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Properties and rapid consolidation of nanocrystalline 8MoSi2-Si3N4 by high frequency induction heated sintering

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Abstract

Nanopowders of MoSi2 and Si3N4 were synthesized from Mo2N and Si by high ball milling. Dense nanostructured 8MoSi2-Si3N4 composite was consolidated by high frequency induction heated sintering (HFIHS) method within two minutes from mechanically synthesized powders of MoSi2 and Si3N4. Highly dense 8MoSi2-Si3N4 composite with a relative density of up to 97 % was produced under simultaneous application of 80 MPa pressure and the induced current. The average grain size and mechanical properties (hardness and fracture toughness) of the composite were investigated.

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Authors and Affiliations

  1. Division of Advanced Materials Engineering, the Research Center of Advanced Materials Development, Chonbuk National University, 664-14 Deokjin-dong 1-ga, Deokjin-gu, Jeonju, Jeonbuk, 561-756, Korea

    Na-Ra Park, In-Yong Ko & In-Jin Shon

  2. Advanced Functional Materials Research Center, Korea Institute of Science and Technology, PO Box 131, Cheongryang, Seoul, 130-650, Korea

    Jin-Kook Yoon & Jung-Mann Doh

  3. Department of Hydrogen and Fuel Cells Engineering, Specialized Graduate School, Chonbuk National University, Jeonbuk, 561-756, Korea

    In-Jin Shon

Authors
  1. Na-Ra Park
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  2. In-Yong Ko
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  3. Jin-Kook Yoon
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  4. Jung-Mann Doh
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  5. In-Jin Shon
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Correspondence to In-Jin Shon.

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Park, NR., Ko, IY., Yoon, JK. et al. Properties and rapid consolidation of nanocrystalline 8MoSi2-Si3N4 by high frequency induction heated sintering. Met. Mater. Int. 17, 233–237 (2011). https://doi.org/10.1007/s12540-011-0408-5

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  • DOI: https://doi.org/10.1007/s12540-011-0408-5

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