Skip to main content
Log in

Influence of Different Thermo-mechanical Cycling Routes on Recovery Stresses of Annealed NiTi Wires

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

In this study, the influence of different thermo-mechanical cycling routes on recovery stresses of annealed NiTi wires has been investigated by using a dynamic mechanical analyzer. The as-received wire was annealed in Argon atmosphere in the temperature range of 350 to 900 °C. Differential scanning calorimeter was used to study the martensite transformation. In route I, the sample is deformed to 2% pre-strain and recovery stress is measured after unloading. In route II, the sample undergoes 3% deformation followed by a free shape recovery and then is reloaded to 2% pre-strain and recovery stress is measured after unloading. In route III, the sample undergoes a constrained thermal cycling at 3% pre-strain followed by a free shape recovery and then recovery stress is measured at 2% pre-strain. The results show that both route II and III can improve the recovery stresses. Route III has higher recovery stresses than route II for samples annealed at 550-700 °C. The improvements of recovery stresses under route II and III are partly attributed to the decrease of A s temperatures after thermo-mechanical cycling. Such information is essential for the proper use of NiTi alloys in smart structures, intelligent controllers, and memory devices.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8

Similar content being viewed by others

References

  1. J. Van Humbeeck, Non-medical Application of Shape Memory Alloys, Mater. Sci. Eng. A, 1999, 273–275, p 134–138

    Article  Google Scholar 

  2. K. Otsuka and X. Ren, Recent Developments in the Research of Shape Memory Alloys, Intermetallics, 1999, 7, p 511–528

    Article  Google Scholar 

  3. D.A. Miller and D.C. Lagoudas, Influence of Cold Work and Heat Treatment on the Shape Memory Effect and Plastic Strain Development of NiTi, Mater. Sci. Eng. A, 2001, 308, p 161–175

    Article  Google Scholar 

  4. Y. Liu and S.P. Galvin, Criteria for Pseudoelasticity in Near-Equiatiomic NiTi Shape Memory Alloys, Acta Mater., 1997, 45(11), p 4431–4439

    Article  Google Scholar 

  5. X. Huang and Y. Liu, Effect of Annealing on the Transformation Behavior and Superelasticity of NiTi Shape Memory Alloy, Scr. Mater., 2001, 45, p 153–160

    Article  Google Scholar 

  6. P. Sittner, Y. Liu, and V. Novak, On the Origin of Lüders-Like Deformation of NiTi Shape Memory Alloy, J. Mech. Phys. Solids, 2005, 53, p 1719–1746

    Article  Google Scholar 

  7. J. Van Humbeeck, Damping Capacity of Thermoelastic Martensite in Shape Memory Alloys, J. Alloys Compd., 2003, 355, p 58–64

    Article  Google Scholar 

  8. Y. Liu, J. Van Humbeeck, R. Stalmans, and L. Delaey, Some Aspects of the Properties of NiTi Shape Memory Alloy, J. Alloys Compd., 1997, 247, p 115–121

    Article  Google Scholar 

  9. Y. Liu and P.G. McCormick, Thermodynamic Analysis of the Martensitic Transformation in NiTi-I: Effect of Heat Treatment on Transformation Behavior, Acta Metall. Mater., 1994, 42(7), p 2401–2406

    Article  Google Scholar 

  10. Y. Liu and P.G. McCormick, Thermodynamic Analysis of the Martensitic Transformation in NiTi-II: Effect of Transformation Cycling, Acta Metall. Mater., 1994, 42(7), p 2401–2406

    Article  Google Scholar 

  11. Y. Liu, Z.L. Xie, J. Van Humbeeck, and L. Delaey, Effect of Texture Orientation on the Martensite Deformation of NiTi Shape Memory Alloy Sheet, Acta Mater., 1999, 47(2), p 645–660

    Article  Google Scholar 

  12. P. Sittner, D. Neov, P. Lukas, and D.M. Toebbens, Neutron Diffraction Studies of the Stress Effect on Texture Transformations in NiTi Shape Memory Alloys, J. Neutron Res., 2004, 12(1–3), p 15–20

    Article  Google Scholar 

  13. P. Šittner, D. Vokoun, and G.N. Dayananda, Recovery Stress Generation in Shape Memory Ti50Ni45Cu5 Thin Wires, Mater. Sci. Eng. A, 2000, 286, p 298–311

    Article  Google Scholar 

  14. P. Šittner, P. Lukas, V. Novak, D. Neov, and M. Ceretti, In Situ Neutron Diffraction Study of Stresses Generated by Shape Memory Alloys, J. Neutron Res., 2001, 9, p 143–150

    Article  Google Scholar 

  15. D. Vokoun, V. Kafka, and C.T. Hu, Recovery Stresses Generated by NiTi Shape Memory Wires Under Different Constraint Conditions, Smart Mater. Struct., 2003, 12, p 680–685

    Article  Google Scholar 

  16. W. Cai, C.S. Zhang, and L.C. Zhao, Recovery Stress in a Ni-Ti-Nb Shape Memory Alloy with Wide Transformation Hysteresis, J. Mater. Sci. Technol., 1994, 10, p 27–30

    Article  Google Scholar 

  17. W. Cai, C.S. Zhang, and L.C. Zhao, Recovery Stress of Ni-Ti-Nb Wide-Hysteresis Shape Memory Alloy Under Constant Strain and Thermomechanical Cycling, J. Mater. Sci. Lett., 1994, 13, p 8–9

    Article  Google Scholar 

  18. V. Brailovski, E. Clément, P. Terriault, and F. Trochu, Influence of Stress Concentration on the Recovery Stress Generation, J. Phys. IV France, 2003, 112, p 231–234

    Article  Google Scholar 

  19. X.J. Yan and J. Van Humbeeck, Influence of Annealing on Recovery Stress of Cold-Worked NiTi Wire, Funct. Mater. Lett., 2009, 2, p 1–6

    Article  Google Scholar 

  20. H. Sadiq, M.B. Wong, R. Al-Mahaidi, and X.L. Zhao, The Effects of Heat Treatment on the Recovery Stresses of Shape Memory Alloys, Smart Mater. Struct., 2010, 19, p 1–7

    Article  Google Scholar 

  21. K.A. Tsoi, J. Schrooten, and R. Stalmans, Part I. Thermomechanical Characteristics of Shape Memory Alloys, Mater. Sci. Eng. A, 2004, 368, p 286–298

    Article  Google Scholar 

  22. K.A. Tsoi, J. Schrooten, and R. Stalmans, Part II. Thermomechanical Characteristics of Shape Memory Alloys, Mater. Sci. Eng. A, 2004, 368, p 299–310

    Article  Google Scholar 

  23. J. Schrooten, K.A. Tsoi, R. Stalmans, Y.J. Zheng, P. Sittner, Comparison Between Generation of Recovery Stresses in Shape Memory Wires and Composites: Theory and Reality, Proc. SPIE-4234, 2001, p 114–124

  24. Y.J. Zheng, J. Schrooten, L.S. Cui, and J. Van Humbeeck, Constrained Thermoelastic Martensitic Transformation Studied by Modulated DSC, Acta Mater., 2003, 51, p 5467–5475

    Article  Google Scholar 

  25. K.A. Tsoi, R. Stalmans, and J. Schrooten, Transformational Behavior of Constrained Shape Memory Alloys, Acta Mater., 2002, 50, p 3535–3544

    Article  Google Scholar 

  26. D.Q. Jiang, L.S. Cui, Y.J. Yan, X.Q. Zhao, and Y. Li, Constrained Martensitic Transformation in an In Situ Lamella TiNi/NbTi Shape Memory Composite, Mater. Sci. Eng. A, 2009, 515, p 131–133

    Article  Google Scholar 

  27. Y. Li, L.S. Cui, H.B. Xu, and D.Z. Yang, Constrained Phase-Transformation of a TiNi Shape Memory Alloy, Metall. Trans. A, 2003, 34, p 219–223

    Article  Google Scholar 

  28. X.J. Yan, Y.L. Ge, and J. Van Humbeeck, Influence of Annealing on the Stress-Assisted Two-Way Memory Effect in Cold-Worked NiTi Wire, Adv. Eng. Mater., 2015, 17(2), p 162–166

    Article  Google Scholar 

  29. X.J. Yan and J. Van Humbeeck, Temperature and Time Dependence on Recovery Stress Relaxation in Nickel Titanium Wire During Isothermal Holding at High Temperatures, Strain, 2013, 49(5), p 451–455

    Article  Google Scholar 

  30. X.J. Yan and J. Van Humbeeck, Evolution of Recovery Stress and Recovery Strain in Annealed NiTi Thin Wire During Constrained Thermal Cycling to High Temperature, Adv. Eng. Mater., 2014, 16(1), p 80–84

    Article  Google Scholar 

  31. X.J. Yan and J. Van Humbeeck, Effect of Annealing on Martensite Stabilization Due to Deformation Via Cooling Under Stress in Cold-Worked NiTi Thin Wire, Mater. Sci. Eng. A, 2012, 558, p 737–741

    Article  Google Scholar 

  32. X.J. Yan, J. Van Humbeeck, Effect of Annealing on Strain-Temperature Response Under Constant Tensile Stress in Cold-Worked NiTi Wire, Smart Mater. Res., 2011, 2011, Article ID 160927

  33. X.J. Yan and J. Van Humbeeck, Influence of Pre-strain on Recovery Stress of Annealed NiTi Thin Wire During Isothermal Holding, J. Alloys Comp., 2011, 509(3), p 1001–1006

    Article  Google Scholar 

  34. K.L. Kyo, R.O. Doná, and O. Jorge, Influence of Thermomechanical Processing on the Martensitic Transformation Temperatures of NiTi SMA Wire, Mater. Sci. Forum, 2010, 643, p 43–48

    Article  Google Scholar 

Download references

Acknowledgments

We gratefully acknowledge the support of the Natural Science Foundation of Liaoning Province of China under Grant No. 2015020224 and the ESF-Grant Mafesha, No. G-0652.05.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to X. J. Yan.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Yan, X.J., Ge, Y.L. & Van Humbeeck, J. Influence of Different Thermo-mechanical Cycling Routes on Recovery Stresses of Annealed NiTi Wires. J. of Materi Eng and Perform 25, 267–273 (2016). https://doi.org/10.1007/s11665-015-1833-2

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-015-1833-2

Keywords

Navigation