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Plasma Dynamic Synthesis of Dispersed Cu/SiC Composites with a Controlled Phase Composition

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Abstract

Obtaining bulk copper-based composite materials with improved physical and mechanical properties often requires pre-treatment of the initial raw materials. Especially it concerns metal matrix composites (MMC) containing copper as a matrix and silicon carbide as a reinforcing component. However, the final properties of Cu/SiC MMC depend on successful solving the problem of silicon solubility in liquid-phase copper during the sintering process. In this work, we demonstrate the possibility of high-energy treatment of copper and silicon carbide by the plasma dynamic method to obtain a pre-activated charge for further sintering. Analytical studies by X-ray diffractomtery (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) methods testify to the possibility of obtaining highly dispersed composite Cu/SiC materials of different phase and grain size composition depending on the synthesis conditions. The application of polymodal Cu/SiC powders pre-activated by the plasma dynamic method as a charge is established to ensure producing bulk samples by the spark plasma sintering (SPS) method and allow increasing the relative density by ~ 5%–10% and the hardness of the final products by more than 30% compared with pure copper samples produced by the same method.

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Data Availability

The datasets generated during and/or analyzed during the current study are not publicly available due to the Russian Federation legislation in the field of materials published abroad but are available from the corresponding author on reasonable request.

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Acknowledgements

This work was supported by the Russian Science Foundation, grant number 21-73-10245, https://rscf.ru/project/21-73-10245/.

Funding

This work was supported by the Russian Science Foundation, Grant number 21–73-10245, https://rscf.ru/project/21-73-10245/.

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Authors and Affiliations

  1. Institute of Environmental and Agricultural Biology (X-BIO), Tyumen State University, 6 Volodarskogo St., Tyumen, Russian Federation, 625003

    Ivan Shanenkov, Dmitriy Nikitin & Alexander Tsimmerman

  2. School of Energy and Power Engineering, Tomsk Polytechnic University, 30 Lenin av., Tomsk, Russian Federation, 634050

    Ivan Shanenkov, Dmitriy Nikitin, Artur Nassyrbayev, Yuliya Vympina, Alexander Tsimmerman & Aleksandr Sivkov

  3. College of Communication Engineering, Jilin University, 2699 Qianjin St., Changchun, 130023, People’s Republic of China

    Aleksandr Sivkov

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Contributions

All authors contributed to the study conception and design. All experiments were performed by AN and AT. Ponomarev, under the supervision of AS. YV was responsible for analyzing synthesized powder by means of SEM and TEM methods. XRD studies and their interpretation were performed by IS. DN was responsible for spark plasma sintering procedure. Material preparation, data collection and analysis were performed by IS and DN. The original draft was written by IS and DN and all authors commented on previous versions of the manuscript. All authors read and approved the final manuscript.

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Correspondence to Ivan Shanenkov.

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Shanenkov, I., Nikitin, D., Nassyrbayev, A. et al. Plasma Dynamic Synthesis of Dispersed Cu/SiC Composites with a Controlled Phase Composition. Met. Mater. Int. 30, 814–831 (2024). https://doi.org/10.1007/s12540-023-01533-4

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