Abstract
A comprehensive and comparative experimental study has been conducted to investigate the effect of thermal-oil ageing on mechanical, thermal and internal structural properties of E-glass fibre/epoxy composite materials. E-glass fibre/epoxy composite specimens were divided into 8 groups according to the certain experimental ageing temperatures. The temperature values were selected as −10, 25, 50, 80, 100, 120 and 140 °C, while the values of the ageing duration were selected as 24, 168, 360, 720 and 1080 h. Thermogravimetric Analysis (TGA) and Differential Thermal Analysis (DTA) tests were performed to determine the thermal properties, tensile tests were used to detect the mechanical properties and a Scanning Electron Microscope (SEM) was used to illustrate the changes in the internal structure of the composites. As a result of this work, unexpectedly no alteration was observed in the mechanical properties of the specimens aged at −10 °C; however, ageing at 120 and 140 °C reduced the maximum load carrying capacities (LCCs) of the specimens especially for further ageing exposure times. Furthermore, the thermal stability of the specimens aged at −10 °C increased with the increasing thermal ageing duration while, for the other thermal ageing temperatures, the thermal stability showed a decreasing trend as the thermal ageing exposure time increased.
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Jahanian E, Zeinedini A (2018) Influence of drilling on mode II delamination of E-glass/epoxy laminated composites. Theor Appl Fract Mech 96:398–407. https://doi.org/10.1016/j.tafmec.2018.06.002
Yilmaz C, Akalin C, Gunal I, Celik H, Buyuk M, Suleman A, Yildiz M (2018) A hybrid damage assessment for E-and S-glass reinforced laminated composite structures under in-plane shear loading. Compos Struct 186:347–354. https://doi.org/10.1016/j.compstruct.2017.12.023
Hu H, Gao G, Hong S et al (2018) The influence of topology and morphology of fillers on the conductivity and mechanical properties of rubber composites. J Polym Res 25:87. https://doi.org/10.1007/s10965-018-1478-6
Mohamed M, El-Maghraby A, El-Latif MA et al (2013) Fe-Ni alloy/polyamide 6 nanocomposites: effect of nanocrystalline metal particles on the mechanical and physical properties of the polymer. J Polym Res 20(6):137. https://doi.org/10.1007/s10965-013-0137-1
Lou CW, Huang CL, Pan YJ et al (2016) Crystallization, mechanical, and electromagnetic properties of conductive polypropylene/SEBS composites. J Polym Res 23:84. https://doi.org/10.1007/s10965-016-0979-4
Tsotsis TK (1995) Thermo-oxidative aging of composite materials. J Compos Mater 29(3):410–422. https://doi.org/10.1177/002199839502900307
Zhang D, He M, He W et al (2017) Influence of thermo-oxidative ageing on the thermal and dynamical mechanical properties of long glass fibre-reinforced poly(butylene terephthalate) composites filled with dopo. Mater (Basel) 10:500. https://doi.org/10.3390/2Fma10050500
Kruželák J, Sýkora R, Hudec I (2015) Influence of mixed sulfur/peroxide curing system and thermo-oxidative ageing on the properties of rubber magnetic composites. J Polym Res 22:636. https://doi.org/10.1007/s10965-014-0636-8
Fan W, Li J, Zheng Y et al (2016) Influence of thermo-oxidative aging on the thermal conductivity of carbon fiber fabric reinforced epoxy composites. Polym Degrad Stab 123:162–169. https://doi.org/10.1016/j.polymdegradstab.2015.11.016
Daily C, Barnard DJ, Jones R et al (2016) Dielectric and infrared inference of thermo-oxidative aging of a bismaleimide composite material. Compos Part B 101:167–175. https://doi.org/10.1016/j.compositesb.2016.06.004
Barbosa AP, Fulco AP, Guerra ESS et al (2017) Accelerated aging effects on carbon fiber/epoxy composites. Compos Part B 110:298–306. https://doi.org/10.1016/j.compositesb.2016.11.004
Buch X, Shanahan MER (2000) Thermal and thermo-oxidative ageing of an epoxy adhesive. Polym Degrad Stab 68:403–411. https://doi.org/10.1016/S0141-3910(00)00028-8
Akderya T, Kemiklioglu U, Sayman O (2016) Effects of thermal ageing and impact loading on tensile properties of adhesively bonded fibre/epoxy composite joints. Compos Part B 95:117–122. https://doi.org/10.1016/j.compositesb.2016.03.073
Rudzinski S, Häussler L, Harnisch C et al (2011) Glass fibre reinforced polyamide composites: thermal behaviour of sizings. Compos Part A 42:157–164. https://doi.org/10.1016/j.compositesa.2010.10.018
Barjasteh E, Bosze EJ, Tsai YI et al (2009) Thermal aging of fiberglass/carbon-fiber hybrid composites. Compos A 40:2038–2045. https://doi.org/10.1016/j.compositesa.2009.09.015
Boubakri A, Haddar N, Elleuch K et al (2011) Influence of thermal aging on tensile and creep behavior of thermoplastic polyurethane. CR Mecanique 339:666–673. https://doi.org/10.1016/j.crme.2011.07.003
Karsli NG, Demirkol S, Yilmaz T (2016) Thermal aging and reinforcement type effects on the tribological, thermal, thermomechanical, physical and morphological properties of poly(ether ether ketone) composites. Compos Part B 88:253–263. https://doi.org/10.1016/j.compositesb.2015.11.013
Kwon D, Shin P, Kim J et al (2017) Interfacial properties and thermal aging of glass Fiber/epoxy composites reinforced with SiC and SiO2 nanoparticles. Compos Part B 130:46–53. https://doi.org/10.1016/j.compositesb.2017.07.045
Shaoquan W, Shangli D, Yub G et al (2017) Thermal ageing effects on mechanical properties and barely visible impact damage behavior of a carbon fiber reinforced bismaleimide composite. Mater Des 115:213–223. https://doi.org/10.1016/j.matdes.2016.11.062
Scida D, Assarar M, Poilâne C et al (2013) Influence of hygrothermal ageing on the damage mechanisms of flax-fibre reinforced epoxy composite. Compos Part B 48:51–58. https://doi.org/10.1016/j.compositesb.2012.12.010
Islam MS, Pickering KL, Foreman NJ (2010) Influence of hygrothermal ageing on the physico mechanical properties of alkali treated industrial hemp fibre reinforced polylactic acid composites. J Polym Environ 18:696–704. https://doi.org/10.1007/s10924-010-0225-9
Anstice PD, Beaumont PWR (1983) Hygrothermal ageing and fracture of glass fibre--epoxy composites. J Mater Sci 18:3404–3408. https://doi.org/10.1007/BF00544167
Valentin D, Paray F, Guetta B (1987) The hygrothermal behaviour of glass fibre reinforced Pa66 composites: a study of the effect of water absorption on their mechanical properties. J Mater Sci 22:46–56. https://doi.org/10.1007/BF01160550
Hu Y, Lang AW, Li X et al (2014) Hygrothermal aging effects on fatigue of glass fiber/polydicyclopentadiene composites. Polym Degrad Stab 110:464–472. https://doi.org/10.1016/j.polymdegradstab.2014.10.018
Rocha IBCM, Raijmaekers S, Nijssen RPL et al (2017) Hygrothermal ageing behaviour of a glass/epoxy composite used in wind turbine blades. Compos Struct 174:110–122. https://doi.org/10.1016/j.compstruct.2017.04.028
Jiang X, Kolstein H, Bijlaard F et al (2014) Effects of hygrothermal aging on glass-fibre reinforced polymer laminates and adhesive of FRP composite bridge: moisture diffusion characteristics. Compos Part A: 57:49–58. https://doi.org/10.1016/j.compositesa.2013.11.002
Foulca MP, Bergereta A, Ferrya L et al (2005) Study of hygrothermal ageing of glass fibre reinforced PET composites. Polym Degrad Stab 89:461–470. https://doi.org/10.1016/j.polymdegradstab.2005.01.025
Berketis K, Tzetzis D (2009) Long-term water immersion ageing characteristics of GFRP composites. J Mater Sci 44(13):3578–3588. https://doi.org/10.1007/s10853-009-3485-9
Ksouri I, De Almeida O, Haddar N (2017) Long term ageing of polyamide 6 and polyamide 6 reinforced with 30% of glass fibers: physicochemical, mechanical and morphological characterization. J Polym Res 24:133. https://doi.org/10.1007/s10965-017-1292-6
Klasztorny M, Nycz DB, Romanowski RK et al (2017) Effects of operating temperatures and accelerated environmental ageing on the mechanical properties of a glassvinylester composite. Mech Compos Mater 53(3):335–350. https://doi.org/10.1007/s11029-017-9665-9
Nicholas J, Mohamed M, Dhaliwal GS et al (2016) Effects of accelerated environmental aging on glass fiber reinforced thermoset polyurethane composites. Compos Part B 94:370–378. https://doi.org/10.1016/j.compositesb.2016.03.059
Guzmán E, Cugnoni J, Gmür T (2014) Multi-factorial models of a carbon fibre/epoxy composite subjected to accelerated environmental ageing. Compos Struct 111:179–192. https://doi.org/10.1016/j.compstruct.2013.12.028
Fitriah SN, Abdul Majid MS, Ridzuan MJM et al (2017) Influence of hydrothermal ageing on the compressive behaviour of glass fibre/epoxy composite pipes. Compos Struct 159:350–360. https://doi.org/10.1016/j.compstruct.2016.09.078
HUNTSMAN - Advanced Materials - Selector guide for composite resin systems. http://www.huntsman.com/advanced_materials/Media%20Library/global/files/EUR_Composites%20-%20Composite%20Resin_Araldite_Epoxy_RTM.pdf Accessed 29 March 2018
ASTM D3039 / D3039M-14, Standard Test Method for Tensile Properties of Polymer Matrix Composite Materials, ASTM International, West Conshohocken, PA, 2014, www.astm.org Accessed 29 March 2018
FUCHS – Product Information – Renolin Therm 320 Heat transfer fluid. http://www.lukoilmarine.com/files/getfile/oil_grade_model/pdf/79/146003929992/ Accessed 29 March 2018
Akderya T, Sayman O, Kemiklioğlu U et al (2018) A comparative study on effects of thermal fatigue caused by thermal-oil cycling on tensile properties of single lap composite joints bonded with different kinds of adhesives. J Adhes. https://doi.org/10.1080/00218464.2018.1440213
Akderya T, Çevik M, Sayman O (2018) Influence of thermal ageing on tensile performance of E-glass fibre/epoxy composite joints bonded with a diverse set of adhesives. J Adhes. https://doi.org/10.1080/00218464.2018.1480371
Liu X, Zhao J, Yang R et al (2018) Effect of lubricating oil on thermal aging of nitrile rubber. Polym Degrad Stab 151:136–143. https://doi.org/10.1016/j.polymdegradstab.2018.03.004
DIN EN ISO 3104 - Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity (ISO/DIS 3104:2017); German and English version pr EN ISO 3104:2017. https://www.din.de/en/getting-involved/standards-committees/nmp/drafts/wdc-beuth:din21:279196067 Accessed 29 March 2018
DIN 51757 - Testing of mineral oils and related materials - Determination of density. https://www.din.de/en/getting-involved/standards-committees/nmp/standards/wdc-beuth:din21:136322149 Accessed 29 March 2018
ASTM D1500–12, Standard Test Method for ASTM Color of Petroleum Products (ASTM Color Scale), ASTM International, West Conshohocken, PA, 2012, www.astm.org Accessed 29 March 2018
DIN EN ISO 2592 - Petroleum and related products - Determination of flash and fire points - Cleveland open cup method (ISO/DIS 2592:2016); German and English version pr EN ISO 2592:2016 https://www.din.de/en/getting-involved/standards-committees/nmp/drafts/wdc-beuth:din21:247493569 Accessed 29 March 2018
DIN ISO 3016 - Petroleum products - Determination of pour point (ISO 3016:1994). https://www.din.de/en/getting-involved/standards-committees/nmp/standards/wdc-beuth:din21:278983355 Accessed 29 March 2018
Bowles KJ (2000) Thermal and mechanical durability of graphite fibre reinforced PMR-15 composites at elevated temperatures. Revol Mater Technol Econom 32
Ksouri I, Haddar N (2018) Long term ageing of polyamide 6 and polyamide 6 reinforced with 30% of glass fibers: temperature effect. J Polym Res 25:153. https://doi.org/10.1007/s10965-018-1551-1
Bennehalli B, Venkateshappa SC, Punyamurthy RD et al (2017) Influence of surface modification on the thermal stability and percentage of crystallinity of natural abaca fiber. Handbook of Composites from Renewable Materials, Scrivener Publishing, Beverly, Massachusetts. https://doi.org/10.1002/9781119441632.ch117/summary
Milanese AC, Cioffi MOH, Voorwald HJC (2012) Thermal and mechanical behaviour of sisal/phenolic composites. Compos Part B 43:2843–2850. https://doi.org/10.1016/j.compositesb.2012.04.048
Anbukarasi K, Kalaiselvam S (2015) Study of effect of fibre volume and dimension on mechanical, thermal, and water absorption behaviour of luffa reinforced epoxy composites. Mater Des 66:321–330. https://doi.org/10.1016/j.matdes.2014.10.078
Monteiro SN, Calado V, Rodriguez RJS et al (2012) Thermogravimetric behavior of natural fibers reinforced polymer composites - an overview. Mater Sci Eng A 557:17–28. https://doi.org/10.1016/j.msea.2012.05.109
Ramnath BV, Kokan SJ, Raja RN et al (2013) Evaluation of mechanical properties of abaca–jute–glass fibre reinforced epoxy composite. Mater Des 51:357–366. https://doi.org/10.1016/j.matdes.2013.03.102
Elkhaoulani A, Arrakhiz FZ, Benmoussa K et al (2013) Mechanical and thermal properties of polymer composite based on natural fibers: Moroccan hemp fibers/polypropylene. Mater Des 49:203–208. https://doi.org/10.1016/j.matdes.2013.01.063
Tanobe V, Sydenstricker THD, Munaro M et al (2005) A comprehensive characterization of chemically treated Brazilian sponge-gourds (Luffa cylindrica). Polym Test 24:474–482. https://doi.org/10.1016/j.polymertesting.2004.12.004
Aji IS, Zainudin ES, Khalina A et al (2012) Thermal property determination of hybridized kenaf/PALF reinforced HDPE composite by thermogravimetric analysis. J Therm Anal Calorim 109:893–900. https://doi.org/10.1007/s10973-011-1807-z
Mahmud CK, Haque Md A, Chowdhury AMS et al (2014) Preparation and characterization of polyester composites reinforced with bleached, Diospyros perigrina (Indian persimmon) treated and unbleached jute mat. J Adv Chem Eng 4:114. https://doi.org/10.4172/2090-4568.1000114
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The authors would like to acknowledge the support of Izmir Katip Çelebi University Scientific Research Projects Coordinatorship under Grant no. 2017-TDR-FEBE-0030. All authors are truly grateful for the support.
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Akderya, T., Çevik, M. Investigation of thermal-oil environmental ageing effect on mechanical and thermal behaviours of E-glass fibre/epoxy composites. J Polym Res 25, 214 (2018). https://doi.org/10.1007/s10965-018-1615-2
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DOI: https://doi.org/10.1007/s10965-018-1615-2