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Hot-Working Characteristics and Dynamic Recrystallization Behavior of Hot Isostatically Pressed FGH4096 Superalloy

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Abstract

Hot-working characteristics, microstructure evolution, and dynamic recrystallization (DRX) of hot isostatically pressed (HIPed) FGH4096 superalloy compressed at the temperature range of 1040 °C to 1130 °C and strain rate range of 0.01 to 10 s−1 were studied. Based on the flow stress curves obtained by friction–temperature correction, a new constitutive equation has been established to predict the flow stresses under different deformation conditions accurately. Also, the hot working maps under different strains were established to optimize the hot working parameters. Different recrystallization behaviors dominate in different hot working regions, and the DRX behavior is sensitive to deformation temperature rather than strain rate. Both continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) are activated for HIPed FGH4096 superalloy under low deformation temperature, while the DDRX dominates under high deformation temperature. The adiabatic shear bands, voids, and cracks along grain boundaries are the main factors of flow instability in the instability regions. The optimized hot working window of T = 1080 °C to 1107 °C and \( \dot{\varepsilon } \) = 10−0.2 to 10−1.3 s−1 was obtained by combining the hot working map and microstructure evolution.

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Acknowledgments

This study was supported by Yantai high-end talent introduction “Double Hundred Plan” (2021), Taishan Scholars Program of Shandong Province (2021), Talent Training Program for Shandong Province Higher Educational Youth Innovative Teams (2019), National Science and Technology Major Project of China (J2019-VI-0023-0140), Natural Science Foundation of Shandong Province (ZR2019MEM012), Major Scientific and Technological Innovation Project in Shandong Province (2019JZZY010325), Science Foundation Program for Distinguished Young Scholars of Shandong (Overseas) (2022HWYQ-084), and Graduate Innovation Foundation of Yantai University (2022).

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  1. Institute for Advanced Studies in Precision Materials, Yantai University, Yantai, 264005, P.R. China

    Wei Liu, Hua Zhang, Zhiling Liu, Jingjing Ruan, Hailiang Huang, Xin Zhou, Lilong Zhu, Shangzhou Zhang & Liang Jiang

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  1. Wei Liu
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Liu, W., Zhang, H., Liu, Z. et al. Hot-Working Characteristics and Dynamic Recrystallization Behavior of Hot Isostatically Pressed FGH4096 Superalloy. Metall Mater Trans A 54, 962–982 (2023). https://doi.org/10.1007/s11661-022-06951-4

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