Abstract
An automatic potentiometric setting dynamic pH titration method for the determination of sodium bicarbonate in compositions of smoke-type fireworks was developed. After wetting the sample with 0.1 mL ethanol, added 60 mL of deionized water for dissolution, ultrasound for 10 min, filtered and removed the insoluble matter, and then used a potentiometric titrator to drop 0.1 mol/L of hydrochloric acid. The experimental results showed that the limit of quantitation was 0.1%, the recoveries were 96.1–104.8% and the relative standard deviation was 0.56–3.11% when the sample weigh 0.2 g. The automatic potentiometric setting dynamic pH titration method is simple to operate and can accurately and quickly determine the content of sodium bicarbonate in compositions of smoke-type fireworks.
References
American Fireworks Standards Laboratory. Standards for Consumer Fireworks. http://www.afsl.org.cn/AFSLStd%202011%20CN%204.pdf. Accessed 26 Jun 2011
Barragan JC, Kubota LT (2016) Nanostructured cupric oxide electrode: an alternative to amperometric detection of carbohydrates in anion-exchange chromatography. Anal Chim Acta 906:89–97. https://doi.org/10.1016/j.aca.2015.11.051
Claire W (2019) Red, white, and boom? How fireworks came to America. National Geographic. https://www.nationalgeographic.com/culture/article/how-fireworks-came-to-america. Accessed 7 Jul 2019
Foulon C, Giulio PD, Lecoeur M (2018) Simultaneous determination of inorganic anions and cations by supercritical fluid chromatography using evaporative light scattering detection. J Chromatogr A 1534:139–149. https://doi.org/10.1016/j.chroma.2017.12.047
Gao H, Wang ST, Hu F, Shen BB, Sun MF, Wang HB, Li L, Fang WJ (2022) Investigation of an uncommon artifact during reducing capillary electrophoresis-sodium dodecyl sulfate analysis of a monoclonal antibody with dynamic light scattering and reversed-phase high-performance liquid chromatography. Pharm Res 39:1959–1968. https://doi.org/10.1007/s11095-022-03303-0
General Administration of Quality Supervision, Inspection and Quarantine of the People’s Republic of China (2012) Determination of essential parameters of chemical raw materials for use in fireworks and firecrackers-part 9: sodium hydrogen carbonate: SN/T 3056.9–2011. China Standards Press, Beijing
General Administration of Quality Supervision, Inspection and Quarantine, National Standardization Administration of the People’s Republic of China (2017) Guidelines for the confirmation and validation of chemical analysis methods for conformity assessment: GB/T 27417–2017. China Standards Press, Beijing
Huang TT (2023) Hunan's export of fireworks and firecrackers reached a historic high of over 4.7 billion yuan, mainly exported to the Americas, Europe, Southeast Asia, and other regions, with the United States being the largest export market. Tencent. https://new.qq.com/rain/a/20230120A07K7A00. Accessed 20 Jan 2023
Li Q, Yu YJ, Wang FF, Chen SW, Yin Y, Lin HP, Che F, Sun P, Qin J, Liu J, Wang HM (2014) Urinary perchlorate exposure and risk in women of reproductive age in a fireworks production area of China. Arch Environ Contam Toxicol 67:42–49. https://doi.org/10.1007/s00244-014-0042-6
Meloun M, Pfeiferova A, Javurek M, Pekarek T (2020) Determination of acid dissociation constants, enthalpy, entropy and Gibbs free energy of the baricitinib by the UV-metric and pH-metric analysis. J Pharm Biomed Anal 191:113532. https://doi.org/10.1016/j.jpba.2020.113532
Nayak AK, Rahman MM, Naidu R, Dhal B, Swain CK, Nayak AD, Tripathi R, Shahid M, Islam MR, Pathak H (2019) Current and emerging methodologies for estimating carbon sequestration in agricultural soils: a review. Sci Total Environ 665:890–912. https://doi.org/10.1016/j.scitotenv.2019.02.125
Nogueira SA, Lemes AD, Chagas AC, Vieira ML, Talhavini M, Morais PO, Coltro WT (2019) Redox titration on foldable paper-based analytical devices for the visual determination of alcohol content in whiskey samples. Talanta 194:363–369. https://doi.org/10.1016/j.talanta.2018.10.036
Nonomura M (2022) Determination of carbon dioxide and acid components in exhaust gas by suppressed ion chromatography. Anal Sci 20:219–222. https://doi.org/10.2116/analsci.20.219
Pohl P, Welna M, Madeja AS, Greda K, Jamroz P, Dzimitrowicz A (2022) Response surface methodology assisted development of a simplified sample preparation procedure for the multielement (Ba, Ca, Cu, Fe, K, Mg, Mn, Na, Sr and Zn) analysis of different coffee brews by means of inductively coupled plasma optical emission spectrometry. Talanta 241:123215. https://doi.org/10.1016/j.talanta.2022.123215
Singh VK, Bikundia DS, Sarswat A, Mohan D (2012) Groundwater quality assessment in the village of Lutfullapur Nawada, Loni, District Ghaziabad, Uttar Pradesh, India. Environ Monit Assess 184:4473–4488. https://doi.org/10.1007/s10661-011-2279-0
Zhang WP, Yang J (2017) Food trial design and statistical analysis, 3rd edn. China Agricultural University, Beijing, pp 471–472
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This work was supported by the Science and Technology Project of the General Administration of Customs, People’s Republic of China (2021HK230).
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Zhang, Ly., Liu, Jg., Han, Y. et al. Determination of sodium bicarbonate in compositions of smoke-type fireworks based on automatic potentiometric setting dynamic pH titration method. Chem. Pap. 78, 645–650 (2024). https://doi.org/10.1007/s11696-023-03099-2
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DOI: https://doi.org/10.1007/s11696-023-03099-2