Abstract
Novel nanomaterials were synthesized by thermal structuring of new soluble ferrocene-containing polychalcones. The products were studied by gel permeation chromatography, IR spectroscopy, transmission electron microscopy, scanning electron microscopy, and TGA. According to transmission electron microscopy data, the statistical average sizes of magnetic nanoparticles ranged from 4 to 45 nm. X-ray diffraction studies of the samples showed the overwhelming predominance of iron in the zero-valent state (Fe0) in the iron-containing nanoparticles.
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This study was financially supported by the Ministry of Science and Higher Education of the Russian Federation and used research equipment of the Center for Molecular Structure Investigation, A. N. Nesmeyanov Institute of Organoelement Compounds, RAS. The authors are grateful to Z. S. Klemenkova for recording the IR spectra and to S. S. Abramchuk and I. V. Nagornova for TEM and SEM investigations, respectively.
No human or animal subjects were used in this research.
The authors declare no competing interests.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, Vol. 72, No. 6, pp. 1334–1342, June, 2023.
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Dvorikova, R.A., Il’yin, M.M., Buzin, M.I. et al. New magnetic nanomaterials based on ferrocene-containing polychalcones. Russ Chem Bull 72, 1334–1342 (2023). https://doi.org/10.1007/s11172-023-3908-9
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DOI: https://doi.org/10.1007/s11172-023-3908-9