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Evaluation of Enhanced UV Protection Property of Dyed Cotton Fabrics Based on Inclusion Complex of β-cyclodextrin with Natural Coumarin Extracted from Cortex fraxini

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Abstract

Inclusion complex formed between β-cyclodextrin (β-CD) and natural coumarins extracted from Cortex fraxini were utilized to dye and enhancing the UV protection properties of cotton fabric. Natural coumarins were extracted from Cortex fraxini and the total amount of natural coumarins was evaluated. The inclusion complex of natural coumarins with β-CD were formed and analyzed by ultraviolet-visible spectrum, fluorescence spectroscopy, FTIR and TGA. The obtained results showed that a stoichiometry of 1:1 inclusion complex was formed and the fluorescence intensities and ultraviolet absorption of the natural coumarins were both enhanced by incorporating into β-CD. β-CD was grafted onto cotton fabric based on esterification of citric acid with cellulose and cyclodextrin in the presence of sodium hypophosphite. The grafted cotton fabric was then dyed with natural coumarins extraction of Cortex fraxini as natural ultraviolet absorbent to form stable inclusion complex. UV protection factor (UPF), UVA transmittance (TUVA) and UVB transmittance (TUVB), wrinkle recovery and tensile strength of dyed fabrics were evaluated and demonstrated that graft modification of fabrics with β-CD resulted enhancement in UV protection property and durability accompanied with increasing in wrinkle recovery properties and decreasing in tensile strength. Furthermore, apparent morphology, FTIR and TGA analysis of inclusion complexes loaded cotton fabrics and the relationship between structure and properties were investigated.

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Acknowledgements

This work was supported by the Natural Science Foundation of Shaanxi Provincial Department of Education [grant number 19JK0362], Science and Technology Guidance Project of China National Textile and Apparel Council [grant number 2019040] and the PhD Research Funds of Xi’an Polytechnic University [grant number BS1721].

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Authors and Affiliations

  1. The Key Laboratory of Space Applied Physics and Chemistry, Ministry of Education and the Key Laboratory of Polymer Science and Technology, Shaanxi Province, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an, 710129, Shaanxi, China

    Jinshu Liu & Xiaoyan Ma

  2. College of Textile Science and Engineering, Xi’an Polytechnic University, Xi’an, 710048, Shaanxi, China

    Jinshu Liu, Wenzhao Shi & Jianwei Xing

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  1. Jinshu Liu
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  2. Xiaoyan Ma
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  4. Jianwei Xing
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Correspondence to Xiaoyan Ma.

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Liu, J., Ma, X., Shi, W. et al. Evaluation of Enhanced UV Protection Property of Dyed Cotton Fabrics Based on Inclusion Complex of β-cyclodextrin with Natural Coumarin Extracted from Cortex fraxini. Fibers Polym 22, 1569–1579 (2021). https://doi.org/10.1007/s12221-021-0445-8

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  • DOI: https://doi.org/10.1007/s12221-021-0445-8

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