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Facile one-step synthesis of PI/Fe3O4 composite microspheres from poly(amic acid) triethylamine salts and Fe(III) ion

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Abstract

Polyimide/magnetite composite microspheres were successfully prepared from poly(amic acid) triethylamine salts and Fe(III) ion via a simple one-step solvothermal process. The formation mechanism of the composite microspheres was explored. The morphology and the structure of the samples were characterized. It was found that polyimide has successfully coated on the surface of the magnetite microspheres and penetrated throughout the crystals via an assembly process. And the magnetic and thermal properties were measured, the results showing that composite microspheres have excellent thermal stabilities and the saturation magnetization is 35.29 emu/g with PI content of 60 wt%.

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Acknowledgments

This work was supported by Yorth Science Foundation of Heilongjiang Province, China (Grant No. QC2014C008), Science Foundation of Heilongjiang Academy of Sciences, China (Nos. 2014-YQ-01, 2015-YX-02 and 2015-YQ-08).

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Authors and Affiliations

  1. School of Material Science and Engineering, Harbin University of Science and Technology, Harbin, 150000, China

    Haoran Zhou & Weimiao Yu

  2. Institute of Petrochemistry, Heilongjiang Academy of Science, Harbin, 150000, China

    Chunyan Qu, Changwei Liu & Dezhi Wang

  3. Institude of Advanced Technology, Heilongjiang Academy of Sciences, Harbin, 150000, China

    Chunyan Qu

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  1. Haoran Zhou
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  2. Weimiao Yu
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  3. Chunyan Qu
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  4. Changwei Liu
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  5. Dezhi Wang
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Correspondence to Haoran Zhou or Changwei Liu.

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Zhou, H., Yu, W., Qu, C. et al. Facile one-step synthesis of PI/Fe3O4 composite microspheres from poly(amic acid) triethylamine salts and Fe(III) ion. J Mater Sci: Mater Electron 26, 9789–9794 (2015). https://doi.org/10.1007/s10854-015-3650-7

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  • DOI: https://doi.org/10.1007/s10854-015-3650-7

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