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Determination of Number Density of Particles Together with Measurement of Their Sizes by Dynamic Light Scattering

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Measurement Techniques Aims and scope

A method is proposed for measuring the size of particles in a dynamic light scattering analyzer along with a determination of their number density in suspension. It is shown that this method can be used to measure the parameters of various nanoparticles, including nonspherical ones. An experimental prototype of a dynamic light scattering analyzer for measuring the number density of nanoparticles along with their sizes is described.

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References

  1. A. H. Puthusserickal, R. Suman, and V. Gunjan, “Making sense of Brownian motion: colloid characterization by dynamic light scattering,” Langmuir, 31, 3–12 (2015).

  2. V. M. Shmidt, Optical Spectroscopy for Chemists and Biologists, Tekhnosfera, Moscow (2007).

    Google Scholar 

  3. W. Haiss, N. T. K. Thanh, J. Aveyard, and D. G. Fernig, “Determination of size and concentration of gold nanoparticles from UV-Vis spectra,” Analyt. Chem., 79, 4215–4221 (2007).

  4. N. G. Khlebtsov, “Determination of size and concentration of gold nanoparticles from extinction spectra,” Analyt. Chem., 80, 6620–6625 (2008).

  5. D. Parmelle, A. Sadovoy, S. Gorelik, P. Free, J. Hobley, and D. G. Fernig, “A rapid method to estimate the concentration of citrate capped silver nanoparticles from UV-visible light spectra,” The Analyst, 139, 4855–4861 (2014).

  6. M. Quinten, Optical Properties of Nanoparticle Systems: Mie and Beyond, John Wiley & Sons, NY (2010).

  7. T. Hendel, M. Wuithschick, F. Kettemann, A. Birnbaum, K. Rademann, and J Polte, “In situ determination of colloidal gold concentrations with UV-Vis spectroscopy: limitations and perspectives,” Analyt. Chem., 86, 11114–11124 (2014).

  8. P. D. Waterman, “Symmetry, unitarity, and geometry in electromagnetic scattering,” Phys. Rev. D, No. 3, 825–839 (1970).

  9. C. F. Bohren and D. R. Huffman, Absorption and Scattering of Light by Small Particles, Wiley Interscience, New York (1983).

    Google Scholar 

  10. C. Matzler, Matlab Codes for Mie Scattering and Absorption, Institut für Angewandte Physik, Bern (2002).

  11. Refractive Index Database, www.refractiveindex.info, acc. March 20, 2018.

  12. B. N. Khlebtsov, V. A. Khanadeev, and N. G. Khlebtsov, “Determination of the size, concentration, and refractive index of silicon dioxide nanoparticles by spectroturbidimetry,” Opt. Spektrosk., 105, No. 5, 801–808 (2008).

    Article  Google Scholar 

  13. M. Glidden and M. Martin, “Characterizing gold nanorods in solution using depolarized dynamic light scattering,” J. Phys. Chem. C, 116, 8128–8137 (2012).

  14. A. D. Levin, E. A. Shmytkova, and B. N. Khlebtsov, “Multipolarization dynamic light scattering of nonspherical nanoparticles in solution,” J. Phys. Chem. C, 121, 3070–3077 (2017).

  15. S. Asano, and G. Yamamoto, “Light scattering by a spheroidal particle,” Appl. Optics, 14, 29–49 (1975).

  16. N. F. Khlebtsov, “T-matrix method in plasmonics – An overview,” J. Quant. Spectrosc. Radiat. Transf., 123, 184–217 (2013).

  17. W. R. Somerville, B. Auguié, and E. D. Le Ru, “User-friendly codes for fast and accurate calculations of light scattering by spheroids,” J. Quant. Spectrosc. Radiat.Transf., 174, 39–55 (2016).

  18. P. Johnson and R. Christy, “Optical constants of noble metals,” Phys. Rev. B, 6, No. 12, 4370–4379 (1972).

    Article  ADS  Google Scholar 

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Correspondence to A. D. Levin.

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Translated from Izmeritel’naya Tekhnika, No. 8, pp. 14–19, August, 2018.

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Levin, A.D., Nagaev, A.I. & Sadagov, A.Y. Determination of Number Density of Particles Together with Measurement of Their Sizes by Dynamic Light Scattering. Meas Tech 61, 760–766 (2018). https://doi.org/10.1007/s11018-018-1498-y

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  • DOI: https://doi.org/10.1007/s11018-018-1498-y

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