Abstract
The present work indicated that both the microstructure morphology and occupation of the selective laser melting processed Ti-6Al-4V exhibited regular transformation as the sampling height varied. In turn, the mechanical performance changed accordingly. Due to the great temperature gradient, the microstructure mainly consisted of martensite α′. Additionally, as the sampling heights increased, the microstructure transformed as the following rule: coarse lamellar α′—fine articular α′—ultrafine Z-zigzag α′. Close examination indicated that the martensite phase can be further distinguished into primary α′, secondary α ′, tertiary α′ and quartic α′ based on the size and the generating location. With the sampling height increased, both the size and volume occupation of tertiary and quartic α′ decreased. The generation and transformation of the tertiary α′ and quartic α′ were significantly affected by the thermal cycle intensity and times. Correspondingly, the tensile strength increased slightly as the sampling height increased.
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L.E. Murr, S.A. Quinones, S.M. Gaytan, M.I. Lopez, A. Rodela, E.Y. Martinez, D.H. Hernandez, E. Martinez, F. Medina and R.B. Wicker, Microstructure and Mechanical Behavior of Ti–6Al–4V Produced by Rapid-Layer Manufacturing, for Biomedical Applications, J. Mech. Behav. Biomed. Mater., 2009, 2(1), p 20–32.
I. Gurrappa, Characterization of Titanium Alloy Ti-6Al-4V for Chemical, Marine and Industrial Applications, Mater. Charact., 2003, 51(2–3), p 131–139.
I. Yadroitsev, P. Krakhmalev and I. Yadroitsava, Selective Laser Melting of Ti6Al4V Alloy for Biomedical Applications: Temperature Monitoring and Microstructural Evolution, J. Alloy. Compd., 2014, 583, p 404–409.
A. Hasçalık and U. Çaydaş, Electrical Discharge Machining of Titanium Alloy (Ti–6Al–4V), Appl. Surf. Sci., 2007, 253(22), p 9007–9016.
E.O. Ezugwu, J. Bonney, R.B. Da Silva and O. Cakir, Surface Integrity of Finished Turned Ti–6Al–4V Alloy with PCD Tools Using Conventional and High Pressure Coolant Supplies, Int. J. Mach. Tools Manuf, 2007, 47(6), p 884–891.
A. Ataee, Y. Li, M. Brandt and C. Wen, Ultrahigh-Strength Titanium Gyroid Scaffolds Manufactured by Selective Laser Melting (SLM) for Bone Implant Applications, Acta Mater., 2018, 158, p 354–368.
L.C. Zhang and H. Attar, Selective Laser Melting of Titanium Alloys and Titanium Matrix Composites for Biomedical Applications: a Review, Adv. Eng. Mater., 2016, 18(4), p 463–475.
L.C. Zhang, H. Attar, M. Calin and J. Eckert, Review on Manufacture by Selective Laser Melting and Properties of Titanium Based Materials for Biomedical Applications, Mater. Technol., 2016, 31(2), p 66–76.
D. Jafari and W.W. Wits, The Utilization of Selective Laser Melting Technology on Heat Transfer Devices for Thermal Energy Conversion Applications: A Review, Renew. Sustain. Energy Rev., 2018, 91, p 420–442.
R. Mahshid, H.N. Hansen and K.L. Højbjerre, Strength Analysis and Modeling of Cellular Lattice Structures Manufactured Using Selective Laser Melting for Tooling Applications, Mater. Des., 2016, 104, p 276–283.
<1-s2.0-S0022024801014245-main.pdf>,
A. Bhattacharjee, B. Saha and J.C. Williams, Titanium Alloys: Part 1—Physical Metallurgy and Processing, Springer, Aerospace Materials and Material Technologiesed., 2017, p 91–115
M. Frkan, R. Konecna, G. Nicoletto and L. Kunz, Microstructure and Fatigue Performance of SLM-Fabricated Ti6Al4V Alloy After Different Stress-Relief Heat Treatments, Transportation Research Procedia, 2019, 40, p 24–29.
D. Agius, K.I. Kourousis, C. Wallbrink and T. Song, Cyclic Plasticity and Microstructure of as-Built SLM Ti-6Al-4V: The Effect of Build Orientation, Mater. Sci. Eng., A, 2017, 701, p 85–100.
W. Xu, E.W. Lui, A. Pateras, M. Qian and M. Brandt, In Situ Tailoring Microstructure in Additively Manufactured Ti-6Al-4V for Superior Mechanical Performance, Acta Mater., 2017, 125, p 390–400.
J. Yang, H. Yang, H. Yu, Z. Wang, H. Wang and X. Zeng, A Novel Approach to In-situ Fabricate Ti-6Al-4V Alloy With Graded Microstructure and Property by Selective Laser Melting, Mater. Lett., 2018, 215, p 246–249.
J. Sun, X. Zhu, L. Qiu, F. Wang, Y. Yang and L. Guo, The Microstructure Transformation of Selective Laser Melted Ti-6Al-4V Alloy, Materials Today Communications, 2019, 19, p 277–285.
T. Vilaro, C. Colin and J.-D. Bartout, As-fabricated and Heat-Treated Microstructures of the Ti-6Al-4V Alloy Processed by Selective Laser Melting, Metall. and Mater. Trans. A., 2011, 42(10), p 3190–3199.
L. Thijs, F. Verhaeghe, T. Craeghs, J. Van Humbeeck and J.-P. Kruth, A Study of the Microstructural Evolution During Selective Laser Melting of Ti–6Al–4V, Acta Mater., 2010, 58(9), p 3303–3312.
J. Lin, Y. Lv, Y. Liu, Z. Sun, K. Wang, Z. Li, Y. Wu and B. Xu, Microstructural Evolution and Mechanical Property of Ti-6Al-4V Wall Deposited by Continuous Plasma Arc Additive Manufacturing Without Post Heat Treatment, J. Mech. Behav. Biomed. Mater., 2017, 69, p 19–29.
J. Yang, H. Yu, J. Yin, M. Gao, Z. Wang and X. Zeng, Formation and Control of Martensite in Ti-6Al-4V Alloy Produced by Selective Laser Melting, Mater. Des., 2016, 108, p 308–318.
A. Di Schino and J. Kenny, Grain Refinement Strengthening of a Micro-Crystalline High Nitrogen Austenitic Stainless Steel, Mater. Lett., 2003, 57(12), p 1830–1834.
F. Yin, G.J. Cheng, R. Xu, K. Zhao, Q. Li, J. Jian, S. Hu, S. Sun, L. An and Q. Han, Ultrastrong Nanocrystalline Stainless Steel and Its Hall-Petch Relationship in the Nanoscale, Scr. Mater., 2018, 155, p 26–31.
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Sun, J., Zhang, C., Wang, X. et al. The Microstructure Transformation and Mechanical Properties in Selective Laser Melting Processed Ti-6Al-4V at Different Heights. J. of Materi Eng and Perform 30, 9237–9244 (2021). https://doi.org/10.1007/s11665-021-06106-3
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DOI: https://doi.org/10.1007/s11665-021-06106-3