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Hydrothermal Synthesis, Structures and Luminescent of 1D Lanthanide–Metal Organic Frameworks Based on Rigid 5-Nitroisophthalic Acid Linker

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Abstract

1D coordination chain frameworks of [Eu(NIPH)(BDCA)(H2O)2]2(H2O)5 (1), [Sm(NIPH)(BDCA)(H2O)2] (2), [Dy(NIPH)(BDCA)(H2O)2]2 (3), [Gd(HNIPH)(BDCA)(H2O)2](H2O)0.5 (4), [Ce(HNIPH)(BDCA)(H2O)2](H2O)0.5 (5), [Nd(HNIPH)(BDCA)(H2O)2](H2O)0.5 (6), [Dy(NIPH)(ox)0.5(H2O)3](H2O)2 (7) [Er2(NIPH)(ox)0.5(H2O)3](H2O)2 (8), [Y2(NIPH)(ox)0.5(H2O)3](H2O)2 (9), [Eu2(NIPH)(ox)0.5(H2O)3](H2O)2 (10) (H2NIPH = 5-nitroisophthalic acid, H2DBCA = biphenyl-2,2′-dicarboxylic acid, ox = oxalic acid) were synthesized by hydrothermal reaction and characterized by single-crystal X-ray diffraction. These compounds were constructed of [Ln2O2] dimers bridged through the carboxylate groups of H2NIPH ligands. These compounds contain an -Ln–O–C–O–Ln- zigzag chain, which connect to each other through the oxygen atoms of the H2NIPH ligands to form a wave-like layer. In addition, when accretion equiv [Bu4N]F at room temperature the compound 1 emission enhancement.

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Acknowledgments

This work was supported by the NSF of Guangxi Province (No. 2012GXNSFAA053031), the Innovation Project of Guangxi University for Nationalities (No. gxun-chx2013096), Guangxi Department of Education (201203YB071), the open fund of Key Laboratory of Guangxi Key laboratory of Chemistry and Engineering of Forest Products (No. GXFC13-08), the national college students’ innovative entrepreneurial training program (No. 201410608015) and the college students’ innovative entrepreneurial training program of Guangxi Province (No. 201410608051).

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Authors and Affiliations

  1. College of Chemistry and Chemical Engineering, Guangxi University for Nationalities, Nanning, 530006, People’s Republic of China

    Shu-Long Wang, Fen Jiang, Man-Yan Huang, Chang-Wei Xiang & Qin Huang

  2. College of Chemistry and Materials, Yulin Normal University, Yulin, 537000, People’s Republic of China

    Fei-Long Hu

  3. Guangxi Key Laboratory of Chemistry and Engineering of Forest Products, Nanning, 530006, People’s Republic of China

    Qin Huang

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Correspondence to Qin Huang.

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Wang, SL., Hu, FL., Jiang, F. et al. Hydrothermal Synthesis, Structures and Luminescent of 1D Lanthanide–Metal Organic Frameworks Based on Rigid 5-Nitroisophthalic Acid Linker. J Inorg Organomet Polym 25, 551–558 (2015). https://doi.org/10.1007/s10904-014-0115-z

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