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Hygro-mechanical behaviour of cement paste and mortar during drying

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Abstract

The hygro-mechanical behaviour of cement paste and mortar during drying was investigated to assess the impact of the presence of aggregates. Samples were cast, and then subjected to air-drying and moderate oven-drying at 38 °C after a long maturation period. Shrinkage and mass variation were monitored and compressive and bending tests were carried out as a function of the drying conditioning mode and composition. The results show that the drying shrinkage of mortar is considerably lower than that of cement paste due to the presence of aggregates in the mixture, as expected, and tends more quickly to stabilisation. However, their relative losses in mass remain close for a given drying conditioning mode. Moreover, the cracks appear on air-dried cement paste, also visible on oven-dried cement paste after the application of hydraulic oil providing sufficient contrast, and then become imperceptible in the case of mortar. The presence of aggregates that leads the compressive strength and in particular the Young’s modulus to rise at the initial (saturated) state accentuates the increase of compressive strength and limits the impact of drying-induced micro-cracking on the Young’s modulus and bending strength at the dried state. Furthermore, the intensification of the rapid drying process of mortar from 38 to 60 °C leads mainly to a slightly lower drying shrinkage reached more quickly to stabilisation and a higher bending strength. All these results show that the performance of cement-based materials is influenced by their drying process and composition.

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References

  • Acker, P.: Comportement mécanique du béton: apport de l’approche physico-chimique. PhD dissertation. Ecole Nationale des Pont et Chaussées, Rapport de Recherche LPC n°152, Paris [in French] (1988)

  • Aili, A., Vandamme, M., Torrenti, J.-M., Masson, B.: A viscoelastic poromechanical model for shrinkage and creep of concrete. Cem. Concr. Res. 129, 105970 (2020)

    Article  Google Scholar 

  • Baroghel-Bouny, V.: Caractérisation des pâtes de ciment et des bétons. PhD dissertation, Ecole Nationale des Ponts et Chaussées, Paris [in French] (1994)

  • Bartlett, F.M., MacGregor, J.G.: Effect of moisture condition on concrete core strengths. ACI Mater. J. 91(3), 227–236 (1994)

    Google Scholar 

  • Bazant, Z.P., Wittmann, F.H.: Creep and Shrinkage in Concrete Structures. Wiley, New York (1982)

    Google Scholar 

  • Bisschop, J., Pel, L., van Mier, J.G.M.: Effect of aggregate size and paste volume on drying shrinkage microcracking in cement-based composites. In: Ulm, F.-J., Bažant, Z.P., Wittmann, F.H. (eds.) Creep, Shrinkage & Durability Mechanics of Concrete and Other Quasi-Brittle Materials, pp. 75–80. Elsevier, Amsterdam (2001)

    Google Scholar 

  • Carde, C., François, R.: Effect of ITZ leaching on durability of cement-based materials. Cem. Concr. Res. 27, 971–978 (1997)

    Article  Google Scholar 

  • Caré, S.: Effect of temperature on porosity and chloride diffusion in cement pastes. Constr. Build. Mater. 22, 1560–1573 (2008)

    Article  Google Scholar 

  • Chen, X.T., Caratini, G., Davy, C.A., Troadec, D., Skoczylas, F.: Coupled transport and poro-mechanical properties of heat-treated mortar under confinement. Cem. Concr. Res. 49, 10–20 (2013)

    Article  Google Scholar 

  • Chunran, W., Shikong, K.: Effect of high-calcium sepiolite on the rheological behaviour and mechanical strength of cement pastes and mortars. Constr. Build. Mater. 196, 105–114 (2019)

    Article  Google Scholar 

  • de Larrard, F., Belloc, A.: L’influence du granulat sur la résistance à la compression des bétons. Bull. Lab. Ponts Chauss. 219, 41–52 (1999)

    Google Scholar 

  • Dong, W., Zhao, X., Zhou, X., Yuan, W.: Effects of moisture gradient of concrete on fracture process in restrained concrete rings: experimental and numerical. Eng. Fract. Mech. 208, 189–208 (2019)

    Article  Google Scholar 

  • Gilkey, H.J.: The moist curing of concrete. Eng. News-Rec. 119, 630–633 (1937)

    Google Scholar 

  • Grassl, P., Wong, H.S., Buenfeld, N.R.: Influence of aggregate size and volume fraction on shrinkage induced micro-cracking of concrete and mortar. Cem. Concr. Res. 40, 85–93 (2010)

    Article  Google Scholar 

  • Hearn, N.: Effect of shrinkage and load-induced cracking on water permeability of concrete. ACI Mater. J. 96, 234–241 (1999)

    Google Scholar 

  • Hotta, H., Takiguchi, K.: Influence of drying and water supplying after drying on tensile strength of cement mortar. Nucl. Eng. Des. 156, 219–228 (1995)

    Article  Google Scholar 

  • Jennings, H.M., Thomas, J.J., Gevrenov, J.S., Constantinides, G., Ulm, F.-J.: A multi-technique investigation of the nanoporosity of cement paste. Cem. Concr. Res. 37, 329–336 (2007)

    Article  Google Scholar 

  • Jennings, H.M., Kumar, A., Sant, G.: Quantitative discrimination of the nano-pore-structure of cement paste during drying: new insight from water sorption isotherms. Cem. Concr. Res. 76, 27–36 (2015)

    Article  Google Scholar 

  • Kanna, V., Olson, R.A., Jennings, H.M.: Effect of shrinkage and moisture content on the physical characteristics of blended cement mortars. Cem. Concr. Res. 28, 1467–1477 (1998)

    Article  Google Scholar 

  • Lagier, F., Jourdain, X., De Sa, C., Benboudjema, F., Colliat, J.B.: Numerical strategies for prediction of drying cracks in heterogeneous materials: comparison upon experimental results. Eng. Struct. 33, 920–931 (2011)

    Article  Google Scholar 

  • Malbois, M.: Multi-scale analysis of drying: effect of aggregates. AJCE Spec. Iss. 35, 570–577 (2017)

    Google Scholar 

  • Maruyama, I., Sasano, H.: Strain and crack distribution in concrete during drying. Mater. Struct. 47, 517–532 (2014)

    Article  Google Scholar 

  • Maruyama, I., Nishioka, Y., Igarashi, G., Kunio, M.: Microstructural and bulk property changes in hardened cement past during the drying process. Cem. Concr. Res. 58, 20–34 (2014)

    Article  Google Scholar 

  • Maruyama, I., Kishi, N., Aili, A.: The relative humidity range for the development of irreversible shrinkage in hardened cement paste. J. Adv. Concr. Technol. 19, 585–592 (2021)

    Article  Google Scholar 

  • Maso, J.C.: La liaison pâte-granulats. In: Baron, J., Sauterey, R. (eds.) Le Béton Hydraulique: Connaissance et Pratique, pp. 247–259. Presses de l’ENPC(1982)

    Google Scholar 

  • Miao, Y., Lu, Z., Wang, F., Wang, H., Li, Y., Lin, J., Jiang, J.: Shrinkage cracking evolvement in concrete cured under low relative humidity and its relationship with mechanical development. J. Build. Eng. 72, 106670 (2023)

    Article  Google Scholar 

  • Mills, R.H.: Strength-maturity relationship for concrete which is allowed to dry. In: RILEM Int. Symp. on Concrete and Reinforced Concrete in Hot Country. Haîfa (1960)

    Google Scholar 

  • Neville, A.M.: Properties of Concrete, 4th edn. Longman, Harlow (1995)

    Google Scholar 

  • Okajima, T., Ishikawa, T., Ichise, K.: Moisture effect on the mechanical properties of cement mortar. Trans. Jpn. Concr. Inst. 2, 125–132 (1980)

    Google Scholar 

  • Ollivier, J.P., Maso, J.C., Bourdette, B.: Interfacial transition zone in concrete. Advn. Cem. Bas. Mat. 2, 30–38 (1995)

    Article  Google Scholar 

  • Parrott, L.J., Hansen, W., Berger, R.L.: Effect of first drying upon the pore structure of hydrated alite paste. Cem. Concr. Res. 10, 647–655 (1980)

    Article  Google Scholar 

  • Pihlajavaara, S.E.: A review of some of the main results of a research on the ageing phenomena of concrete, effect of moisture conditions on strength, shrinkage and creep of mature concrete. Cem. Concr. Res. 4, 761–771 (1974)

    Article  Google Scholar 

  • Popovics, S.: Effect of curing method and moisture condition on compressive strength of concrete. ACI Mater. J. 83, 650–657 (1986)

    Google Scholar 

  • Price, W.H.: Factors influencing concrete strength. J. ACI. 47, 417–432 (1951)

    Google Scholar 

  • Rangaraju, P.R., Olek, J., Diamond, S.: An investigation into the influence of inter-aggregate spacing and the extent of the ITZ on properties of Portland cement concretes. Cem. Concr. Res. 40, 1601–1608 (2010)

    Article  Google Scholar 

  • Rhardane, A., Alam, S.Y., Grondin, F.: The role of surface micro-cracks in cementitious materials responsible for the Pickett effect. Mech. Time-Depend. Mater. 26, 719–740 (2021)

    Article  Google Scholar 

  • Rougelot, T., Skoczylas, F., Burlion, N.: Water desorption and shrinkage in mortars and cement pastes: experimental study and poromechanical model. Cem. Concr. Res. 39, 36–44 (2009)

    Article  Google Scholar 

  • Scrivener, K.L., Bentur, A., Pratt, P.L.: Quantitative characterisation of the transition zone in high-strength concrete. Adv. Cem. Res. 1, 230–237 (1988)

    Article  Google Scholar 

  • Soleilhet, F., Benboudjema, F., Jourdain, X., Gatuing, F.: Role of pore pressure on cracking and mechanical performance of concrete subjected to drying. Cem. Concr. Compos. 114, 103727 (2020)

    Article  Google Scholar 

  • Szczesniak, M., Rougelot, T., Burlion, N., Shao, J.F.: Compressive strength of cement-based composites: roles of aggregate diameter and water saturation degree. Cem. Concr. Compos. 37, 249–258 (2013)

    Article  Google Scholar 

  • Thomas, J.J., Allen, A.J., Jennings, H.M.: Structural changes to the calcium-silicate-hydrate gel phase of hydrated cement with age, drying, and resaturation. J. Am. Ceram. Soc. 91, 3362–3369 (2008)

    Article  Google Scholar 

  • Tran, D.L., Mouret, M., Cassagnebère, F., Phung, Q.T.: Effects of intrinsic granular porosity and mineral admixtures on durability and transport properties of recycled aggregate concretes. Mater. Today Commun. 33, 104709 (2022)

    Article  Google Scholar 

  • Uchikawa, H., Hanehara, S., Hirao, H.: Influence of microstructural change under stress on the strength related properties of hardened cement mortar and paste. Adv. Cem. Bas. Mat. 6, 87–98 (1997)

    Article  Google Scholar 

  • Völkl, J.J., Beddoe, R.E., Setzer, M.J.: The specific surface of hardened cement paste by small-angle X-ray scattering. Cem. Concr. Res. 17, 81–88 (1988)

    Article  Google Scholar 

  • Vu, X.H., Malecot, Y., Daudeville, L., Buzaud, E.: Experimental analysis of concrete behaviour under high confinement: effect of the saturation ratio. Int. J. Solids Struct. 46, 1105–1120 (2009)

    Article  MATH  Google Scholar 

  • Wittmann, F.H.: Creep and shrinkage mechanisms. In: Bažant, Z.P., Wittmann, F.H. (eds.) Creep and Shrinkage in Concrete Structures, pp. 129–161. Wiley, New York (1982)

    Google Scholar 

  • Wong, H.S., Zobel, M., Buenfeld, N.R., Zimmerman, R.W.: Influence of the interfacial transition zone and microcracking on the diffusivity, permeability and sorptivity of cement-based materials after drying. Mag. Concr. Res. 61, 571–589 (2009)

    Article  Google Scholar 

  • Wu, Z., Wong, H.S., Buenfeld, N.R.: Transport properties of concrete after drying-wetting regimes to elucidate the effects of moisture content, hysteresis and microcracking. Cem. Concr. Res. 98, 136–154 (2017)

    Article  Google Scholar 

  • Yurtdas, I., Leklou, N.: Effect of re-saturation after drying on hydric and strength behaviour of mortar. Mater. Struct. 54, 186 (2021)

    Article  Google Scholar 

  • Yurtdas, I., Burlion, N., Skoczylas, F.: Experimental characterisation of the drying effect on uniaxial mechanical of mortar. Mater. Struct. 37, 170–176 (2004)

    Article  Google Scholar 

  • Yurtdas, I., Burlion, N., Shao, J.F., Li, A.: Evolution of the mechanical behaviour of a high performance self-compacting concrete under drying. Cem. Concr. Compos. 33, 380–388 (2011)

    Article  Google Scholar 

  • Yurtdas, I., Burlion, N., Shao, J.F.: Evolution of mechanical behaviour of mortar with re-saturation after drying. Mater. Struct. 48, 3343–3355 (2015)

    Article  Google Scholar 

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  1. MATIM, Université de Reims Champagne-Ardenne, Reims, France

    I. Yurtdas

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Yurtdas, I. Hygro-mechanical behaviour of cement paste and mortar during drying. Mech Time-Depend Mater (2023). https://doi.org/10.1007/s11043-023-09619-7

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