Skip to main content
Log in

Roadmap for radioanalytical reference and performance evaluation materials for current and emerging issues

  • Published:
Journal of Radioanalytical and Nuclear Chemistry Aims and scope Submit manuscript

Abstract

Reference materials are fundamental tools for radiochemistry measurements laboratories to establish and evaluate analytical methods, test measurement capabilities, quantify radionuclides, compare analytical results, and establish legal confidence defensibility in measurement results. Over the past decades the focus of low-level environmental reference material producers have adapted to evolving national and international priorities and needs. This document provides a Roadmap of high priority current and future low-level radionuclide Certified Reference and Performance Evaluation Materials that subject-matter experts have identified at NIST and other public workshops (Blueprints) as crucial to metrologists and program directors to address national and international issues.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Daubert v. Merrell Dow Pharmaceuticals, Inc., 509 US 579, 589 (1993)

  2. Hutchinson JMR, Mann WB, Eds (1978) Metrology needs in the measurement of environmental radioactivity. Environment International, 1:7

  3. Hutchinson JMR (1979) Report of the Woods Hole Conference on the Development of Naturally Contaminated Radioactivity Standards—International Committee for Radionuclide Metrology—ICRM Newsletter. Environment International vol 2, p 49

  4. Inn KGW, Kurosaki H, Frechou C, Gilligan C, Jones R, LaMont S, Leggitt J, Li C, McCroan K, Swatski R (2008) A blueprint for radioanalytical metrology CRMs, intercomparisons, and PE. Appl Radiat Isot 66:835–840

    Article  CAS  Google Scholar 

  5. Liggett WS, Inn KGW, Hutchinson JMR (1984) Statistical assessment of sub-sampling procedures. Environ Int 10:143–151

    Article  CAS  Google Scholar 

  6. Lin ZC, Inn KGW, Filliben JJ (2001) An alternative statistical approach for interlaboratory comparison data evaluation. J Radioanal Nucl Chem 248:163–173

    Article  CAS  Google Scholar 

  7. ISO Guide 30 (1992) Terms and definitions used in connection with reference materials. International Organization for Standardization, Geneva

    Google Scholar 

  8. ISO Guide 31 (2000) Reference materials—contents of certificates and labels. International Organization for Standardization, Geneva

    Google Scholar 

  9. ISO Guide 34 (2000) General requirements for the competence of reference material producers. International Organization for Standardization, Geneva

    Google Scholar 

  10. Kramer GH, Inn KGW (1991) A summary of the proceedings of the workshop on standard phantoms for in vivo radioactivity measurement. Health Phys 61:893–895

    Article  CAS  Google Scholar 

  11. Inn KGW, Lin ZC, Liggett WS, Schima FJ, Krey P, Feiner MS, Liu CK, Holloway R, Harvey J, Larsen IL, Beasley T, Huh CA, McCurdy D, Germain P, Yamamoto M, Handl J, Popplewell DS, Woods MJ, Jerome SM, Bates TH, Holmes A, Harvey BR, Odell KJ, Warren BB, Young P (1996) Low-level radioactivity ocean sediment standard reference material. Appl Radiat Isot 47:967–970

    Article  CAS  Google Scholar 

  12. Leggitt J, Inn KGW, Goldberg S, Essex R, LaMont S, Chase S (2009) Nuclear forensics—metrological basis for legal defensibility. J Radioanal Nucl Chem 282:997–1001

    Article  CAS  Google Scholar 

  13. Inn KGW, Johnson CM Jr, Oldham W, Jerome S, Tandon L, Schaaff T, Jones R, Mackney D, MacKill P, Palmer B, Smith D, LaMont S, Griggs J (2013) The urgent requirement for new radioanalytical certified reference materials for nuclear safeguards, forensics, and consequence management. J Radioanal Nucl Chem 296:5–22

    Article  CAS  Google Scholar 

  14. NIST SRM (2015). https://www-s.nist.gov/srmors/browseMaterials.cfm?subkey=19&tableid=131

  15. IAEA CRM (2015). https://nucleus.iaea.org/rpst/ReferenceProducts/ReferenceMaterials/Radionuclides/index.htm

  16. IRMM CRM (2015). https://ec.europa.eu/jrc/sites/default/files/catalogue_nuclear_crm.pdf

  17. NBL CRM (2014). http://science.energy.gov/nbl/certified-reference-materials/

  18. NPL CRM (2015). http://www.npl.co.uk/science-technology/radioactivity/products-and-services/primary-and-secondary-standards

  19. Gascó C, Trinidad JA, Suárez JA, Llauradó M, Valiño F (2012) Evaluación de la intercomparación analítica de radionucleidos en muestras ambientales campaña 2010–2011 (cenizas de alimentos). Consejo de Seguridad Nuclear Report

  20. Korean Rice CRM (2015). http://kcdb.bipm.org/appendixB/appbresults/CCRI(II)-S9/CCRI(II)-S9_Technical_Protoccol.pdf

  21. Wätjen U, Spasova Y, Vasile M, Szántó Z, Emteborg H, Voitsekhovych O (2013) Certification of the reference material IRMM-426 for radionuclides in dried bilberries. Appl Radiat Isot 87:475–479

    Article  Google Scholar 

  22. Minai Y, Miura T, Yonezawa C, Iwamoto H, Shibukawa M, Takagai Y, Furukawa M, Arakawa F, Okada Y, Kakita K, Kojima I, Hirai S (2015) Certified reference materials of agricultural products and foods bearing radioactivity derived from Fukushima Dai-ichi nuclear power plant. Journal of Radioanalytical and Nuclear Chemistry (in press)

  23. Yonezawa C (2015) Preliminary compilation of the International Inter-Comparison Exercise of Fish CRMs. Japan Institute of International Affairs

Download references

Acknowledgments

The authors gratefully acknowledge the subject matter experts that selflessly contributed to the generation of the CRM Blueprints, and the funding agencies that allowed them to attend the workshops.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Kenneth G. W. Inn.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Inn, K.G.W., LaMont, S., Jerome, S. et al. Roadmap for radioanalytical reference and performance evaluation materials for current and emerging issues. J Radioanal Nucl Chem 307, 2529–2538 (2016). https://doi.org/10.1007/s10967-016-4694-8

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10967-016-4694-8

Keywords

Navigation