Abstract
This work is part of a project aimed at developing a new biocomposite material that can be used for thermal insulation purposes. This material is mainly composed of sunflower stem chips. A chitosan-based biomatrix is used as binder between them. We focus here only on the mechanical response of this biocomposite. The goal is to investigate experimentally the link between its macroscopic response and phenomena which occur at the scale of the constituents, namely the bark and pith chips. The grid method, which is one of the full-field measurement systems employed in experimental mechanics to measure displacement and strain fields, is employed because of the very heterogeneous nature of this material. This heterogeneity is not only due to the contrast in rigidity between bark and pith, but also to the presence of voids within the material. These voids, as well as the presence of pith, lead us to develop and employ a specific marking procedure for the specimen surface under investigation. Two values for the mass percent fraction of chitosan are investigated, to observe the influence of this parameter on the global stiffness of the material and on local phenomena that occur in its bulk. The full-field measurement technique employed here leads us to detect and quantify significant heterogeneities in the strain fields, which are closely related to the material heterogeneities themselves.
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References
Witz JF, Roux S, Hild F, Reunier JB (2008) Mechanical properties of crimped mineral wools, Identification from digital image correlation. J Eng Mater Technol 130(12):1–7
Hild F, Maire E, Roux S, Witz JF (2009) Three-dimensional analysis of a compression test on stone wool. Acta Mater 57(12):3310–3320
Roma LC, Martello LS, Savastano H (2008) Evaluation of mechanical, physical and thermal performance of cement-based tiles reinforced with vegetable fibers. Constr Build Mater 22(1):668–674
Ortiz O, Castells F, Sonnemann G (2009) Sustainability in the construction industry: A review of recent developments based on lca. Constr Build Mater 23(1):28–39
Korjenic A, Petranek V, Zach J, Hroudova J (2011) Development and performance evaluation of natural thermal-insulation materials composed of renewable resources. Energy Build 43:2518–2523
Hajj NE, Dheilly RM, Aboura Z, Benzeggagh M, Queneudec M (2011) Development of thermal insulating and sound absorbing agro-sourced materials from auto linked flax-tows. Ind Crop Prod 34:921–928
Panyakaew S, Fotios S (2011) New thermal insulation boards made from coconut husk and bagasse. Energy Build 43:1732–1739
Bentchikou M, Guidoum A, Scrivener K, Silhadi K, Hanini S (2012) Effect of recycled cellulose fibres on the properties of lightweight cement composite matrix. Constr Build Mater 34(1):451–456
Chikhi M, Agoudjil B, Boudenne A, Gherabli A (2013) Experimental investigation of new biocomposite with low cost for thermal insulation. Energy Build 66(1):267–273
Benfratello S, Capitano C, Peri G, Rizzo G, Scaccianoce G, Sorrentino G (2013) Thermal and structural properties of a hemp-lime biocomposite. Constr Build Mater 48:745–754
Sun S, Mathias J-D, Toussaint E, Grédiac M (2013) Hygromechanical characterization of sunfower stems. Ind Crop Prod 46:50–59
Sun S, Mathias J-D, Toussaint E, Grédiac M (2014) Characterizing the variance of mechanical properties of sunflower bark for biocomposite applications. Bioresources 9(1):922–937
Pennec F, Alzina A, Tessier-Doyen N, Nait-Ali B, Mati-Baouche N, De Baynast H, Smith D.S (2013) A combined finite-discrete element method for calculating the effective thermal conductivity of bio-aggregates based materials. Int J Heat Mass Transfer 60:274–283
Patel AK, Michaud P, Petit E, De Baynast H, Grédiac M, Mathias J-D (2013) Development of a chitosan-based adhesive. application to wood bonding. Journal of Applied Polymer Science, Wiley 127(6):5014–5021
Mati-Baouche N, De Baynast H, Sun S, Lebert A, Sacristan Lopez-Mingo CJ, Leclaire P, Michaud P (2014) Mechanical, thermal and acoustical characterizations of a insulating bio-based composite made from sunflower stalks particles and chitosan, Industrial Crops and Products. Accepted
4108-10 DIN (2008) Anwendungsbezogene Anforderungen an Wrmedämmstoffe-Werkmässig hergestellte Wärmedmmstoffe, Ausgabe
Patel AK, Michaud P, De Baynast H, Grédiac M, Mathias J.-D (2013) Preparation of chitosan-based adhesives and assessment of their mechanical properties. Journal of Applied Polymer Science, Wiley 127(5):3869–3876
Patel AK, De Baynast H, Mathias JD, Grédiac M, Michaud P Adhesive Composition Including deacetylated Chitosan. 2013. United States Patent Application 20130143041
FAOSTAT. Fao statistics division 2012: World sunflower seed area harvested. http://faostat3.fao.org/faostat-gateway/go/to/download/Q/QC/F
Yan ZL, Wang H, Lau KT, Pather S, Zhang JC, Lin G, Ding Y (2013) Reinforcement of polypropylene with hemp fibres. Compos Part B: Eng 46:221–226
Andersons J, Joffe R (2009) Estimation of the tensile strength of an oriented flax fiber-reinforced polymer composite. Compos Part A: Appl Sci Manuf 42(9):1229–1235
Hautala M, Pasila A, Pirila J (2004) Use of hemp and flax in composite manufacture: a search for new production methods. Compos Part A: Appl Sci Manuf 35(1):11–16
Mathias J-D, Alzina Grédiac A, Michaud P, Roux P, De Baynast H, Delattre C, Dumoulin N, Faure T, Larrey-Lassalle P, Mati-Baouche N, Pennec F, Sun S, Tessier-Doyen N, Toussaint E, Wei W (2014) Valorising sunflower stems as natural fibres for biocomposite applications: an environmental and socio-economic opportunity. Submitted
Mati-Baouche N, De Baynast H, Vial C, Audonnet F, Sun S, Petit E, Pennec F, Prevot V, Michaud P (2014) Physico-chemical, thermal and mechanical characterizations of solubilized and solid state chitosans. Submitted
Wu LQ, Eembree H, Balgley B, Smith P, Payne G (2002) Utilizing renewable resources to create functional polymers: chitosan-based associative thickener. Environ Sci Technol 36:3446–3454
Salome: the Open Source Integration Plateform for Numerical Simulation. http://www.salome-platform.org/
Aster Code for Windows. http://sourceforge.net/projects/asterwin/
Abdou A, Boudaiwi I (2013) The variation of thermal conductivity of fibrous insulation materials under different levels of moisture content. Constr Build Mater 43:533–544
Badulescu C, Grédiac M, Haddadi H, Mathias JD, Balandraud X, Tran HS (2011) Applying the grid method and infrared thermography to investigate plastic deformation in aluminium multicrystal. Mech Mater 43(11):36–53
Delpueyo D, Grédiac M, Balandraud X, Badulescu C (2012) Investigation of martensitic microstructures in a monocrystalline Cu-Al-Be shape memory alloy with the grid method and infrared. Mech Mater 45(1):34–51
Chrysochoos A, Surrel Y (2012) Chapter 1. Basics of metrology and introduction to techniques. In: Grédiac M, Hild F (eds) Full-field measurements and identification in solid mechanics, pp 1–29. Wiley
Surrel Y (1994) Moiré and grid methods in optics: a signal-processing approach , Proceedings of the SPIE, volume 2342, pp 213–220
Surrel Y (2000) Photomechanics, Topics in Applied Physic 77, chapter Fringe Analysis, pp 55–102. Springer
Badulescu C, Grédiac M, Mathias J-D, Roux D (2009) A procedure for accurate one-dimensional strain measurement using the grid method. Experimental Mechanics 49(6):841–854. Springer
Badulescu C, Grédiac M, Mathias J-D (2009) Investigation of the grid method for accurate in-plane strain measurement. Meas Sci Technol 20:095102. doi:10.1088/0957-0233/20/9/095102. IOP Science
Sur F, Grédiac M (2014) Towards deconvolution to enhance the grid method for in-plane strain measurement. Inverse Problems and Imaging 8(1):259–291
Grédiac M, Sur F, Badulescu C, Mathias J-D (2013) Using deconvolution to improve the metrological performance of the grid method. Optics and Lasers in Engineering 51:716–734
Kumagai S, Xia S, Notbohm J, Rosakis A, Ravichandran G (2013) Three-dimensional displacement and shape measurement with a diffraction assisted grid method. Strain 49(5). doi:10.1111/str.12046
Avril A, Vautrin S, Surrel Y (2004) Grid method: application to the characterization of cracks. Exp Mech 44(1):37–43
Kim MR, Wisnom J-H, Pierron F, Avril S (2009) Local stiffness reduction in impacted composite plates from full-field measurements. Compos Part A: Appl Sci Manuf 40(12):1961–1974
Ri K, Nanbara S, Saka M, Kobayashi D (2013) Dynamic thermal deformation measurement of large-scale, high-temperature piping in thermal power plants utilizing the sampling moiré method and grating magnets. Exper Mech 53(9):1635–1646
(2011) Sikaflex®-11 FC+ data sheet, #525
Piro JL, Grédiac M (2004) Producing and transferring low-spatial-frequency grids for measuring displacement fields with moiré and grid methods. Experimental Techniques 28(4):23–26
Chiang CL (2003) Statistical methods of analysis. World Scientific Pub Co Inc.
Matlab 2009 b. the Language of Technical Computing. http://www.mathworks.com/products/matlab/
Acknowledgments
The authors would like to thank the French National Research Agency (ANR), Céréales Vallée, and ViaMéca for their financial support (ANR-10-ECOT-004 Grant).
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Sun, S., Grédiac, M., Toussaint, E. et al. Applying a Full-Field Measurement Technique to Characterize the Mechanical Response of a Sunflower-Based Biocomposite. Exp Mech 55, 917–934 (2015). https://doi.org/10.1007/s11340-015-9988-1
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DOI: https://doi.org/10.1007/s11340-015-9988-1