Skip to main content
SpringerLink
Log in

Synthesis, characterization, and morphological control of Na1/2Bi1/2Cu3Ti4O12 through modify sol–gel method

  • Published:
Journal of Materials Science: Materials in Electronics Aims and scope Submit manuscript

Abstract

This paper describes the synthesis of Na1/2Bi1/2Cu3Ti4O12 (BNCTO) with different morphologies like nanoparticles, micro cubic, and micro sheet structure prepared by modify sol–gel method, using different surfactants (SDS, CTAB, PVP, and PVA). This study aimed to investigate the effects of different surfactant such as SDS, CTAB, PVP, and PVA and chelating agent on the morphology and particle size of final products. It was found that the size and morphology of the products could be greatly influenced by the aforementioned parameters. To our knowledge, this is the first report on the synthesis of Na1/2Bi1/2Cu3Ti4O12 nanostructure with different morphologies in the presence of salicylic acid as a chelating agent. The as-synthesized products were characterized by powder X-ray diffraction, scanning electronic microscopy, ultraviolet–visible, and energy dispersive spectrometry analysis of X-ray techniques.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. H. Zeynali, H. Akbari, R.K. Ghasabeh, Y. Azizian-Kalandaragh, S.M. Hosseinpour-Mashkani, J. Supercond. Nov. Magn. 26, 713 (2012)

    Article  Google Scholar 

  2. R. Dittmer, E.M. Anton, W. Jo, H. Simons, J.E. Daniels, M. Hoffman, J. Pokorny, I.M. Reaney, J. Rodel, J. Am. Ceram. Soc. 1–6, 3519 (2012)

    Article  Google Scholar 

  3. H. Zeynali, S.B. Mousavi, S.M. Hosseinpour-Mashkani, Mater. Lett. 144, 65 (2015)

    Article  Google Scholar 

  4. A. Javidan, S. Rafizadeh, S.M. Hosseinpour-Mashkani, Mater. Sci. Semicond. Process. 27, 468 (2014)

    Article  Google Scholar 

  5. C.C. Homes, T. Vogt, S.M. Shapiro, S. Wakimoto, A.P. Ramirez, Science 293, 673 (2001)

    Article  Google Scholar 

  6. M.A. Subramanian, L. Dong, N. Duan, B.A. Reisner, A.W. Sleight, J. Solid State Chem. 151, 323 (2000)

    Article  Google Scholar 

  7. A.P. Ramirez, M.A. Subramanian, M. Gardel, G. Blumberg, D. Li, T. Vogt, S.M. Shapiro, Solid State Commun. 115, 217 (2000)

    Article  Google Scholar 

  8. M.C. Ferrarelli, T.B. Adams, A. Feteira, D.C. Sinclair, A.R. West, Appl. Phys. Lett. 89, 212904 (2006)

    Article  Google Scholar 

  9. C. Masingboon, S. Maensiri, T. Yamwong, P.L. Anderson, S. Seraphin, Appl. Phys. A 91, 87 (2008)

    Article  Google Scholar 

  10. M.A. Subramanian, D. Li, N. Duan, B.A. Reisner, A.W. Sleight, J. Solid State Chem. 151, 323 (2000)

    Article  Google Scholar 

  11. A.P. Ramirez, M.A. Subramanian, M. Gardel, G. Blumberg, D. Li, T. Vogt, S.M. Shapiro, Solid State Commun. 115, 217 (2000)

    Article  Google Scholar 

  12. C.C. Holmes, T. Vogt, S.M. Shapiro, S. Wakimoto, A.P. Ramirez, Science 293, 637 (2001)

    Google Scholar 

  13. D.C. Sinclair, T.B. Adams, F.D. Morrison, A.R. West, Appl. Phys. Lett. 80, 2153 (2002)

    Article  Google Scholar 

  14. S.Y. Chung, I.L.D. Kim, S.J.L. Kang, Nat. Mater. 3, 774 (2004)

    Article  Google Scholar 

  15. R.K. Grubbs, E.L. Venturini, P.G. Clem, J.J. Richardson, B.A. Tuttle, G.A. Samara, Phys. Rev. B 72, 104111 (2005)

    Article  Google Scholar 

  16. T.T. Fang, H.K. Shiau, J. Am. Ceram. Soc. 87, 2072 (2004)

    Article  Google Scholar 

  17. T.B. Adams, D.C. Sinclair, A.R. West, Adv. Mater. (Weinheim, Germany) 14, 1321 (2002)

    Article  Google Scholar 

  18. J. Li, M.A. Subramanian, H.D. Rosenfeld, C.Y. Jones, B.H. Toby, A.W. Sleight, Chem. Mater. 16, 5223 (2004)

    Article  Google Scholar 

  19. S.M. Hosseinpour-Mashkani, M. Ramezani, M. Vatanparast, Mater. Sci. Semicond. Process. 26, 112 (2014)

    Article  Google Scholar 

  20. S.M. Hosseinpour-Mashkani, M. Ramezani, Mater. Lett. 130, 259 (2014)

    Article  Google Scholar 

  21. M. Zheng, R. Yu, J. Chen, J. Zhao, G. Liu, X. Xing, J. Meng, J. Am. Ceram. Soc. 91, 544 (2008)

    Article  Google Scholar 

Download references

Acknowledgments

Authors are grateful to council of University of Arak for providing financial support to undertake this work.

Author information

Authors and Affiliations

  1. Department of Chemistry, Arak Branch, Islamic Azad University, Arak, Iran

    Majid Ramezani

  2. Young Researchers and Elites Club, Arak Branch, Islamic Azad University, Arak, Iran

    Ali Sobhani-Nasab & S. Mostafa Hosseinpour-Mashkani

Authors
  1. Majid Ramezani
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Ali Sobhani-Nasab
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. S. Mostafa Hosseinpour-Mashkani
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to S. Mostafa Hosseinpour-Mashkani.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Ramezani, M., Sobhani-Nasab, A. & Hosseinpour-Mashkani, S.M. Synthesis, characterization, and morphological control of Na1/2Bi1/2Cu3Ti4O12 through modify sol–gel method. J Mater Sci: Mater Electron 26, 4848–4853 (2015). https://doi.org/10.1007/s10854-015-2992-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10854-015-2992-5

Keywords

Search

Navigation