Abstract
Synchronous fluorescence spectrum coupled with multivariate curve resolution alternating least square (MCR-ALS) and artificial neural network (ANN) has been used for the analysis of edible vegetable oil. Four types of edible vegetable oil extracted from seed were stored at 65 °C for 0, 1, 5, 9, 13 and 17 days under control conditions. Synchronous fluorescence spectra were obtained for each sample in the excitation wavelength range of 200–800 nm with offsets (Δλ) of 10, 20, 30, 40, 50, 60, 70, 80, 90, 100, 110, 120, 130, 140, 150, 160, 170 and 180 nm between emission and excitation wavelengths. The relationship between excitation emission matrix data and peroxide value were analyzed using ANN and MCR-ALS algorithms. The regression results indicated that a rapid method for oil freshness evaluation was developed with correlation coefficient for train set and test set of 1 and 0.96, respectively.
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References
Aladedunye F (2016) Toxic contaminants of thermo-oxidatively processed edible oils/fats. Lipid Technol 28:117–121
Andersen CM, Bro R (2003) Practical aspects of PARAFAC modeling of fluorescence excitation-emission data. J Chemom 17:200–215
Bro R (1997) PARAFAC. Tutorial and applications. Chemom Intell Lab Syst 38:149–171
Cao J, Li H, Xia X et al (2015) Effect of fatty acid and tocopherol on oxidative stability of vegetable oils with limited air. Int J Food Prop 18:808–820
Cheng P, Wang Y, Chen Z et al (2016) Identification and determination of oil pollutants based on 3-D fluorescence spectrum combined with self-weighted alternating trilinear decomposition algorithm. J Opt Soc Korea 20:204–211
Douny C, Tihon A, Bayonnet P et al (2015) Validation of the analytical procedure for the determination of malondialdehyde and three other aldehydes in vegetable oil using liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS) and application to linseed oil. Food Anal Methods 8:1425–1435
Guo L, Xie MY, Yan AP et al (2006) Simultaneous determination of five synthetic antioxidants in edible vegetable oil by GC-MS. Anal Bioanal Chem 386:1881–1887
Jin H, Hwang SJ, Shin JK (2008) Using synchronous fluorescence technique as a water quality monitoring tool for an urban river. Water Air Soil Pollut 191:231–243
Kumar K, Mishra A (2012) Application of parallel factor analysis to total synchronous fluorescence spectrum of dilute multifluorophoric solutions: addressing the issue of lack of trilinearity in total synchronous fluorescence data set. Analyt Chim Acta 755:37–45
Li XQ, Ji C, Sun YY et al (2009) Analysis of synthetic antioxidants and preservatives in edible vegetable oil by HPLC/TOF-MS. Food Chem 113:692–700
Matsunami H, Montmayeur JP, Buck LB (2000) A family of candidate taste receptors in human and mouse. Nature 404:601–604
Sahar A, Boubellouta T, Portanguen S et al (2009) Synchronous front-face fluorescence spectroscopy coupled with parallel factors (PARAFAC) analysis to study the effects of cooking time on meat. J Food Sci 74:E534
Sayago A, Morales MT, Aparicio R (2004) Detection of hazelnut oil in virgin olive oil by a spectrofluorimetric method. Eur Food Res Technol 218:480–483
Stedmon CA, Bro R (2008) Characterizing dissolved organic matter fluorescence with parallel factor analysis: a tutorial. Limnol Oceanogr Methods 6:572–579
Wan NRWI, Ramli ZAC, Ismail M (2015) Recovery and purification of crude glycerol from vegetable oil transesterification. Sep Purif Rev 44:250–267
Wang JY, Wu HL, Sun YM et al (2014) Simultaneous determination of phenolic antioxidants in edible vegetable oils by HPLC-FLD assisted with second-order calibration based on ATLD algorithm. J Chromatogr B Analyt Technol Biomed Life Sci 947–948:32–40
Wu PG, Yang DJ, Zhang L et al (2012) Simultaneous determination of 17 phthalate esters in edible vegetable oils by GC-MS with silica/PSA-mixed solid-phase extraction. J Sep Sci 35:2932–2939
Zhang C, Bailey DP, Suslick KS (2006) Colorimetric sensor arrays for the analysis of beers: a feasibility study. J Agric Food Chem 54:4925–4931
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This study was sponsored by National Natural Science Foundation of China (31701685); Anhui Postdoctoral Science Foundation (2017B218); Anhui Postdoctoral Science (Chuzhou university) Foundation (2018bsh001).
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Gu, H., Sun, Y. & Lv, R. A feasibility study for rapid evaluation of oil quality undergoing oven treatment using synchronous fluorescence spectrum. Chem. Pap. 73, 1953–1959 (2019). https://doi.org/10.1007/s11696-019-00748-3
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DOI: https://doi.org/10.1007/s11696-019-00748-3