Abstract
E-nose technology has been successfully employed in determination of rancidity in nutraceutical-rich drop cookies. The cookies were formulated with extracts obtained by supercritical carbon dioxide extractions and post-extraction sample matrices of black pepper and small cardamom. Rancidity in cookies was estimated by comparing the odor profiles of stored cookies with the profiles of deliberately rancid cookies (training sets), using e-nose. PCA plots along with spoilage indices obtained from Mahalanobis distances calculated from e-nose responses revealed that the extracts and post-extraction sample matrices of these spices performed as natural antioxidants in preventing rancidity in cookies. Both the extracts enhanced the shelf lives of cookies by at least 120 days; post-extraction matrices of black pepper and small cardamom enhanced the same by 80 and 40 days, respectively. These findings were further affirmed by biochemical analyses and linear regression equations were generated for prediction of FFA content, PV, and MDA values from the spoilage indices of each type of cookie. Thus, spoilage indices can circumvent the requirement of conducting cumbersome biochemical assays for estimation of rancidity in cookies. Similar applications of e-nose technology and spoilage indices can be envisaged for other bakery products also.
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References
Bhattacharya, N., Tudu, B., Jana, A., Ghosh, D., Bandhopadhyaya, R., & Saha, A. B. (2008). Illumination heating and physical raking for increasing sensitivity of electronic nose measurements with black tea. Sensors and Actuators B, 131, 37–42.
Chatterjee, D., Bhattacharjee, P., Lechat, H., Ayouni, F., & Vabre, V. (2012). Assessment of shelf-life of cookies formulated with clove extracts using electronic nose: estimation of rancidity in cookies. Proceedings of the 2012 Sixth International Conference on Sensing Technology, doi: 10.1109/ICSensT.2012.6461709 (pp. 404–409). Kolkata, ISBN 978–1–4673-2245-4.
Chatterjee, D., Bhattacharjee, P., Lechat, H., Ayouni, F., Vabre, V., & Bhattacharyya, N. (2014). Electronic nose setup for estimation of rancidity in cookies. In A. Mason, S. C. Mukhopadhyay, K. P. Jayasundera, & N. Bhattacharyya (Eds.), Sensing technology: current status and future trends II, smart sensors, measurement and instrumentation (pp. 1–27). Springer International Publishing: Switzerland.
Dutta, S., & Bhattacharjee, P. (2015). Enzyme-assisted supercritical carbon dioxide extraction of black pepper oleoresin for enhanced yield of piperine-rich extract. Journal of Bioscience and Bioengineering, 120, 17–23.
Dutta, S., & Bhattacharjee, P. (2016). Microencapsulation of enzyme-assisted supercritical carbon dioxide extract of small cardamom by spray drying. Journal of Food Measurement and Characterization. doi:10.1007/s11694-016-9398-9.
Gan, H. L., Tan, C. P., Che Man, Y. B., NorAini, I., & Nazimah, S. A. H. (2005). Monitoring the storage stability of RBD palm olein using the electronic nose. Food Chemistry, 89, 271–282.
Ghosh, S., Bhattacharjee, P., & Das, S. (2015). 1,8-Cineol-rich cardamom seed (Elettaria cardamomum) extracts using green technologies and conventional extractions: process analysis, phytochemical characterization, and food application. Separation Science and Technology, 50, 1974–1985.
Pratima, A., & Yadave, M. C. (2000). Effect of incorporation of liquid dairy by-product on chemical characteristic of soy fortified biscuits. Journal of Food Science and Technology, 37, 158–161.
Sakac, M. B., Gyura, J. F., Misan, A. C., Seres, Z. I., Pajin, B. S., & Soronja-Simovicm, D. M. (2010). Antioxidant activity of cookies supplemented with sugarbeet dietary fiber. Sugar Industry, 136, 151–157.
Vinaixa, M., Vergara, A., Duran, C., Llobet, E., Badia, C., Brezmes, J., Vilanova, X., & Correig, X. (2005). Fast detection of rancidity in potato crisps using e-noses based on mass spectrometry or gas sensors. Sensors and Actuators B, 106, 67–75.
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The authors acknowledge Department of Science & Technology, Government of West Bengal (WBDST), India [Grant number: 675(Sanc.)/ST/P/S&T/11G-1/2011)] and Spices Board, Cochin, Government of India, for providing financial supports for this study.
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Dutta, S., Bhattacharjee, P. & Bhattacharyya, N. Assessment of Shelf Lives of Black Pepper and Small Cardamom Cookies by Metal Oxide-Based Electronic Nose Using Spoilage Index. Food Bioprocess Technol 10, 2023–2033 (2017). https://doi.org/10.1007/s11947-017-1962-8
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DOI: https://doi.org/10.1007/s11947-017-1962-8