomass Valor 15, 2611–2623 (2024). https://doi.org/10.1007/s12649-023-02311-4
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s12649-023-02311-4