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A Simple Method to Evaluate the Purity of Synthetic Hydroxyapatite Granules

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Journal of Applied Spectroscopy Aims and scope

Using a method based on the spectrophotometric analysis of the liquids remaining after washing ceramic granules, the type of impurity was determined, the wavelength for measuring the impurity was established, and the type of cuvette (polystyrene or quartz) was analyzed. The absorbance of the samples was measured at wavelengths between 190 and 1100 nm. The results showed that both cuvette types are useful; however, the greatest absorbances were detected using quartz ones at low wavelengths around 190 nm. The comparison of absorption spectra from the samples, centrifuged and noncentrifuged, enabled us to define the impurities as small apatite particles.

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References

  1. Z. Shi, X. Huang, Y. Cai, R. Tang, and D. Yang, Acta Biomater., 5, 338–345 (2009).

    Article  Google Scholar 

  2. M. Motskin, D. M. Wright, K. Muller, N. Kyle, T. G. Gard, A. E. Porter, and J. N. Skepper, Biomaterials, 30, 3307–3317 (2009).

    Article  Google Scholar 

  3. M. F. Hsieh, L. H. Perng, T. S. Chin, and H. G. Perng, Biomaterials, 22, 2601–2607 (2001).

    Article  Google Scholar 

  4. A. Jillavenkatesa and R. A. Condrate Sr., J. Mater. Sci., 33, 4111–4119 (1998).

    Article  ADS  Google Scholar 

  5. S. Sakai, T. Anada, K. Tsuchiya, H. Yamazaki, H.C. Margolis, and O. Suzuki, Dent. Mater. J., 35, 216–224 (2016).

    Article  Google Scholar 

  6. A. Sroka-Bartnicka, L. Borkowski, G. Ginalska, A. Slosarczyk, and S.G. Kazarian, Spectrochim. Acta A, 171, 155–161 (2017).

    Article  ADS  Google Scholar 

  7. A. Slosarczyk, Z. Paszkiewicz, and C. Paluszkiewicz, J. Mol. Struct., 744, 657–661 (2005).

    Article  ADS  Google Scholar 

  8. L. Borkowski, A. Sroka-Bartnicka, P. Draczkowski, A. Ptak, E. Zieba, A. Slosarczyk, and G. Ginalska, Mat. Sci. Eng. C: Mater., 62, 260–267 (2016).

    Article  Google Scholar 

  9. M. Kazanci, P. Fratzl, K. Klaushofer, and E. P. Paschalis, Calcified Tissue Int., 79, 354–359 (2006).

    Article  Google Scholar 

  10. I. Mobasherpour, M.S. Heshajin, A. Kazemzadeh, and M. Zakeri, J. Alloy Compd., 430, 330–333 (2007).

    Article  Google Scholar 

  11. A. Farzadi, F. Bakhshi, M. Solati-Hashjin, M. Asadi-Eydivand, and N. A. Osman, Ceram. Int., 40, 6021–6029 (2014).

    Article  Google Scholar 

  12. K. P. Tank, P. Sharma, D. K. Kanchan, and M. J. Joshi, Cryst. Res. Technol., 46, 1309–1316 (2011).

    Article  Google Scholar 

  13. S. Joschek, B. Nies, R. Krotz, and A. Gopferich, Biomaterials, 21, 1645–1658 (2000).

    Article  Google Scholar 

  14. A. Stoch, W. Jastrzebski, E. Długon, W. Lejda, B. Trybalska, G. J. Stoch, and A. Adamczyk, J. Mol. Struct., 744, 633–640 (2005).

    Article  ADS  Google Scholar 

  15. K. A. Hing, S. M. Best, and W. Bonfield, J. Mater. Sci.: Mater., 10, 135–145 (2005).

    Google Scholar 

  16. Y. Shen, J. Liu, K. Lin, and W. Zhang, Mater. Lett., 70, 76–79 (2012).

    Article  Google Scholar 

  17. R. N. Panda, M. F. Hsieh, R. J. Chung, and T. S. Chin, J. Phys. Chem. Solids, 64, 193–199 (2003).

    Article  ADS  Google Scholar 

  18. C. Jäger, T. Welzel, W. Meyer-Zaika, and M. Epple, Magn. Reson. Chem., 44, 573–580 (2006).

    Article  Google Scholar 

  19. A. K. Nayak, Int. J. Chem. Tech. Res., 2, 903–907 (2010).

    Google Scholar 

  20. V. P. Orlovskii, V. S. Komlev, and S. M. Barinov, Inorg. Mater., 38, 973–984 (2002).

    Article  Google Scholar 

  21. L. Bernard, M. Freche, J. L. Lacout, and B. Biscans, Powder Technol., 103, 19–25 (1999).

    Article  Google Scholar 

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Correspondence to L. Borkowski.

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Published in Zhurnal Prikladnoi Spektroskopii, Vol. 86, No. 5, pp. 802–806, September–October, 2019.

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Borkowski, L., Wojcik, M. & Ginalska, G. A Simple Method to Evaluate the Purity of Synthetic Hydroxyapatite Granules. J Appl Spectrosc 86, 885–889 (2019). https://doi.org/10.1007/s10812-019-00910-5

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  • DOI: https://doi.org/10.1007/s10812-019-00910-5

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