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Fabrication of Z-scheme Bi5O7I/MIL-53(Fe) hybrid with improved photocatalytic performance under visible light irradiation

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Abstract

A series of Bi5O7I/MIL-53(Fe) (BOI/MIL-w) composites were successfully prepared by a facile in-situ solvothermal approach. The matched energy bands enabled Bi5O7I and MIL-53(Fe) to form a Z-scheme heterojunction which resulted in an efficient separation of the photo-induced electron–hole pairs. The photocatalytic activity of BOI/MIL-w was evaluated by the degradation of Rhodamine B (RhB) in water under the visible light irradiation. Compared with Bi5O7I, photocatalytic performances of BOI/MIL-w notably boosted. When the content of added MIL-53(Fe) was 3 wt%, BOI/MIL-3 presented the highest activity with a degradation efficiency of 99.7% only after 60 min of irradiation. The reaction rate constant k could reach 0.0992 min−1 which was nearly 12.6 times as high as that of Bi5O7I. Moreover, BOI/MIL-w had a good stability and reusability, which could ensure its practical application. Trapping experiments confirmed that h+ and ·O2− were the dominant active species during the photocatalytic process, and further demonstrated the formation of the Z-scheme heterojunction facilitated the photocatalytic performance of BOI/MIL-w.

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Acknowledgements

The authors gratitude for the support from the Nation Natural Science Foundation of China (Grant No. 51273155) and the Fundamental Research Funds for the Central Universities (Grant Nos. 2018-IB-025 and 2019-IB-004).

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  1. Nan Zhou and Junjie Tan have contributed equally to this work.

Authors and Affiliations

  1. School of Chemistry, Chemical Engineering and Life Science, Wuhan University of Technology, Wuhan, 430070, People’s Republic of China

    Nan Zhou, Junjie Tan, Xi Li, Lu Wang, Chenglong Jin, Ming Chen, Zhengsong Yu, Yani Liang, Zhidong Qiu, Wenlong Li, Yulin Dong, Zhizhong Xie, Yawei Lin & Deyu Qu

  2. School of Materials Science and Engineering, Wuhan University of Technology, Wuhan, 430070, People’s Republic of China

    Chaocan Zhang

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Zhou, N., Tan, J., Li, X. et al. Fabrication of Z-scheme Bi5O7I/MIL-53(Fe) hybrid with improved photocatalytic performance under visible light irradiation. J Mater Sci: Mater Electron 31, 4822–4835 (2020). https://doi.org/10.1007/s10854-020-03044-z

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