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Propylene oxide as a new reagent for mixed SiO 2 -based aerogels preparation

  • Invited Paper: Nano- and macroporous materials (aerogels, xerogels, cryogels, etc.)
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Abstract

A two-stage technique is developed to synthesize SiO2-based aerogels using propylene oxide as a reagent. By this technique, we were able to synthesize mixed SiO2–Cr2O3 and SiO2–Yb2O3 aerogels containing 0.4–1.3% at. of the dopant.

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References

  1. Aegerter MA, Leventis N, Koebel MM (2011) Aerogels handbook. Springer, Dordrecht, Heidelberg, London

    Book  Google Scholar 

  2. Yoldas BE, Annen MJ, Bostaph J (2000) Chem Mater 12:2475–2484

    Article  Google Scholar 

  3. Husing N, Schubert U (1998) Angew Chem Int Edit 37:23–45

    Article  Google Scholar 

  4. Fricke J, Lu X, Wang P, Buttner D, Heinemann U (1992) Int J Heat Mass Transf 35:2305–2309

    Article  Google Scholar 

  5. Conroy JFT, Hosticka B, Davis SC, Smith AN, Norris PM (1999) Microscale Thermophys Eng 3:199–215

    Article  Google Scholar 

  6. Hrubesh LW (1998) J Non-Cryst Solids 225:335–342

    Article  Google Scholar 

  7. Aristov YI, Restuccia G, Tokarev MM, Cacciola G (2000) React Kinet Catal Lett 69:345–353

    Article  Google Scholar 

  8. Antczak T, Mrowiec-Bialon J, Bielecki S, Jarzebski AB, Malinowski JJ, Lachowski AI, Galas E (1997) Biotechnol Tech 11:9–11

    Article  Google Scholar 

  9. Pierre M, Buisson P, Fache F, Pierre A (2000) Biocatal Biotransform 18:237–251

    Article  Google Scholar 

  10. Soleimani Dorcheh A, Abbasi MH (2008) J Mater Process Technol 199:10–26

    Article  Google Scholar 

  11. Baetens R, Jelle BP, Gustavsen A (2001) Energ Build 43:761–769

    Article  Google Scholar 

  12. Chung MK, Schlaf M (2004) J Am Chem Soc 126:7386–7392

    Article  Google Scholar 

  13. Feinle A, Flaig S, Puchberger M, Schubert U, Hüsing N (2015) Chem Commun 51:2339–2341

    Article  Google Scholar 

  14. Jenningsa AR, McColluma J, Wilkinsa AJ, Mannib SM, Iacono ST (2017) RSC Adv 7:21962–21968

    Article  Google Scholar 

  15. Lermontov SA, Sipyagina NA, Malkova AN, Yarkov AV, Vasil’ev SG, Simonenko NP, Baranchikov AE, Ivanov VK (2016) RSC Adv 6:80766–80772

    Article  Google Scholar 

  16. Rao AV, Bhagat SD, Hirashima H, Pajonk GM (2006) J Colloid Interface Sci 300:279–285

    Article  Google Scholar 

  17. Kavale MS, Mahadik DB, Parale VG, Wagh PB, Gupta SC, Rao AV, Barshilia HC (2011) Appl Surf Sci 258:158–162

    Article  Google Scholar 

  18. Chao X, Jun S, Bin Z (2009) J Non-Cryst Solids 355:492–495

    Article  Google Scholar 

  19. Tamon H, Sone T, Okazaki M (1997) J Colloid Interface Sci 188:162–167

    Article  Google Scholar 

  20. Baumann TF, Gash AE, Chinn SC, Sawvel AM, Maxwell RS, Satcher JH (2005) Chem Mater 17:395–401

    Article  Google Scholar 

  21. Gash AE, Tillotson TM, Satcher JH, Poco JF, Hrubesh LW, Simpson RL (2001) Chem Mater 13:999–1007

    Article  Google Scholar 

  22. Gash AE, Tillotson TM, Satcher Jr JH, Hrubesh LW, Simpson RL (2001) J Non-Cryst Solids 285:22–28

    Article  Google Scholar 

  23. Clapsaddle BJ, Sprehn DW, Gash AE, Satcher JH, Simpson RL (2004) J Non-Cryst Solids 350:173–181

    Article  Google Scholar 

  24. He J, Li X, Su D, Ji H, Zhang X (2016) J Mater Chem A 4:5632–5638

    Article  Google Scholar 

  25. Schubert U (2016) J Sol–Gel Sci Technol 79:249–261

    Article  Google Scholar 

  26. Vioux A (1997) Chem Mater 9:2292–2299

    Article  Google Scholar 

  27. Veith M (2002) Dalton Trans 12:2405–2412

    Article  Google Scholar 

  28. Singh A, Mehrotra RC (2004) Coord Chem Rev 248:101–118

    Article  Google Scholar 

  29. Rupp W, Husing N, Shubert U (2002) J Mater Chem 12:2594–2596

    Article  Google Scholar 

  30. Lermontov S, Malkova A, Yurkova L, Straumal E, Gubanova N, Baranchikov A, Smirnov M, Tarasov V, Buznik V, Ivanov V (2014) J Supercrit Fluid 89:28–32

    Article  Google Scholar 

  31. Lermontov SA, Malkova AN, Yurkova LL, Straumal EA, Gubanova NN, Baranchikov AYe, Ivanov VK (2014) Mater Lett 116:116–119

    Article  Google Scholar 

  32. Lermontov SA, Sipyagina NA, Malkova AN, Yarkov AV, Baranchikov AE, Kozik VV, Ivanov VK (2014) RSC Adv 4:52423–52429

    Article  Google Scholar 

  33. Wang S, Raychaudhuri S, Sarkar (1993) US Pat 5,264,197, 23 Nov 1993

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Acknowledgements

Financial support from the Russian Science Foundation (Grant 14–13-01150, aerogels synthesis, texture properties) is greatly appreciated and Russian Foundation for Basic Research (Grant 16-29-10736, XRD and EDX experiments) is greatly appreciated.

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Authors and Affiliations

  1. Institute of Physiologically Active Compounds of the Russian Academy of Sciences, 1 Severnij pr., Chernogolovka, 142432, Russia

    S. A. Lermontov, A. N. Malkova, N. A. Sipyagina & E. A. Straumal

  2. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences, 31 Leninsky av., Moscow, 119991, Russia

    A. E. Baranchikov & V. K. Ivanov

Authors
  1. S. A. Lermontov
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  2. A. N. Malkova
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  3. N. A. Sipyagina
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  4. E. A. Straumal
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  5. A. E. Baranchikov
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  6. V. K. Ivanov
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Correspondence to S. A. Lermontov.

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Lermontov, S.A., Malkova, A.N., Sipyagina, N.A. et al. Propylene oxide as a new reagent for mixed SiO 2 -based aerogels preparation. J Sol-Gel Sci Technol 84, 377–381 (2017). https://doi.org/10.1007/s10971-017-4429-5

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  • DOI: https://doi.org/10.1007/s10971-017-4429-5

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