Skip to main content
Log in

Magnetizing roast and magnetic separation of iron in rare-earth tailings

  • Materials, Metallurgy, Chemical and Environmental Engineering
  • Published:
Journal of Central South University Aims and scope Submit manuscript

Abstract

Magnetic separation of iron in rare-earth tailings was achieved by magnetizing roast process with coal as reductant. Effects of the temperature, carbon to oxygen ratio, and cooling type on magnetic susceptibility and composition of rare-earth tailings were investigated. The results show that roast conditions with the temperature of 650 °C, carbon to oxygen ratio of 3.85, and holding time of 2.5 h are in favor of reduction of Fe2O3 to Fe3O4 when the roasted rare-earth tailings is cooled along with furnace. Under these roast conditions, magnetic susceptibility of rare-earth tailings is 2.36 that is very close to theoretical value (2.33). However, magnetic separation results of iron in rare-earth tailings cooled along with furnace are not satisfactory. Through comparing magnetic separation results of iron in rare-earth tailings cooled by different ways, it is found that water cooling is more favored of magnetic separation of iron in the roasted rare-earth tailings than furnace cooling and air cooling. Grade and recovery of iron in concentrate from rare-earth tailings cooled by water are 45.00%-49.00% and 65.00%-77.50%, respectively.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. JIU Shao-wu, XUE De-long, LI H, SONG Hai-xia, ZHANG L. An investigation into magnetization of siderite powder by roasting in suspension state [J]. Metal Mine, 2008, 386(8): 33–35. (in Chinese)

    Google Scholar 

  2. ZHANG Han-quan, YU Yong-fu, PENG Ze-you, CHEN W. Study on flash magnetizing roasting of Huangmei Limonitic ore [J]. Iron and Steel, 2009, 44(7): 11–14. (in Chinese)

    Google Scholar 

  3. LI Chao, DUN Heng-hu, BAI Jing, LI Long-tu. Innovative methodology for comprehensive utilization of iron ore tailings: Part 1. The recovery of iron from iron ore tailings using magnetic separation after magnetizing roasting [J]. Journal of Hazardous Materials, 2010, 174(1/2/3): 71–77.

    Article  Google Scholar 

  4. YANG Hui-fen, JING Li-li, ZHANG Bao-gang. Recovery of iron from vanadium tailings with coal-based direct reduction followed by magnetic separation [J]. Journal of Hazardous Materials, 2011, 185(2/3): 14.5-1411.

    Google Scholar 

  5. LEON Y S, CHANDRA V. A process for enhanced removal of iron from bauxite ores [J]. International Journal of Mineral Processing, 1991, 31(3/4): 233–246.

    Google Scholar 

  6. LI Mi, PENG Bing, CHAI Li-yuan, PENG Ning, YAN Huan, HOU Dong-ke. Recovery of iron from zinc leaching residue by selective reduction roasting with carbon [J]. Journal of Hazardous Materials, 2012, 237-238: 323–330.

    Article  Google Scholar 

  7. ZHANG Ya-li, LI Huai-mei, YU Xian-jin. Recovery of iron from cyanide tailings with reduction roasting–water leaching followed by magnetic separation [J]. Journal of Hazardous Materials, 2012, 213-214: 167–174.

    Article  Google Scholar 

  8. SUN Yong-sheng, HAN Yue-xin, Gao Peng, WANG Ze-hong, REN Duo-zhen. Recovery of iron from high phosphorus oolitic iron ore using coal-based reduction followed by magnetic separation [J]. International Journal of Minerals, Metallurgy, and Materials, 2013, 20(5): 411–419.

    Article  Google Scholar 

  9. YIN Jia-qing, LV Xue-wei, BAI Chen-guang, QIU Gui-bao, MA Shi-wei, XIE Bing. Dephosphorization of iron ore bearing high phosphorous by carbothermic reduction assisted with microwave and magnetic separation [J]. ISIJ International, 2012, 52(9): 1579–1584.

    Article  Google Scholar 

  10. WANG Cheng-hang, TONG X, SUN Ji-peng. Research on the magnetizing roasting and magnetic separation of an oolitic hematite ore [J]. Metal Mine, 2009(5): 57–59. (in Chinese)

    Google Scholar 

  11. YANG Dao-guo, GU Tian-long, ZHOU Huai-ying, ZENG Jian-min, JIANG Zheng-yi. Recovery of niobium from baogang tailings by carbochlorination [J]. Advanced Materials Research, 2011, 201-203: 1691–1698.

    Article  Google Scholar 

  12. ZHAO Rui-chao, ZHANG Bang-wen, LI Bao-wei. Experimental research on separation of iron from the flotation tailings of Bayun Obo rare-earth minerals [J]. Multipurpose Utilization of Mineral Resources, 2008, 4: 34–38. (in Chinese)

    Google Scholar 

  13. YANG He, RONG Yi, TANG Rong, XUE Xiang-xin, LI Yong. Recovery of iron from Baotou rare earth tailings by magnetizing roast [J]. Rare Metals, 2013, 32(6): 616–621.

    Article  Google Scholar 

  14. ZHANG Yong, MA Peng-qi, CHE Li-ping, QIAN Jian-biao, MA Yan-ping, REN Jun-huan. Study on rare earth flotation from Baogang tailings [J]. Chinese Rare Earths, 2010, 30(2): 93–96. (in Chinese)

    Google Scholar 

  15. ZHANG Li, CHEN Shu, XIONG Xiang-jun, YU Xian-wang, WANG Jun-jie. Directional migration behavior of cerium during sintering process of mischmetal doped cemented carbide [J]. Journal of Central South University of Technology, 2008, 15(1): 6–10.

    Article  Google Scholar 

  16. WANG Jian-ping, YU Ke-xu. Experimental study on gas curtain-assisted high gradient magnetic separation of iron tailing [J]. Multipurpose Utilization of Mineral Resources, 2012, 3: 38–41. (in Chinese)

    Google Scholar 

  17. ZhANG Li-qing, ZHAO Ling-yan, ZHOU Hua-feng, YUAN Ben-fu. Co-extraction of rare earth and iron from baogang tailings [J]. The Chinese Journal of Process Engineering, 2012, 12(2): 218–222. (in Chinese)

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to He Yang  (杨合).

Additional information

Foundation item: Project(2012CBA01205) supported by National Basic Research Program of China, Projects(50934004, 51274061) supported by the National Natural Science Foundation of China; Project(N110502002) supported by the Fundamental Research Funds for the Central Universities, China

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Yang, H., Rong, Y., Han, C. et al. Magnetizing roast and magnetic separation of iron in rare-earth tailings. J. Cent. South Univ. 23, 1899–1905 (2016). https://doi.org/10.1007/s11771-016-3245-3

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11771-016-3245-3

Key words

Navigation