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Ionic liquid dispersive microextraction and spectrophotometric determination of trace uranyl ion in water samples

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Abstract

In the present study, spectrophotometric determination of uranyl with 2-(5-Bromo-2-pyridylazo)-5-(diethylamino) phenol after ionic liquid based microextraction has been developed. Effect of experimental parameters were optimized to achieve high sensitivity and stability of the complex. The analytical parameters such as linear range (1.33–670 µg L−1), limit of detection (0.97 µg L−1) and enrichment factor (150) were calculated for the method. The relative standard deviation of ten replicate measurement of uranyl was 6.53 and 2.59 % for 66 and 133 µg L−1 uranium, respectively. The proposed method was used to determine the uranyl ions in spiked water samples.

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Acknowledgments

The authors are fully grateful for the financial support of the Unit of the Scientific Research Projects of Cumhuriyet University and Gaziosmanpasa University. Dr. Mustafa Tuzen thanks to Turkish Academy of Sciences for financial support.

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Authors and Affiliations

  1. Faculty of Pharmacy, Cumhuriyet University, 58140, Sivas, Turkey

    Esra Bağda

  2. Chemistry Department, Faculty of Science and Arts, Gaziosmanpasa University, 60250, Tokat, Turkey

    Mustafa Tuzen

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  1. Esra Bağda
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  2. Mustafa Tuzen
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Correspondence to Esra Bağda.

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Bağda, E., Tuzen, M. Ionic liquid dispersive microextraction and spectrophotometric determination of trace uranyl ion in water samples. J Radioanal Nucl Chem 306, 385–392 (2015). https://doi.org/10.1007/s10967-015-4126-1

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  • DOI: https://doi.org/10.1007/s10967-015-4126-1

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