This study focuses on the determination of drugs, namely nimesulide, amoxicillin, and tribulus terrestris, in an alkaline medium as well as in blood samples, urine, and commercial tablets. The study examines such factors as reproducibility, repeatability, robustness, and accuracy in the determination of the drugs in the samples.
Similar content being viewed by others
References
H. N. Deepakumari, M. K. Prashanth, B. C. Vasantha Kumar, and H. D. Revanasiddappa, J. Appl. Spectrosc., 81, 1004–1011 (2015).
N. Rajendraprasad and K. Basavaiah, J. Appl. Spectrosc., 83, 392–397 (2016).
M. M. Moein, A. El Beqqali, and M. Abdel-Rehim, J. Chromatogr. B, 1043, 3–11 (2017).
T. T. He, C. O. L. Ung, H. Hu, and Y. Wang, Eur. J. Integr Med., 7, 55–66 (2015).
P. Kaur, S. K. Singh, M. Gulati, and Y. Vaidya, J. Appl. Spectrosc., 82, 1060–1063 (2016).
X. Sun, K. Xue, X. Jiao, Q. Chen, L. Xu, H. Zheng, and Y. Ding, J. Chromatogr. B, 1027, 139–148 (2016).
A. P. Dewani, S. M. Dabhade, R. L. Bakal, C. K. Gadewar, A. V. Chandewar, and S. Patra, Arab. J. Chem., 8, 591–598 (2015).
I. M. P. Silva, M. A. Carvalho, C. S. Oliveira, D. M. Profirio, R. B. Ferreira, and P. P. Corbi, Inorg. Chem. Commun., 70, 47–50 (2016).
L. M. M. Lê, L. Eveleigh, I. Hasnaoui, P. Prognon, A. Baillet-Guffroy, and E. Caudron, J. Pharm. Biomed. Anal., 138, 249–255 (2017).
K. Shah, E. Hassan, F. Ahmed, I. Anis, M. Rabnawazand, and R. Shah, Ecotoxicol. Environ. Saf., 141, 25–29 (2017).
M. Ahmadi, T. Madrakian, and A. Afkhami, Talanta, 148, 122–128 (2016).
M. N. Uddin, S. Das, S. H. Khan, S. K. Shill, H. R. Bhuiyan, and R. Karim, J. Taibah Univ. Sci., 10, 755–765 (2016).
L. Shen, H. Wang, P. Chen, C. Yu, Y. Liang, and C. Zhang, J. Food Drug. Anal., 24, 199–205 (2016).
M. Ganzera, E. Bedir, and I. A. Khan, J. Pharm. Sci., 90, 1752–1758 (2001).
A. Saiyed, N. Jahan, S. Ajij A. Makbul, M. Ansari, H. Bano, and S. H. Habib, Integ. Med. Res., 5, 293–300 (2016).
B. C. Lourencao, R. A. Medeiros, and O. Fatibello-Filho, J. Electroanal. Chem., 754, 154–159 (2015).
A. Petruczynik, K. Wróblewski, M. Szultka-Młyńska, B. Buszewski, H. Karakuła-Juchnowicz, J. Gajewski, J. Morylowska-Topolska, and M. Waksmundzka-Hajnos, J. Pharm. Biomed. Anal., 127, 68–80 (2016).
M. S. Chernov'yants, A. O. Dolinkin, A. V. Chernyshev, E. V. Khohlov, and E. G. Golovanova, J. Pharm. Sci., 99, 1567–1573 (2010).
T. R. L. Dadamos, B. H. Freitas, D. H. M. Gênova, R. D. Espírito-Santo, E. R. P. González, S. Lanfredi, and Marcos F. S. Teixeira, Sensors Actuators B: Chem., 169, 267–273 (2012).
ANVISA. Agencia Nacional De Vigilância Sanitária. Farmacopeia Brasileira, Vol. 1, 5th ed., Brasilia (2010b).
S. L. R Ellison and A. Williams, Eurachem/CITAC guide: Quantifying Uncertainty in Analytical Measurement, 3rd ed., London, Eurachem (2012).
A. A. Gouda, M. I. K. El-Sayed, A. S. Amin, and R. E. Sheikh, Arab. J. Chem., 6, 145–163 (2013).
V. J. Pereira, R. L. Matos, S. G. Cardoso, R. O. Soares, G. L. Santana, G. M. N. Costa, and S. A. B. Vieira de Melo, J. Supercrit. Fluids, 81, 128–146 (2013).
W. Mäntele and E. Deniz, Spectrochim. Acta, A, 173, 965–968 (2017).
P. Atkins, Físico-Química: Fundamentos, 3rd ed., LTC (2003).
D. Djekic, R. Pinto, and P. A. Vorkas, Int. J. Cardiol., 222, 1042–1048 (2016).
S. L. R. Ellison, T. J. Farrant, and V. Barwick, Practical Statistics for the Analytical Scientist: A Bench Guide, Royal Society of Chemistry, UK (2009).
R. J. N. B. Silva, Talanta, 148, 177–190 (2016).
T. R. L. Dadamos and M. F. S. Teixeira, Electrochim. Acta, 54, 4552–4558 (2009).
I. Kuselman, F. Pennecchi, R. J. N. B. Silva, and D. B. Hibbert, Talanta, 164, 189–195 (2017).
M. Sega, F. Pennecchi, S. Rinaldi, and F. Rolle, Anal. Chim. Acta, 920, 10–17 (2016).
E. Theodorsson, Clin. Lab. Med., 37, 15–34 (2017).
Joint Committee for Guides in Metrology, International Vocabulary of Metrology-Basic and General Concepts and Associated Terms (VIM), JCGM 200, BIPM (2012).
Author information
Authors and Affiliations
Corresponding author
Additional information
Abstract of article is published in Zhurnal Prikladnoi Spektroskopii, Vol. 85, No. 6, p. 1022, November–December, 2018.
Rights and permissions
About this article
Cite this article
Pino, K.F.D., Oliveira, L.N., Silva, M.J. et al. Spectrophotometric Determination of Nimesulide, Tribulus terrestris, and Amoxicillin in an Alkaline Medium, in Clinical an Commercial Samples. J Appl Spectrosc 85, 1151–1157 (2019). https://doi.org/10.1007/s10812-019-00774-9
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10812-019-00774-9