Abstract
The NdFeB/Co multilayer films were prepared by magnetron sputtering. After that, the samples were annealed at 600 °C for 20 min. The surface morphology, phase structures and magnetic properties of Mo (50 nm)/[NdFeB (100 nm)/Co(y)]×10/Mo (50 nm) thin films were researched by AFM, XRD and VSM, respectively. The results show that the films show stronger perpendicular magnetic anisotropy. When the thickness of Co layers is 10 nm, the coercivity H c⊥ is the maximum, 295 kA/m. However, for y=10-20, the reduced remanence M/M s of films has increased. When the thickness of Co layers is 20-30 nm, the NdFeB/Co multilayer films obtained more superior magnetic properties with M/M s =0.95.
Similar content being viewed by others
References
KIM Y B, CHO S H, KIM H T, RYU K S, LEE S H, LEE K H, KAPUSTIN G A. Effects of buffer layer temperature on the magnetic properties of NdFeB thin film magnets [J]. Journal of Magnetism and Magnetic Materials, 2004, 272: E1917-E1919.
SERRONA L, FUJISAKI R, SUGIMURA A, OKUDA T, ADACHI N, OHSATO H, SAKAMOTO I, NAKANISHA A, MOTOKAWA M, PING D H, HONO K. Enhanced magnetic properties of Nd–Fe–B thin films crystallized by heat treatment [J]. Journal of Magnetism and Magnetic Materials, 2003, 260(3): 406–414.
CONSTANTINESCU C, PATROI E, CODESCU M, DINESCU M. Effect of nitrogen environment on NdFeB thin films grown by radio frequency plasma beam assisted pulsed laser deposition[J]. Materials Science and Engineering B, 2013, 178(4): 267–271.
KHOA T V, HA N D, HONG S M, JIN H M, KIM G W, HIEN T D, TAI L T, DUONG N P, LEE K E, KIM C G, KIN C O. Composition dependence of crystallization temperature and magnetic property of NdFeB thin films [J]. Journal of Magnetism and Magnetic Materials, 2006, 304(1): E246-E248.
JIANG Y, MASAOKA S, FUJITA T, UEHARA M, TOYONAGA T, FUJII K, HIGUCHII K, MAENAKA K. Fabrication of a vibration-driven electromagnetic energy harvester with integrated NdFeB/Ta multilayered micro-magnets [J]. Journal of Micromechanics and Microengineering, 2011, 21(9): 095014.
ARAKI T, NAKANISHI T, UMEMURA T. Texture of Nd-Fe-B thin films prepared by magnetron sputtering [J]. Journal of Applied Physics, 1999, 85(8): 4877–4879.
SERRONA L, SUGIMURA A, ADACHI N, OKUDA T, NAKANISHI A, MOTOKWA M, PING D H, HONO K. Structure and magnetic properties of high coercive NdFeB films with a perpendicular anisotropy [J]. Applied Physics Letters, 2003, 82(11): 1751–1753.
PARHOFER S M, WECKER J, KUHRT C, GIERES G, SCHULTZ L. Remanence enhancement due to exchange coupling in multilayers of hard-and softmagnetic phases [J]. Magnetics, IEEE Transactions on, 1996, 32(5): 4437–4439.
CONSTANTINESCU C, SCARISOREANU N, MOLDOVAN A, DINESCU M, PETRESCU L, EPUREANU G. Thin films of NdFeB deposited by PLD technique [J]. Applied Surface Science, 2007, 253(19): 8192–8196.
BROWN D, MA B M, CHEN Z. Developments in the processing and properties of NdFeB-type permanent magnets [J]. Journal of Magnetism and Magnetic Materials, 2002, 248(3): 432–440.
UEHARA M. Microstructure and permanent magnet properties of a perpendicular anisotropic NdFeB/Ta multilayered thin film prepared by magnetron sputtering [J]. Journal of Magnetism and Magnetic Materials, 2004, 284: 281–286.
MANAF A, BUCKLEY R A, DAVIES H A. New nanocrystalline high-remanence Nd-Fe-B alloys by rapid solidification [J]. Journal of Magnetism and Magnetic Materials, 1993, 128(3): 302–306.
CUI B, SUN X K, XIONG L Y, CUI B Z, SUN X K, XIONG L Y, LIU W, ZHANG L D, YANG Z Q, WANG A M, DENG J N. Effects of preparation processes on structure and magnetic properties of Nd2Fe14B/ α–Fe-type nanocomposite magnets [J]. Journal of Materials Research, 2001, 16(3): 709–715.
JIANG H, O’SHEA M J. Structure and magnetic properties of NdFeB thin films with Cr, Mo, Nb, Ta, Ti, and V buffer layers [J]. Journal of Magnetism and Magnetic Materials, 2000, 212(1): 59–68.
GUO Guang-wei, TANG Guang-ze, WANG Ya-jun, GUO G W, TANG G Z, WANG Y J, MA X X, WANG Y J. Composition design and properties of CoNdZr amorphous films deposited by unbalanced magnetron sputtering [J]. Journal of Central South University, 2009, 16: 719–724.
CUI B Z, O’SHEA M J. Hard magnetic properties of rapidly annealed NdFeB/Co films and intergrain interactions [J]. Journal of Magnetism and Magnetic Materials, 2004, 279(1): 27–35.
HIROSAWA S, MATSUURA Y, YAMAMOTO H, FUJIMURA S, SAGAWA M, TAMAUCHI H. Magnetization and magnetic anisotropy of R2Fe14B measured on single crystals [J]. Journal of Applied Physics, 1986, 59(3): 873–879.
SCHULTZ L, WECKER J, HELLSTERN E. Formation and properties of NdFeB prepared by mechanical alloying and solid-state reaction [J]. Journal of Applied Physics, 1987, 61(8): 3583–3585.
DAVIES H A. Nanocrystalline exchange-enhanced hard magnetic alloys [J]. Journal of Magnetism and Magnetic Materials, 1996, 157: 11–14.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Fu, Yd., Wang, Sy., Zhu, Xs. et al. Influence of modulated structure on magnetic properties of NdFeB/Co multilayer thin films. J. Cent. South Univ. 22, 3282–3286 (2015). https://doi.org/10.1007/s11771-015-2867-1
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11771-015-2867-1