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Effect of P–Si Binary System on the Formation Mechanism of AZ91D MAO Coating

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Abstract

To enhance the corrosion resistance of magnesium alloy while improving its surface roughness to enhance organic bonding, the single pulse micro-arc oxidation treatment was conducted on magnesium alloy specimens for a duration of 1200 seconds. The treatment employed a mixed electrolyte of Na3PO4/Na2SiO3 with varying proportions, aiming primarily to investigate the treatment mechanism. Voltage–time response curves were recorded throughout the entire process. Characterization of the bioceramic films was achieved through the application of SEM, XRD, and XPS techniques, elucidating phase formation, surface morphologies, elemental distribution, and chemical valence. Subsequently, measurements were taken to assess the porosity of the film layer, alterations in thickness, roughness, and the kinetic potential polarization curves. The experimental findings reveal that P and Si elements influence the performance of AZ91D MAO coating by affecting cascading discharge and channel blockage. When the concentration ratio of PO43−/SiO32− in the mixed electrolyte reached 0.02 mol L−1/0.08 mol L−1, the icorr of MAO coating measured 4.6391 μA cm−2, indicating better corrosion resistance.

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Acknowledgments

We are grateful for the financial support from the Fundamental Research Funds for the Central Universities of China (Grant No. 2022CDJQY-014), 2022 Jiangsu Provincial Science and technology plan special fund BE2022110 (key research and development plan, industry prospect and key core technology), the China Postdoctoral Science Foundation (Grant No. 2021M700569) and Chongqing Postdoctoral Science Foundation (Grant No. cstc2021jcyj-bshX0087).

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Authors and Affiliations

  1. State Key Laboratory of Mechanical Transmissions, College of Materials Science and Engineering, Chongqing University, Chongqing, 400044, P.R. China

    Yuhui Zhang, Guangyin Liu, Xiaoping Li, Dajun Zhai, Qin Tang, Shiqi Chen, Hanbing Li & Jun Shen

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  1. Yuhui Zhang
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Zhang, Y., Liu, G., Li, X. et al. Effect of P–Si Binary System on the Formation Mechanism of AZ91D MAO Coating. Metall Mater Trans A 55, 1229–1242 (2024). https://doi.org/10.1007/s11661-024-07322-x

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