Abstract
Compressive mechanical properties of lattice structures made of titanium alloy Ti–6Al–4V, obtained using selective laser melting, are studied in three different metal conditions: in as-built SLM state, after chemical-heat treatment by ion nitriding, and after annealing. Specimen relative porosity is 50, 60, 70 and 80%. It is established that ion nitriding of lattice structures leads to formation upon them of antifriction layer surfaces several tens of micrometers thick. It is revealed that nitrogen saturation of surface layers for specimens with a degree of porosity of 50, 60, 70% does not have a significant effect on basic mechanical properties during compression, although it leads to an increase by more than 20% in surface hardness of beam elements. It is established that annealing at 720 °C leads to decomposition of the original martensitic α′-phase and to formation of a two-phase (α + β) structure, and removal of residual stresses.
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References
Kaschel RF, Celikin M, Dowling DP (2020) Effects of laser power on geometry, microstructure and mechanical properties of printed Ti–6Al–4V parts. J Mater Process Technol 278(116539)
Pol’kin I.S. (2015) Titanium alloy additive technology. Technologiya Legkikh Splavov (3):11–16
Wu X, Mei J, Boyer R, Williams J (2016) 3D-printing if titanium alloys , quality control of the product obtained and original powder. Tekhnol Legkikh Splavov (2):15–18
Yu. Loginov, Stepanov S, Khanykova E (2017) Effect of pore architecture of titanium implants on stress-strain state upon compression. Solid State Phenom 265:606–610
Koju N, Niraula S, Fotovvati B (2022) Additively manufactured porous Ti6Al4V for bone implants: a review. Metals 12(4):6872
Bandyopadhyay A, Espana F, Balla VK, Bose S, Ohgami Y, Davies NM (2010) Influence of porosity on mechanical properties and in vivo response of Ti6Al4V implants. Acta Biomater 6(4):1640–1648
Gilev MV, Volokitina EA, Loginov YN, Golodnov AI, Stepanov SI, Antoniali YV, Izmodenova MY, Zverev FN (2017) Optimization of bone defect augmentation with titanium cellular implants within operative traumatology and orthopedics. Vestn Ural Meditsin Akad Nauk 14(4):435–442
Loginov YN, Stepanov SI, Dub VA, Haschetmikova IA (2019) Quality of thin titanium cellular structure elements prepared by selective laser melting. Liteishchik Rossii (4):27–31
Stepanov SI, Loginov YN, Kuznetsov VP, Popov AA (2018) Effect of annealing on the structure and properties of titanium alloy with cellular architecture for medical applications. Met Sci Heat Treat 60(5–6):315–321
Lukina E, Kollerov M, Meswania J, Panin P, Khon A, Blunn G (2017) The influence of TiN and DLC deposition on the wear resistance of Nitinol—Ti6Al4V combination for the medical application. Mater Today Proc 4(3):4675–4679
Gorelyuk IN, Yas’kiv OI, Fedirko VN, Pastukh IM, Mashovets NS (2007) Application of combined nitriding methods for wear resistant coating formation on titanium alloys. Uproch Tekhnol Pokrytiya 7(31):29–33
Toboła D, Morgiel J, Maj L, Pomorska M, Wytrwal-Sarna M (2022) Effect of tribo-layer developed during turning of Ti–6Al–4V ELI alloy on its low-temperature gas nitriding. Appl Surf Sci 602(154327)
Wen K, Zhang C, Gao Y (2022) Influence of gas pressure on the low-temperature plasma nitriding of surface-nanocrystalline TC4 titanium alloy. Surf Coatings Technol 436(128327)
Zhao B, Wang H, Qiao N, Wang C, Hu M (2017) Corrosion resistance characteristics of a Ti–6Al–4V alloy scaffold that is fabricated by electron beam melting and selective laser melting for implantation in vivo. Mater Sci Eng C 70:832–841
Kamkar S, Mohammadi M, Karimi M, Salehi M (2022) Electrochemical and biological properties of mono- and bilayer nitride coatings deposited on Ti–6%Al–4%V alloy. Mater Chem Phys 286(126185)
Loginov YN, Koptyug A, Popov VV, Belikov SV, Mukanov G, Golodnov AI, Stepanov SI (2022) Compression deformation and fracture behavior of additively manufactured Ti–6Al–4V cellular structures. Intern J Lightweight Mater Manuf 5(1):126–135
Nguyen HD, Pramanik A, Basak AK, Dong Y, Prakash C, Debnath S, Shankar S, Jawahir IS, Dixit S, Buddhi D (2022) A critical review on additive manufacturing of Ti–6Al–4V alloy: microstructure and mechanical properties. J Mater Res Technol 18:4641–4661
Halevy I, Zamir G, Winterrose M, Ghose S, Grandini C, Moreno A (2010) Crystallographic structure of Ti6Al4V, TiHP and TiCP under high-pressure. J Physics Conf Ser (215)
Xia Z, Chen C, Zhu H, Hu Z, Nagarajan B, Guo L, Xi Z (2020) Study of residual stress in selective laser melting ofTi6Al4V. Mater Des 193(108846)
Chen LY, Huang JC, Lin CH, Pan CT, Chen SY, Yang TL, Lin DY, Lin HK, Jang JSC (2017) Anisotropic response of Ti–6Al–4V alloy fabricated by 3D printing selective laser melting. Mater Sci Eng A 682:389–395
Gayathri YKB, Kumar RL, Ramalingam VV, Priyadharshini GS, Kumar KS, Prabhu TR (2022) Additive manufacturing of Ti–6Al–4V alloy for biomedical applications. J Bio- Tribo-Corrosion 8(4):98
Wang J, Liu A, Ao Q, Wu C, Ma J, Cao P (2023) Energy absorption characteristics and preparation of porous titanium with high porosity. Mater Today Commun 34(105003)
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Work was carried out within the scope of a state assignment of the Russian Federation Ministry of Education and Science (theme No. FEUZ-2023-0015)
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Translated from Metallurg, No. 11, pp. 40–47, November, 2023. Russian DOI: https://doi.org/10.52351/00260827_2023_11_40
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Loginov, Y.N., Stepanov, S.I. & Slukin, E.Y. Effect of post-treatment on lattice structure and properties of additively prepared Ti–6Al–4V alloy. Metallurgist (2024). https://doi.org/10.1007/s11015-024-01658-w
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DOI: https://doi.org/10.1007/s11015-024-01658-w
Keywords
- Additive technology
- 3D-printing
- Titanium alloy
- Phase composition
- Chemical-heat treatment
- Nitrided layer
- Compression test