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A new metal–organic framework based on 4,4′-bibenzoic acid-2,2′-sulfone: synthesis, crystal structure and magnetic property

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Abstract

A new metal–organic framework (MOF), namely, {[Ni(BPS)(4,4′-bipy)]n}, (BPS = 4,4′-bibenzoic acid-2,2′-sulfone, bipy = 4,4-Bipyridine) (1), with 3D framework has been synthesized under solvothermal condition and characterized by single crystal X-ray diffraction, PXRD, TGA, FT-IR and SQUID magnetometry. Topological analysis indicates that 1 is a 3D (3,5)-connected framework with the short point symbol of (63)(67·83). The magnetic experiments reveal that 1 exhibits typical ferromagnetic exchange in Ni(II) ions.

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Acknowledgements

We are grateful for the financial support from the Science and Technology Research Projects of the Education Department of Jiangxi Province (No. GJJ190887). University-level Optional Project of Shangrao Normal University (201906)

Funding

This research was supported by the Science and Technology Research Projects of the Education Department of Jiangxi Province (No. GJJ190887). University-level Optional Project of Shangrao Normal University (201,906).

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Authors and Affiliations

  1. College of Chemistry and Environmental Science, Shangrao Normal University, Shangrao, 334001, JiangXi Province, People’s Republic of China

    Shixian Xu, Xi Chen, Li Qi, Feng Zhu, Linhai Liu, Lixia Quan & Jiurong Hu

  2. State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals, Lanzhou University of Technology, Lanzhou, 730050, People’s Republic of China

    Ming Zhong

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  1. Shixian Xu
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  2. Xi Chen
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  3. Li Qi
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  4. Feng Zhu
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  5. Linhai Liu
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  7. Jiurong Hu
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  8. Ming Zhong
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Correspondence to Shixian Xu or Ming Zhong.

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Xu, S., Chen, X., Qi, L. et al. A new metal–organic framework based on 4,4′-bibenzoic acid-2,2′-sulfone: synthesis, crystal structure and magnetic property. J Porous Mater 28, 481–486 (2021). https://doi.org/10.1007/s10934-020-01002-y

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