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The Synthesis of Silicon Carbide in Rhombohedral Form with Different Chemicals

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Abstract

This study describes the attempt at producing silicon carbide using a simpler and less costly method. Within the study, XRD, EDX, and FTIR analyses were performed to determine the structural properties of the product, and SEM analyses were used to identify its surface properties. The characteristics such as porosity and surface area were determined through BET analysis. The starting reagents were compared with the product using FTIR analysis, whereas the product was compared with a sample of SiC procured from a supplier who manufactures high-purity products through BET analysis. In EDX analysis, approximately 72 pct Si and 28 pct C were identified. The vibrational peaks of the synthesized product (characteristics Si-C bonds) were observed at around 1076 cm−1 (FTIR analysis). At the same time, the outcomes were compared with major publications in the literature.

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References

  1. Y. Yang, Z.M. Lin and Li J.T: J Eur Ceram Soc 2009, vol. 9, pp. 175–80.

    Article  Google Scholar 

  2. B. Elyassi, T.W. Kim and Sahimi M: Mater Chem Phys 2009, vol. 118, pp. 259–63.

    Article  Google Scholar 

  3. H.B. Jin, J.T. Li, M.S. Cao and Agathopoulos S:. PowderTechnol 2009, vol. 196, pp. 229–32.

    Article  Google Scholar 

  4. Y. Goldberg, M.E. Levinshtein and Rumyantsev S.L. In:Properties of Advanced Semiconductor Materials GaN, AlN, SiC, BN, SiC, SiGe. Levinshtein M.E., Rumyantsev S.L., Shur M.S. (Eds), Wiley, New York, 2001, pp. 93-148.

    Google Scholar 

  5. S.E. Saddow: Silicon Carbide Biotechnology a Biocompatible Semiconductor for Advanced Biomedical Devices and Applications. First Edition, Elsevier, Waltham, USA, 2012, pp. 122-124.

    Google Scholar 

  6. A.S. Gusev, S.M. Ryndya, A.V. Zenkevich, N.I. Kargin, D.V. Averyanov and Grekov M.M.: Mod. Electron. Mater. 2015, vol. 1, pp. 120-125.

    Article  Google Scholar 

  7. X. Luo, W. Ma, Y. Zhou, D. Liu, B. Yang and Dai Y: Nano Scale Res Lett; 2010, vol. 5, pp. 252–6.

    Article  Google Scholar 

  8. W.M. Zhou, Y.F. Zhang, X.M. Niu and Min G.Q: Lecture Notes in Nanoscale Science and Technology, 3, Springer, New York, 2008, p. 17.

  9. H.J. Chio, H.K. Seong, J.C. Lee and Sung Y.M: J. Cryst. Growth 2004, vol. 269, pp. 472–8

    Article  Google Scholar 

  10. G.W. Ho, S.W. Wong, D.J. Kang and Welland M.E: Nanotechnology 2004, vol. 15, pp. 996–9

    Article  Google Scholar 

  11. H.J. Li, Z.J. Li, A.L. Meng, K.Z. Li, X.N. Zhang, Xu Y.P: J. Alloys Compd. 2003, vol. 352, pp. 279–82

    Article  Google Scholar 

  12. Y.J. Zhang, N.L. Wang, R.R. He, X.H. Chen and Zhu J: Solid State Commun. 2001, vol. 118, pp. 595–8

    Article  Google Scholar 

  13. BS Yigezu, MM Mahapatra, PK Jha: J. Miner. Mater. Charact. Eng. 2013, vol. 1, pp. 124-30.

    Google Scholar 

  14. G. Treffer, J. Neuhiiuser and Marx G: Mikrochim. Acta 125 (1997) 325-330

    Article  Google Scholar 

  15. B.M. Moshtaghioun, R. Poyato, F.L. Cumbrera, S. de Bernardi-Martin, A. Monshi, M.H. Abbasi, F. Karimzadeh and Dominguez-Rodriguez A: J. Europ. Ceramic Soc. 2012, vol. 32, 1787–94

    Article  Google Scholar 

  16. J. Hong, A. Goullet and Turban G: Thin Solid Films 2000, vol. 364, pp. 144−149.

    Article  Google Scholar 

  17. Y. Nur, H.M. Cengiz, M.W. Pitcher and Toppare L.K.: J. Mater. Sci. 2009, vol 44, pp. 2774–2779.

    Article  Google Scholar 

  18. P.A. Bianconi, S.J. Joray, B.L. Aldrich, J. Sumranjit, D.J. Duffy, D.P. Long, J.L. Lazorcik, L. Raboin, J.K. Kearns, S.L. Smulligan and Babyak J.M: J. Am. Chem. Soc., 2004, vol. 126, pp. 3191–202

    Article  Google Scholar 

  19. I. Karbovnyk, P. Savchyn, A. Huczko, M.C. Guidi, C. Mirri and Popov AI: Mater. Sci. Forum, 2015, vol. 821-823, pp. 261-4.

    Article  Google Scholar 

  20. R.G. Munro: J. Phys. Chem. Ref. Data, 1997, vol. 26, pp. 1195-203.

    Article  Google Scholar 

  21. R. Moene, L.F. Kramer, J. Schoonman, M. Makkee, J.A. Maulijn: Appl. Catal. A, 1997, vol. 162, pp. 181-91.

    Article  Google Scholar 

  22. P. Krawiec and Kaskel S: J. Solid State Chem. 2006, vol. 179, pp. 2281–9.

    Article  Google Scholar 

  23. M.B. Shiflett, H.C. Foley: Science 1999, vol. 285, pp. 1902-5.

    Article  Google Scholar 

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Acknowledgment

This study was patented by Erciyes University Teknopark A.Ş.

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Authors and Affiliations

  1. Department of Science Education, Faculty of Education, Erciyes University, 38039, Kayseri, Turkey

    İ. AFŞIN KARİPER

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  1. İ. AFŞIN KARİPER
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Correspondence to İ. AFŞIN KARİPER.

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Manuscript submitted August 8, 2016.

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KARİPER, İ.A. The Synthesis of Silicon Carbide in Rhombohedral Form with Different Chemicals. Metall Mater Trans A 48, 3108–3112 (2017). https://doi.org/10.1007/s11661-017-4050-9

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