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Effect of niobium addition on hot deformation behaviors of medium carbon ultra-high strength steels

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Abstract

The hot deformation behaviors of two medium carbon ultra-high strength steels with different niobium contents were investigated by using Zener-Hollmom parameter and processing map, and the effect of niobium addition on the hot deformation behavior of medium carbon steel was determined. The hot compression tests were conducted on a Gleeble-3500 thermo-mechanical simulator deformed at temperatures from 850 to 1 200 °C and strain rates from 0.001 to 1 s−1. The processing maps of two test steels were built at a true strain of 0.7 based on dynamic materials model (DMM). There are two peak efficiency domains and two flow instability regions in both test steels. However, the peak efficiency domains of Nb-bearing steel move to higher temperature due to the inhibition of dynamic recrystallization (DRX), and the instability domains of Nb-bearing steel are enlarged due to the precipitation of Nb-containing particles during hot deformation. The optimum process parameters of Nb-bearing and Nb-free steels for industrial production were determined according to the processing map and the microstructural observation.

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References

  1. Meng Fanmao. Application of Niobium, Vanadium and Titanium in Special Steel[J]. Microalloying Technology, 2001, 1(1): 28–33

    Google Scholar 

  2. Dong Tao. To Promote the Development and Application of the Microalloying Technology in Our Country[J]. Microalloying Technology, 2001, 1(1): 9–41

    Google Scholar 

  3. Yong Qilong. Physical Metallurgical Data of Niobium in Steel[J]. Journal of Iron and Steel Research, 1998, 10(2): 66–69

    Google Scholar 

  4. Yong Qilong, Ma Mingtu. Micro Alloys-Physical and Mechanical Metallurgy[M]. Beijing: Mechanical Industry Press, 1989

    Google Scholar 

  5. Dong Tao, Fu Junyan. Physical Metallurgy of Micro Niobium Treated Steel[J]. Microalloying Technology, 2002, 2(3): 48–53

    Google Scholar 

  6. Wilmes S, Zwick G. Effect of Niobium and Vanadium as an Alloying Element in Tool Steels with High Chromium Content[C]. 6 th International Tooling Conference(Karlstad university), 2002

    Google Scholar 

  7. Feng Rui. Metal Physics[M]. Beijing: Science Press, 1999

    Google Scholar 

  8. HU Xin-bin, LI Lin, WU Xiao-chun. Application of Niobium Microalloying in Special Steels[J]. Heat Treatment of Metals, 2003, 28(6): 5–10

    Google Scholar 

  9. Zhang Shusong, Tong Ailian. The Toughness Mechanism and Technology Approach of Steel[M]. Beijing: Weapon Industry Press, 1995

    Google Scholar 

  10. Klaus, V R C Guimarues. Effect of Niobium in Works Steels and Application[J]. Microalloying Technology, 2002, 2(2): 49–53

    Google Scholar 

  11. Mercer C and Soboyejo W O. Hall-Petch Relationships in Gamma Titanium Aluminides[J]. Scripta Materialin, 1996, 35(1): 17–22

    Article  Google Scholar 

  12. TSUJII N, ABE G. High Temperature Low Cycle Fatigue Behavior of a 4.2Cr-2.5Mo-V-Nb Hot Work Tool Steel[J]. Journal of Material Science Letters, 1996, 15: 1251–1254

    Article  Google Scholar 

  13. TSUJII N, ABE G. Effect of Testing Atmosphere on Low Cycle Fatigue of Hot Work Tool Steel at Elevated Temperature[J]. ISIJ. International, 1995, 35(7): 920–926

    Article  Google Scholar 

  14. Azevedo R, Barbosa E, Pereloma V. Development of Ultrafme Grain Ferrite in Low C-Mn and Nb-Ti Microauyed Steels after Waml Torsion and Intercritical Annealing[J]. Materials Science and Engineeger A, 2005, 4(2): 98–108

    Article  Google Scholar 

  15. Cheng L, Chang H, Tang B, et al. Deformation and Dynamic Recrystallization Behavior of a High Nb Containing Ti Al Alloy[J]. Journal of Alloys and Compounds, 2013, 552: 363–369

    Article  Google Scholar 

  16. Nakashima S, Takashima K, Harase J. Effect of Thickness on Secondary Recrystallization of Fe-3%Si[J]. Acta Metallurgicalet Materialia, 1994, 42:539

    Google Scholar 

  17. ZHANG Zhao-hui, LIU Yong-ning, LIANG Xiao-kai, et al. The Effect of Nb on Recrystallization Behavior of a Nb Micro-alloyed Steel[J]. Materials Science and Engineering A, 2008, 474: 254–260

    Article  Google Scholar 

  18. Sandstrom R, Lagneborg R. A Model for Hot Working Occurring by Recrystallization[J]. Acta Metallurgica, 1975, 23(3): 387–398

    Article  Google Scholar 

  19. Rollett AD, Srolovitz DJ, Doherty RD, et al. Computer Simulation of Recrystallization in Non-uniformly Deformed Metals[J]. Acta Metallurgica, 1989, 37(2): 627–639

    Article  Google Scholar 

  20. Gottstein G, Frommert M, Goerdeler M, et al. Predicting the Critical Conditions for Dynamic Recrystallization in the Austenitic Steel 800H[J]. Materials Science and Engineering A, 2004, 387–389: 604–608

    Article  Google Scholar 

  21. Dehghan-Manshadi A, Barnett M R, Hodgson P D, et al. Recrystallization in AISI 304 Austenitic Stainless Steel During and after Hot Deformation[J]. Materials Science and Engineering A, 2008, 485: 664–672

    Article  Google Scholar 

  22. Dong L, Zhong Y, Ma Q, et al. Dynamic Recrystallization and Grain Growth Behavior of 20SiMn low Carbon Alloy Steel[J]. Tsinghua Sci. Technol., 2008, 13: 609–613

    Article  Google Scholar 

  23. Poliak E I, Jonas J J. A one-parameter Approach to Determining the Critical Condition for the Initiation of Dynamic Recrystallization[J]. Acta Materialia, 1996, 44(1): 127–136

    Article  Google Scholar 

  24. Meng Gang, Li Bolong, Li Hongmei, et al. Hot Deformation and Proeess-ing Maps Of an Al-5.7wt% Mg Alloy with Erbium[J]. Materials Science and Engineering A, 2009, 517(1-2): 132–137

    Article  Google Scholar 

  25. Kyu H O, Jeong J S, Koo Y M, et al. The Evolution of the Rolling and Recrystallization Textures in Cold-rolled Al Containing High Mn Austenitic Steels[J]. Materials Chemistry and Physics, 2015, 161: 9–18

    Article  Google Scholar 

  26. Xua T C, Peng X D, Qin J, et al. Dynamic Recrystallization Behavior of Mg-Li-Al-Nd Duplex Alloy during Hot Compression[J]. Journal of Alloys and Compounds, 2015, 639: 79–88

    Article  Google Scholar 

  27. Frost HJ, Ashby MF. Defomation Mechanism Maps, the Plasticity and Creep Of Metals and Ceramics[M]. London:Pergamon Press, 1982

    Google Scholar 

  28. Zrink J, Kvackaj T, Sripinproach D, et al. Influence of Plastic Deformation Conditions on Structure Evolution in Nb-Ti Microalloyed Steel[J]. Journal of Material Processing Technilogy, 2003, 133: 236–242

    Article  Google Scholar 

  29. Liu H, Xue F, Bai J, et al. Effect of Heat Treatments on the Micro-structure and Mechanical Properties of an Extruded Mg95.5Y3Zn1.5 Alloy[J]. Materials Science and Engineering: A, 2013, 585(0): 261–267

    Article  Google Scholar 

  30. Sivakesavam, Y V R K Prasad. Hot Deformation Behavior of as-cast Mg-2Zn-1Mn Alloy in Compression: a Study with Processing Map[J]. Materials Science and Engineering A, 2003, 362(1-2): 118–124

    Article  Google Scholar 

  31. PS Robi, US Dixit. Application of Neural Networks Ingenerating Processing Map for Hot Working[J]. Journal of Materials Proeessing Technology, 2003, 142(l): 289–297

    Article  Google Scholar 

  32. Huang C, Hawbolt EB, Chen X, et al. Flow Stress Modeling and Warm Rolling Simulation Behavior of Two Ti-Nb Interstitial-free Steels in the Ferrite Region[J]. Acta Mater., 2001(49): 1445–1452

    Article  Google Scholar 

  33. Shukla A K, Narayana Murty S V S, Sharma S C, et al. Constitutive Modeling of hot Deformation Behavior of Vacuum hot Pressed Cu-8Cr-4Nb Alloy[J]. Materials and Design, 2015, 75: 57–64

    Article  Google Scholar 

  34. Liu XiaoYall, Pan QingLin, He YunBin. Flow Behavior and Microstructural Evolution of Al-Cu-Mg-Ag Alloy During Hot Compression Deformation[J]. Materials Science and Engineering A, 2009, 500(1-2): 150–154

    Article  Google Scholar 

  35. Chen J, Wang Z, Lu S. Effects of Electric Parameters on Microstructure and Properties of Mao Coating Fabricated on ZK60 Mg Alloy in Dual Electrolyte[J]. Rare Metals, 2012, 31(2): 172–177

    Article  Google Scholar 

  36. Xu DK, Han EH. Effects of Icosahedral Phase Formation on the Microstructure and Mechanical Improvement of Mg Alloys: A Review[J]. Progress in Natural Science: Materials International, 2012, 22(5): 364–385

    Article  Google Scholar 

  37. Quan GZ, Li GS, Chen T, et al. Dynamic Recrystallization Kinetics of 42CrMo Steel During Compression at Different Temperatures and Strain Rates[J]. Materials Science and Engineering: A, 2011, 528(13-14): 4643–4651

    Article  Google Scholar 

  38. Zhu YM, Morton AJ, Nie JF. Growth and Transformation Mechanisms of 18R and 14H in Mg-Y-Zn Alloys[J]. Acta Materialia, 2012, 60(19): 6562–6572

    Article  Google Scholar 

  39. Xu SW, Zheng MY, Kamado S, et al. Dynamic Microstructural Changes During Hot Extrusion and Mechanical Properties of a Mg-5.0Zn-0.9Y-0.16Zr (wt%) Alloy[J]. Materials Science and Engineering: A, 2011, 528(12): 4055–4067

    Article  Google Scholar 

  40. Cho S H, Kang K B, Jonas J J. Mathematical Modeling of the Recry-stallization Kinetics of Nb Microalloyed Steels[J]. ISIJ International, 2001, 41(7): 766–773

    Article  Google Scholar 

  41. Vervynck S, Verbeken K, Thibaux P, et al. Recrystallization-precipitation Interaction during Austenite Hot Deformation of a Nb Microalloyed Steel Mater[J]. Materials Science and Engineering A, 2011, 528: 5519–5528

    Article  Google Scholar 

Download references

Acknowledgements

Thanks for the supporting tests of State Key Laboratory of Material Processing and Die & Mould Technology and Analysis and Test Center in Huazhong University of Science and Technology.

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Correspondence to Lichao Zhang  (张李超) or Yusheng Shi  (史玉升).

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Supported by the National 863 Program of China (No.2015AA042505), Hubei Department of Education Youth Program (No.Q20123001), Hubei Province Natural Science Foundation (No.2014 cfb177), Wuhan Huaxia Fine Blanking Technology Co., LTD Program (No.YYYY2014-015)

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Yang, X., Zhang, L., Shi, Y. et al. Effect of niobium addition on hot deformation behaviors of medium carbon ultra-high strength steels. J. Wuhan Univ. Technol.-Mat. Sci. Edit. 32, 162–172 (2017). https://doi.org/10.1007/s11595-017-1575-0

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  • DOI: https://doi.org/10.1007/s11595-017-1575-0

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