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Electrical, optical and high energy radiation shielding study of TMI-doped multi-component glasses

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Abstract

Barium-boro-bismuthate glass system having composition xMoO3-(10−x)V2O5-25BaO-20B2O3-45Bi2O3 (where x = 0.0, 1.0, 3.0, 5.0 and 8.0 mol%) were prepared through melt-quench technique and studied their electrical, optical and thermal behaviour. The analysis of frequency and temperature-dependent curves of dielectric parameters and ac conductivity for all prepared compositions, suggests their usability in energy storage, semiconducting and non-linear opto-electronic applications. Optical parameters, such as indirect allowed band gap, refractive index and Urbach energy for as-synthesized and annealed glasses (annealed at 723 K for 5 h) were calculated using UV–Vis optical absorption spectra. A small increase in indirect optical band-gap values (i.e. from 1.89 to 2.16 eV) with increasing molybdenum content, suggests a decrease in localized states inside band-gap. Small change in values of refractive indices after annealing indicates transparent glass ceramic nature of all annealed glass samples. Characteristic temperatures including glass transition (Tg ~ 405 °C) and peak crystallization (Tc ~ 450 °C) for glass samples were identified from Differential Thermal Analysis (DTA) curve. Gamma ray shielding ability of glasses was investigated through Phy-X/PSD program. Shielding parameters, including mass attenuation coefficient (μm), half value layer (HVL), mean free path (MFP), effective atomic number (Zeff) suggests their usability for gamma ray shielding and nuclear waste storage purposes in nuclear reactors. As per HVL parameter, 3-cm-thick glass layer of prepared samples can diminish the intensity of incident radiations to half of its initial value.

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Data availability

The datasets generated or analyzed during the current study are available from the corresponding author on reasonable request. The datasets are presented in the main manuscript.

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Acknowledgements

Authors are thankful to Department of Science and Technology (DST) Delhi, for providing experimental support facilities under FIST Research Grant (Sanction Order No. & Date: SR/FST/PS-1/2018/32). Author Vikas is thankful to UGC, New Delhi for providing financial assistance under JRF Fellowship F. No.-16-9(June 2018)/2019(NET/CSIR).

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No funding was received to assist with preparation of this manuscript. The authors declare they have no financial interest.

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Authors and Affiliations

  1. Department of Physics, Deenbandhu Chhotu Ram University of Science and Technology, Murthal, Haryana, India

    Vikas Attri, M. S. Dahiya, Ashima Hooda & Satish Khasa

  2. Directorate of Education, Govt. of NCT, Delhi, India

    M. S. Dahiya

  3. Central University of Haryana, Mahendragarh, Haryana, India

    Rakesh Kumar

  4. Department of Physics, Guru Jambheswer University of Science and Technology, Hisar, Haryana, India

    A. Agarwal

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  1. Vikas Attri
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The authors confirm their contribution to this article as follows: VA: Conceptualization, Methodology, Validation, Formal analysis, Investigation, Data Curation, Writing—Original Draft, Visualization. RK: Methodology, Data Curation. MSD: Formal analysis, Data Curation,Writing—Review & Editing, AH: Resources,Writing—Review & Editing, AA: Resources,Writing—Review & Editing. SK: Resources,Visualization, Validation,Writing—Review & Editing, Supervision, Project administration.

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Correspondence to Satish Khasa.

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Attri, V., Dahiya, M.S., Kumar, R. et al. Electrical, optical and high energy radiation shielding study of TMI-doped multi-component glasses. J Mater Sci: Mater Electron 34, 1273 (2023). https://doi.org/10.1007/s10854-023-10625-1

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